Crystal structure of 1,2 : 5,6 : 9,10 : 13,14 : 17,18 : 21,22 : 25,26 : 29,30 : 33,34 : 37,38 decabenzo-3,7,11,15,19,23,27,31,35,39-decadehydro[40]annulene (C80H40), a 40-membered macrocyclic ring and the synthesis and characterization of its 80-(C160H80), 120-(C240H120), 160-(C320H160) and 200-(C400H200) membered ring homologues

1994 ◽  
pp. 1257 ◽  
Author(s):  
Kyle P. Baldwin ◽  
Richard S. Simons ◽  
John Rose ◽  
Paul Zimmerman ◽  
David M. Hercules ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Membered Ring ◽  
Synthesis And Characterization ◽  
Macrocyclic Ring

Synthese und Charakterisierung achtgliedriger Cyclometallaphosphazene von Niob(V) und Titan(IV) sowie cyclischer und acyclischer Verbindungen von Molybdän(VI) mit Perfluoralkyl-Gruppen – Kristallstruktur von [Ph2PNONbCl3]2 · 4 MeCN / Synthesis and Characterization of Eight-Membered Dimetallacyclophosphazenes with Niobium(V) and Titanium(IV) and Cyclic as well as Acyclic Compounds of Molybdenum(VI) Containing Perfluoroalkyl-Groups – X-Ray Crystal Structure of [Ph2PNONbCl3]2·4MeCN

1992 ◽  
Vol 47 (11) ◽  
pp. 1609-1613 ◽  
Author(s):  
Petra Olms ◽  
Herbert W. Roesky ◽  
Klaus Keller ◽  
Mathias Noltemeyer
Keyword(s):  
Crystal Structure ◽  
Membered Ring ◽  
Synthesis And Characterization ◽  
X Ray ◽  
Ring Compounds

Me3SiOPPh2NSiMe3 (1) reacts with NbCl5 and CpTiCl3 to form the eight-membered ring compounds [Ph2PNONbCl3]2 (2) and [Ph2PNOTiClCp]2 (3). The reaction of (C2F5)2P(Cl)=NSiMe3 (4) with MoO2Cl2 and MoOCl4 in CH2C12 quantitatively yields the compounds [MoOCl3-O-P(C2F5)2=NSiMe3]4 (5) and (C2F5)2P(Cl)=N-MoOCl3 (6).Through recrystallization from MeCN, compound 2 has been isolated and characterized by means of X-ray analysis as the MeCN adduct 2 a.

Synthesis and characterization of monomeric siloxo palladium(II) complexes: crystal structure of [Pd(tmeda)(C6F5)(OSiPh3)]

2004 ◽  
Vol 689 (11) ◽  
pp. 1872-1875 ◽  
Author(s):  
José Ruiz ◽  
Consuelo Vicente ◽  
Venancio Rodrı́guez ◽  
Natalia Cutillas ◽  
Gregorio López ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Synthesis And Characterization

Synthesis and characterization of isocyanide containing rhenium(III) complexes trans-[ReCl3(CNR)(PPh3)2] and crystal structure of trans-[ReCl3(CN-t-C4H9)(PPh3)2]

1995 ◽  
Vol 232 (1-2) ◽  
pp. 235-239 ◽  
Author(s):  
Hartmut Spies ◽  
Matthias Glaser ◽  
F.Ekkehardt Hahn ◽  
Thomas Lügger ◽  
Dieter Scheller
Keyword(s):  
Crystal Structure ◽  
Synthesis And Characterization
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