High temperature solution calorimetry. Part 1. Development of a spherical solution calorimeter
Keyword(s):
A high temperature solution calorimeter of a novel design has been developed whereby the separated components are brought together and mixed within a completely enclosed, vacuum-sealed cell. The instrument consists of an inner spherical compartment containing the reaction cell, surrounded by a number of concentric spherical shells made of Inconel alloy. The calorimeter may be operated at temperatures up to 1 200 °C. The temperature-sensing circuit includes a differential thermopile, a d-c. microvolt amplifier, and a recording millivoltmeter. With this instrument calorific effects of the order of 0.1 cal could be detected.
2002 ◽
Vol 163
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pp. 186-193
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1987 ◽
Vol 51
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pp. 1755-1763
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1978 ◽
Vol 10
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pp. 243-248
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1978 ◽
Vol 42
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pp. 367-375
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2011 ◽
Vol 56
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pp. 585-592
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2013 ◽
Vol 113
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pp. 189-197
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1994 ◽
Vol 9
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pp. 3121-3124
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