Room Temperature Electrochemical Synthesis of Oxygenates through a Carbonate Anion Pathway

2012 ◽  
Keyword(s):  
Electrochemical Synthesis ◽  
Room Temperature ◽  
Carbonate Anion

scholarly journals Scaling Up the Production of Electrodeposited Nanowires: A Roadmap towards Applications

Nanomaterials ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 1657
Author(s):  
Claudia Fernández-González ◽  
Jesús C. Guzmán-Mínguez ◽  
Alejandra Guedeja-Marrón ◽  
Eduardo García-Martín ◽  
Michael Foerster ◽  
...  
Keyword(s):  
Electrochemical Synthesis ◽  
Room Temperature ◽  
Scaling Up ◽  
Magnetic Configuration ◽  
Metallic Nanowires ◽  
Production Time ◽  
Novel Synthesis ◽  
Conventional Methods

The use of metallic nanowires is mostly reduced to scientific areas where a small quantity of nanostructures are needed. In order to broaden the applicability of these nanomaterials, it is necessary to establish novel synthesis protocols that provide a larger amount of nanowires than the conventional laboratory fabrication processes at a more competitive cost. In this work, we propose several modifications to the conventional electrochemical synthesis of nanowires in order to increase the production with considerably reduced production time and cost. To that end, we use a soft anodization procedure of recycled aluminum at room temperature to produce the alumina templates, followed by galvanostatic growth of CoFe nanowires. We studied their morphology, composition and magnetic configuration, and found that their properties are very similar to those obtained by conventional methods.

One-step electrochemical synthesis of Bi3.84W0.16O6.24 with superior photocatalytic activities

RSC Advances ◽  
2015 ◽  
Vol 5 (26) ◽  
pp. 20234-20237 ◽  
Author(s):  
Zuwei Song ◽  
Hui Dai ◽  
Jiantao Tong
Keyword(s):  
Electrochemical Synthesis ◽  
Room Temperature ◽  
Photocatalytic Activities ◽  
One Step

Bi3.84W0.16O6.24 nanoparticles were successfully prepared by a facile electrochemical route at room temperature in just 10 minutes.

Room Temperature Electrochemical Synthesis of Crystalline GaOOH Nanoparticles from Expanding Liquid Metals

Langmuir ◽  
2018 ◽  
Vol 34 (26) ◽  
pp. 7604-7611 ◽  
Author(s):  
Benchaporn Lertanantawong ◽  
Jamie D. Riches ◽  
Anthony P. O’Mullane
Keyword(s):  
Electrochemical Synthesis ◽  
Room Temperature ◽  
Liquid Metals

The room temperature electrochemical synthesis of N-doped graphene and its electrocatalytic activity for oxygen reduction

2015 ◽  
Vol 51 (7) ◽  
pp. 1198-1201 ◽  
Author(s):  
Feng-Xiang Ma ◽  
Jiong Wang ◽  
Feng-Bin Wang ◽  
Xing-Hua Xia
Keyword(s):  
Oxygen Reduction ◽  
Electrochemical Synthesis ◽  
Electrocatalytic Activity ◽  
Active Sites ◽  
Room Temperature ◽  
N Source ◽  
N Doping ◽  
Doped Graphene ◽  
Electrochemical Energy

N doping in graphene can be achieved using a facile and mild approach using electrochemical energy at room temperature with ammonia as the N source, which occurs at the carbon active sites generated in situ during the removal of oxygen containing species at cathodic potentials.

Electrochemical Synthesis of Sulfinic Esters via Aerobic Oxidative Esterification of Thiophenols with Alcohols

Synthesis ◽  
2020 ◽  
Vol 52 (18) ◽  
pp. 2705-2712 ◽  
Author(s):  
Jingya Yang ◽  
Xi-Cun Wang ◽  
Hongyan Zhou ◽  
Jiaokui Duan ◽  
Dongtai Xie ◽  
...  
Keyword(s):  
Electrochemical Synthesis ◽  
Oxidative Coupling ◽  
Room Temperature ◽  
Reaction Conditions ◽  
Oxidative Esterification ◽  
Scale Preparation ◽  
Redox Reagent ◽  
Sulfinic Esters

A method for the electrochemical synthesis of sulfinic esters by aerobic oxidative coupling of thiophenols and alcohols has been developed. Using electrons as the redox reagent and O2 in air as the oxygen source, the reactions proceeded smoothly at room temperature, even for a gram-scale preparation. No use of catalyst, clean redox reagent, green and abundant oxygen source, and mild reaction conditions make this strategy eco-friendly.

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