scholarly journals Laser Powder Bed Fusion of Pure Tungsten: Effects of Process Parameters on Morphology, Densification, Microstructure

Materials ◽  
2020 ◽  
Vol 14 (1) ◽  
pp. 165
Author(s):  
Junfeng Li ◽  
Yunxiao Wu ◽  
Bokang Zhou ◽  
Zhengying Wei

Tungsten has been widely used in many industrial fields due to its excellent properties. However, owing to its characteristics of inherent brittleness at room temperature and high melting point, it is difficult to prepare tungsten parts with high complexity via traditional methods. In the present work, tungsten samples were prepared by laser powder bed fusion. The influence of each process parameter including laser power, scanning speed, and hatch spacing on the surface morphology, densification, and microstructure of tungsten samples was systematically investigated. The results showed that the use of the appropriate parameters, especially high laser power, can effectively improve the surface quality and obtain a dense surface. The tungsten samples with a relative density of 98.31% were obtained with optimized parameter combinations: a laser power of 300 W, scanning speed of 400 mm/s, and hatch spacing of 0.08 mm. Compared with scanning speed and hatch spacing, the laser power had a more obvious influence on the relative density. Additionally, for the grain morphology by microstructure inspection, elongated curved grains gradually transformed into fine straight columnar grains as the scanning speed increased. The hatch spacing would change the grain morphology slightly but had no significant effect on the grain size.

Materials ◽  
2021 ◽  
Vol 14 (11) ◽  
pp. 2945
Author(s):  
Mohamed Abdelhafiz ◽  
Kassim S. Al-Rubaie ◽  
Ali Emadi ◽  
Mohamed A. Elbestawi

The process–structure–property relationships of copper laser powder bed fusion (L-PBF)-produced parts made of high purity copper powder (99.9 wt %) are examined in this work. A nominal laser beam diameter of 100 μm with a continuous wavelength of 1080 nm was employed. A wide range of process parameters was considered in this study, including five levels of laser power in the range of 200 to 370 W, nine levels of scanning speed from 200 to 700 mm/s, six levels of hatch spacing from 50 to 150 μm, and two layer thickness values of 30 μm and 40 μm. The influence of preheating was also investigated. A maximum relative density of 96% was obtained at a laser power of 370 W, scanning speed of 500 mm/s, and hatch spacing of 100 μm. The results illustrated the significant influence of some parameters such as laser power and hatch spacing on the part quality. In addition, surface integrity was evaluated by surface roughness measurements, where the optimum Ra was measured at 8 μm ± 0.5 μm. X-ray photoelectron spectroscopy (XPS) and energy-dispersive X-ray spectroscopy (EDX) were performed on the as-built samples to assess the impact of impurities on the L-PBF part characteristics. The highest electrical conductivity recorded for the optimum density-low contaminated coils was 81% IACS.


Author(s):  
Felix Schmeiser ◽  
Erwin Krohmer ◽  
Christian Wagner ◽  
Norbert Schell ◽  
Eckart Uhlmann ◽  
...  

AbstractLaser powder bed fusion is an additive manufacturing process that employs highly focused laser radiation for selective melting of a metal powder bed. This process entails a complex heat flow and thermal management that results in characteristic, often highly textured microstructures, which lead to mechanical anisotropy. In this study, high-energy X-ray diffraction experiments were carried out to illuminate the formation and evolution of microstructural features during LPBF. The nickel-base alloy Inconel 625 was used for in situ experiments using a custom LPBF system designed for these investigations. The diffraction patterns yielded results regarding texture, lattice defects, recrystallization, and chemical segregation. A combination of high laser power and scanning speed results in a strong preferred crystallographic orientation, while low laser power and scanning speed showed no clear texture. The observation of a constant gauge volume revealed solid-state texture changes without remelting. They were related to in situ recrystallization processes caused by the repeated laser scanning. After recrystallization, the formation and growth of segregations were deduced from an increasing diffraction peak asymmetry and confirmed by ex situ scanning transmission electron microscopy. Graphical Abstract


2021 ◽  
pp. 107680
Author(s):  
Sayed Ehsan Saghaian ◽  
Mohammadreza Nematollahi ◽  
Guher Toker ◽  
Alejandro Hinojos ◽  
Narges Shayesteh Moghaddam ◽  
...  

