The solvothermal synthesis and characterization of quaternary arsenic chalcogenides CsTMAsQ3 (TM = Hg, Cd; Q = S, Se) using Cs+ as a structure directing agent: from 1D anionic chains to 2D anionic layers

Xin-Yu Tian; Cui-Xia Du; GeTu ZhaoRi; MuGe SheLe; Yongsheng Bao; Menghe Baiyin

doi:10.1039/d0ra05058j

The solvothermal synthesis and characterization of quaternary arsenic chalcogenides CsTMAsQ3 (TM = Hg, Cd; Q = S, Se) using Cs+ as a structure directing agent: from 1D anionic chains to 2D anionic layers

RSC Advances ◽

10.1039/d0ra05058j ◽

2020 ◽

Vol 10 (57) ◽

pp. 34903-34909

Author(s):

Xin-Yu Tian ◽

Cui-Xia Du ◽

GeTu ZhaoRi ◽

MuGe SheLe ◽

Yongsheng Bao ◽

...

Keyword(s):

Solvothermal Synthesis ◽

Mixed Solvents ◽

Synthesis And Characterization ◽

Structure Directing Agent

Presented is a method involving TM–As–Q (TM = Hg, Cd; Q = S, Se) quaternary arsenic chalcogenides and different mixed solvents which has been used to synthesize four new quaternary chalcogenide compounds.

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Solvothermal synthesis and characterization of LaPO4 with hierarchical nanostructure in mixed solvents of ethanol and water

Materials Letters ◽

10.1016/j.matlet.2014.03.092 ◽

2014 ◽

Vol 124 ◽

pp. 173-176 ◽

Cited By ~ 8

Author(s):

Ming-Guo Ma ◽

Fu Deng ◽

Ke Yao

Keyword(s):

Solvothermal Synthesis ◽

Mixed Solvents ◽

Synthesis And Characterization ◽

Hierarchical Nanostructure

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Solvothermal Synthesis and Characterization of Hierarchical Calcium Carbonate Spheres

Advanced Materials Research ◽

10.4028/www.scientific.net/amr.912-914.318 ◽

2014 ◽

Vol 912-914 ◽

pp. 318-320 ◽

Cited By ~ 1

Author(s):

Yin Xia Chen ◽

Xian Bing Ji ◽

Yu Lian Quan

Keyword(s):

Calcium Carbonate ◽

Solvothermal Synthesis ◽

Mixed Solvents ◽

Average Diameter ◽

Synthesis And Characterization ◽

Solvothermal Process ◽

X Ray Diffraction ◽

X Ray ◽

Experimental Parameters

Hierarchical calcium carbonate spheres composed of nanoparticles has been successfully synthesized via a solvothermal process. The structures are fabricated by the reaction of Ca (CH3COO)2with (CO(NH2)2) at 110 °C in diethylene glycolwater mixed solvents in the presence of polyvinylpyrrolidone. The as-prepared products were characterized by field emission scanning electron microscopy (FESEM) and X-ray diffraction (XRD). The characterization results revealed that the average diameter of the hierarchical calcium carbonate spheres is about 5 μm, and the size of the nanoparticals range from 50 to 100 nm. In addition, a small amount of bundle-like aragonite calcium carbonate is also obtained in the experimental parameters.

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