scholarly journals Reversible rearrangement of magnetic nanoparticles in solution studied using time-resolved SAXS method

2019 ◽  
Vol 26 (4) ◽  
pp. 1294-1301
Author(s):  
Lanqing Huang ◽  
Jingeng Mai ◽  
Qihui Zhu ◽  
Zhen Guo ◽  
Siying Qin ◽  
...  

Superparamagnetic nanoparticles have broad applications in biology and medicines. Quantitative measurements of magnetic beads in solution are essential in gaining comprehensive understanding of their dynamics and developing applications. Here, using synchrotron X-ray sources combined with well controlled magnetic fields, the results from small-angle X-ray scattering (SAXS) experiments on superparamagnetic particles in solution under the influence of external magnetic fields are reported. The particles mostly remain in monodispersed states and the linear aggregates tend to be aligned with the external magnetic field. After removing the magnetic fields, the superparamagnetic nanoparticles quickly recover to their original states indicating high reversibility of the rearrangement under the control of a magnetic field. The external magnetic field instrument composed of paired permanent magnets is integrated into the SAXS beamline at the Shanghai Synchrotron Radiation Facility providing a platform for studying time-resolved dynamics induced by magnetic fields.

2014 ◽  
Vol 70 (a1) ◽  
pp. C149-C149
Author(s):  
Bruce Gaulin

Magnetic fields obtained by discharging a large capacitor bank through Helmholtz coils can be produced in excess of 25 T for relatively short periods of time, ~ 1 msec and longer. When combined with modern facilities for diffraction at modern neutron and synchrotron x-ray sources, one can study the structure and phase diagrams of new materials under extremes of magnetic field. I will present two such studies, each focussing on a new magnetic material which exhibit exotic low temperature states. I will show time-resolved neutron Laue diffraction on the multiferroic magnet MnWO4 [1], and time-resolved synchrotron x-ray studies of large magneto-elastic effects in the geometrically-frustarted pyrochlore magnet Tb2Ti2O7 [2], both in magnetic fields up to ~ 30 T. Such studies of new materials in extreme sample environments can be very revealing as to the nature of their exotic low temperature states.


RSC Advances ◽  
2021 ◽  
Vol 11 (25) ◽  
pp. 15422-15427
Author(s):  
Petr A. Chernavsky ◽  
Nellie V. Kim ◽  
Victor A. Andrianov ◽  
Yurii D. Perfiliev ◽  
Alla A. Novakova ◽  
...  

The kinetics of hydrogen reduction of magnetite was investigated in different magnetic fields.


RSC Advances ◽  
2021 ◽  
Vol 11 (28) ◽  
pp. 17051-17057
Author(s):  
Anna Eichler-Volf ◽  
Yara Alsaadawi ◽  
Fernando Vazquez Luna ◽  
Qaiser Ali Khan ◽  
Simon Stierle ◽  
...  

PS/CoPd Janus particles respond very sensitively to application of low external magnetic fields. Owing to the magnetic properties, the PS/CoPd particles may be used, for example, to sense the presence of weak magnetic fields as micro-magnetometers.


2021 ◽  
Vol 3 (4) ◽  
Author(s):  
Yogesh Kumar ◽  
Rabia Sultana ◽  
Prince Sharma ◽  
V. P. S. Awana

AbstractWe report the magneto-conductivity analysis of Bi2Se3 single crystal at different temperatures in a magnetic field range of ± 14 T. The single crystals are grown by the self-flux method and characterized through X-ray diffraction, Scanning Electron Microscopy, and Raman Spectroscopy. The single crystals show magnetoresistance (MR%) of around 380% at a magnetic field of 14 T and a temperature of 5 K. The Hikami–Larkin–Nagaoka (HLN) equation has been used to fit the magneto-conductivity (MC) data. However, the HLN fitted curve deviates at higher magnetic fields above 1 T, suggesting that the role of surface-driven conductivity suppresses with an increasing magnetic field. This article proposes a speculative model comprising of surface-driven HLN and added quantum diffusive and bulk carriers-driven classical terms. The model successfully explains the MC of the Bi2Se3 single crystal at various temperatures (5–200 K) and applied magnetic fields (up to 14 T).


