Potentiometric determination of ascorbic acid in pharmaceutical preparations using a copper based mercury film electrode

1997 ◽  
Vol 16 (3) ◽  
pp. 545-551 ◽  
Author(s):  
P Riyazuddin ◽  
M.M Abdul Kamal Nazer
2013 ◽  
Vol 10 (4) ◽  
pp. 498-504 ◽  
Author(s):  
Lorena Martiniano ◽  
Joseany Almeida ◽  
Glene Cavalcante ◽  
Edmar Marques ◽  
Teresa Fonseca ◽  
...  

2013 ◽  
Vol 11 (5) ◽  
pp. 736-741 ◽  
Author(s):  
Robert Piech ◽  
Beata Paczosa-Bator

AbstractThe renewable mercury film electrode, applied for the determination of papaverine traces using differential pulse adsorptive stripping voltammetry (DP AdSV) is presented. The calibration graph obtained for papaverine is linear from 1.25 nM (0.42 µg L−1) to 95 nM (32.2 µg L−1) for a preconcentration time of 60 s, with correlation coefficient of 0.998. For the renewable mercury electrode (Hg(Ag)FE) with a surface area of 9.1 mm2 the detection limit for a preconcentration time of 60 s is 0.7 nM (0.24 µg L−1). The repeatability of the method at a concentration level of the analyte as low as 17 µg L−1, expressed as RSD is 3.3% (n=5). The proposed method was successfully applied and validated by studying the recovery of papaverine from drugs, urine and synthetic solution.


1994 ◽  
Vol 349 (7) ◽  
pp. 546-551 ◽  
Author(s):  
María Pedrero ◽  
Belén Casado ◽  
F. Javier Manuel de Villena ◽  
Jose M. Pingarrón

2006 ◽  
Vol 61 (1) ◽  
pp. 72-76 ◽  
Author(s):  
S. V. Kovaleva ◽  
V. P. Gladyshev ◽  
T. B. Rubinskaya

2011 ◽  
Vol 14 (1) ◽  
pp. 22-27 ◽  
Author(s):  
Arnaldo Aguiar Castro ◽  
Ricardo Queiroz Aucelio ◽  
Nicolas Adrian Rey ◽  
Eliane Monsores Miguel ◽  
Percio Augusto Mardini Farias

1991 ◽  
Vol 245 ◽  
pp. 177-181 ◽  
Author(s):  
Gioacchino Scarano ◽  
Cristina Romei ◽  
Alfredo Seritti ◽  
Alberto Zirino

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