A cost-effective acid digestion method using closed polypropylene tubes for inductively coupled plasma optical emission spectrometry (ICP-OES) analysis of plant essential elements

2011 ◽  
Vol 3 (12) ◽  
pp. 2854 ◽  
Author(s):  
Matthew S. Wheal ◽  
Teresa O. Fowles ◽  
Lyndon T. Palmer
2018 ◽  
Vol 273 ◽  
pp. 159-166 ◽  
Author(s):  
Darya Ilieva ◽  
Andriana Surleva ◽  
Manuela Murariu ◽  
Gabi Drochioiu ◽  
Mohd Mustafa Al Bakri Abdullah

This study is aimed at development of an analytical method for the determination of heavy metals and arsenicin waste material from barite recovery by dual view inductively coupled plasma optical emission spectrometry (ICP-OES) after wet digestion. Aquaregia open digestion method was used for sample preparation. A soil certified reference material was used to study the efficiency of wet digestion procedure applied to sterile dump material. The sensitivity, accuracy, and precision of the method were determined. The achieved detection limits are: Arsenic (As) 0.80; Copper (Cu) 0.29; Lead (Pb) 0.29; Zink (Zn) 0.30; Cadmium (Cd) 0.11; Chromium (Cr) 0.09; Nickel (Ni) 0.02, mg.kg-1.The developed method is applied for the determination of hazardous metals and arsenic in sterile dump material from closed barite mine in the region of Tarnita-Suceava, Romania.


Author(s):  
Masoud Aghahoseini ◽  
Gholamhassan Azimi ◽  
M. K. Amini

Determination of traces of Cd, Co, Cu, Mn and Pb elements in zirconium and its alloys by inductively coupled plasma optical emission spectrometry (ICP OES) suffers from severe spectral interferences...


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