2015 ◽  
Vol 15 (1) ◽  
pp. 41-48 ◽  
Author(s):  
Matthias Ratajczak ◽  
Thomas Wondrak ◽  
Klaus Timmel ◽  
Frank Stefani ◽  
Sven Eckert

AbstractIn continuous casting DC magnetic fields perpendicular to the wide faces of the mold are used to control the flow in the mold. Especially in this case, even a rough knowledge of the flow structure in the mold would be highly desirable. The contactless inductive flow tomography (CIFT) allows to reconstruct the dominating two-dimensional flow structure in a slab casting mold by applying one external magnetic field and by measuring the flow-induced magnetic fields outside the mold. For a physical model of a mold with a cross section of 140 mm×35 mm we present preliminary measurements of the flow field in the mold in the presence of a magnetic brake. In addition, we show first reconstructions of the flow field in a mold with the cross section of 400 mm×100 mm demonstrating the upward scalability of CIFT.


2016 ◽  
Vol 12 (S329) ◽  
pp. 369-372
Author(s):  
C. L. Fletcher ◽  
V. Petit ◽  
Y. Nazé ◽  
G. A. Wade ◽  
R. H. Townsend ◽  
...  

AbstractRecent spectropolarimetric surveys of bright, hot stars have found that ~10% of OB-type stars contain strong (mostly dipolar) surface magnetic fields (~kG). The prominent paradigm describing the interaction between the stellar winds and the surface magnetic field is the magnetically confined wind shock (MCWS) model. In this model, the stellar wind plasma is forced to move along the closed field loops of the magnetic field, colliding at the magnetic equator, and creating a shock. As the shocked material cools radiatively it will emit X-rays. Therefore, X-ray spectroscopy is a key tool in detecting and characterizing the hot wind material confined by the magnetic fields of these stars. Some B-type stars are found to have very short rotational periods. The effects of the rapid rotation on the X-ray production within the magnetosphere have yet to be explored in detail. The added centrifugal force due to rapid rotation is predicted to cause faster wind outflows along the field lines, leading to higher shock temperatures and harder X-rays. However, this is not observed in all rapidly rotating magnetic B-type stars. In order to address this from a theoretical point of view, we use the X-ray Analytical Dynamical Magnetosphere (XADM) model, originally developed for slow rotators, with an implementation of new rapid rotational physics. Using X-ray spectroscopy from ESA’s XMM-Newton space telescope, we observed 5 rapidly rotating B-types stars to add to the previous list of observations. Comparing the observed X-ray luminosity and hardness ratio to that predicted by the XADM allows us to determine the role the added centrifugal force plays in the magnetospheric X-ray emission of these stars.


2018 ◽  
Vol 6 ◽  
Author(s):  
A. Rigby ◽  
J. Katz ◽  
A. F. A. Bott ◽  
T. G. White ◽  
P. Tzeferacos ◽  
...  

Magnetic field measurements in turbulent plasmas are often difficult to perform. Here we show that for ${\geqslant}$kG magnetic fields, a time-resolved Faraday rotation measurement can be made at the OMEGA laser facility. This diagnostic has been implemented using the Thomson scattering probe beam and the resultant path-integrated magnetic field has been compared with that of proton radiography. Accurate measurement of magnetic fields is essential for satisfying the scientific goals of many current laser–plasma experiments.


2021 ◽  
Vol 105 ◽  
pp. 184-193
Author(s):  
Ilya Aleksandrovich Frolov ◽  
Andrei Aleksandrovich Vorotnikov ◽  
Semyon Viktorovich Bushuev ◽  
Elena Alekseevna Melnichenko ◽  
Yuri Viktorovich Poduraev

Magnetorheological braking devices function due to the organization of domain structures between liquid and solid magnetic materials under the action of an electromagnetic or magnetic field. The disc is most widely used as a rotating braking element that made of a solid magnetic material due to the large area of contact with a magnetorheological fluid. Many factors affect the braking characteristics of the magnetorheological disc brake. Specifically, the value of the magnetic field and how the field is distributed across the work element is significantly affected at the braking torque. There are different ways to generate a magnetic field. In this study, the method of installation of permanent magnets into the construction, allowing to increase the braking torque of the magnetorheological disc brake is proposed. Simulation modelling showing the distribution of the magnetic field across the disk depending on the installation of permanent magnets with different pole orientations were carried out. The model takes into account the possibility of increasing the gap between solid magnetic materials of the structure, inside them which the magnetorheological fluid is placed. Comparative estimation of the distribution of the magnetic fields depending on the chosen method of installation of permanent magnets with different orientations of their poles is carried out. Further research is planned to focus on a comparative assessment of the distribution of magnetic fields depending on the selected material of the braking chamber.


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