2021 ◽  
Author(s):  
ling zhang ◽  
Wenhe Liao ◽  
Tingting Liu ◽  
Huiliang Wei ◽  
Changchun Zhang

Abstract The printing quality of the laser powder bed fusion (LPBF) components largely depends on the presence of various defects such as massive porosity. Thus, the efficient elimination of pores is an important factor to the production of a sound LPBF product. In this work, the efficacy of two in situ laser remelting approaches on the elimination of pores during LPBF of a titanium alloy Ti-6.5Al-3.5Mo-l.5Zr-0.3Si (TC11) were assessed using both experimental and computational methods. These two remelting methods are the surface remelting, and the layer-by-layer printing and remelting. A multi-track and multi-layer phenomenological model was established to compute the evolution of pores with the temperature and velocity fields. The results showed that surface remelting with a high laser power such as 180 W laser can effectively eliminate pores within three deposited layers. However, such a remelting cannot reach defects in deeper regions. Alternatively, the layer-by-layer remelting with a laser power of 180 W can effectively eliminate the pores formed in the previous layer in real time. The results obtained from this work can provide useful guidance for the in situ control of printing defects supported by the real time monitoring, feedback and operation systems of the intelligent LPBF equipment.


Author(s):  
Yunpeng Ren ◽  
Heng Lu ◽  
Dongyang Xu ◽  
Yan Chen ◽  
Zhiduo Xin ◽  
...  

Laser powder bed fusion additive manufacturing of superalloys has received increasing attention in these years. In this article, the influence of parameters of laser powder bed fusion on mechanical properties and microstructures of nickel-based superalloy GH536 was investigated. Influence of laser power, scanning speed, hatch space and building direction on mechanical properties was discussed, and the optimal parameters were obtained. The relative density of samples fabricated by laser powder bed fusion could be as high as 99.5%. The processing window of laser energy density with 8.56 × 104–1.15 × 105 J/cm3 should be employed to make sure that the relative density is higher than 98%. The ultimate tensile strength and yield stress of GH536 sample made by laser powder bed fusion were 950 and 606 MPa, respectively, which were superior to samples with the tensile strength of 767 MPa and yield strength of 379 MPa prepared by traditional hot forging method. The hardness of the sample could reach 316.8 HV.


2019 ◽  
Vol 3 (1) ◽  
pp. 21 ◽  
Author(s):  
Morgan Letenneur ◽  
Alena Kreitcberg ◽  
Vladimir Brailovski

A simplified analytical model of the laser powder bed fusion (LPBF) process was used to develop a novel density prediction approach that can be adapted for any given powder feedstock and LPBF system. First, calibration coupons were built using IN625, Ti64 and Fe powders and a specific LPBF system. These coupons were manufactured using the predetermined ranges of laser power, scanning speed, hatching space, and layer thickness, and their densities were measured using conventional material characterization techniques. Next, a simplified melt pool model was used to calculate the melt pool dimensions for the selected sets of printing parameters. Both sets of data were then combined to predict the density of printed parts. This approach was additionally validated using the literature data on AlSi10Mg and 316L alloys, thus demonstrating that it can reliably be used to optimize the laser powder bed metal fusion process.


2021 ◽  
Vol ahead-of-print (ahead-of-print) ◽  
Author(s):  
You-Cheng Chang ◽  
Hong-Chuong Tran ◽  
Yu-Lung Lo

Purpose Laser powder bed fusion (LPBF) provides the means to produce unique components with almost no restriction on geometry in an extremely short time. However, the high-temperature gradient and high cooling rate produced during the fabrication process result in residual stress, which may prompt part warpage, cracks or even baseplate separation. Accordingly, an appropriate selection of the LPBF processing parameters is essential to ensure the quality of the built part. This study, thus, aims to develop an integrated simulation framework consisting of a single-track heat transfer model and a modified inherent shrinkage method model for predicting the curvature of an Inconel 718 cantilever beam produced using the LPBF process. Design/methodology/approach The simulation results for the curvature of the cantilever beam are calibrated via a comparison with the experimental observations. It is shown that the calibration factor required to drive the simulation results toward the experimental measurements has the same value for all settings of the laser power and scanning speed. Representative combinations of the laser power and scanning speed are, thus, chosen using the circle packing design method and supplied as inputs to the validated simulation framework to predict the corresponding cantilever beam curvature and density. The simulation results are then used to train artificial neural network models to predict the curvature and solid cooling rate of the cantilever beam for any combination of the laser power and scanning speed within the input design space. The resulting processing maps are screened in accordance with three quality criteria, namely, the part density, the radius of curvature and the solid cooling rate, to determine the optimal processing parameters for the LPBF process. Findings It is shown that the parameters lying within the optimal region of the processing map reduce the curvature of the cantilever beam by 17.9% and improve the density by as much as 99.97%. Originality/value The present study proposes a computational framework, which could find the parameters that not only yield the lowest distortion but also produce fully dense components in the LPBF process.


Author(s):  
J. C. Heigel ◽  
B. M. Lane

This work presents high speed thermographic measurements of the melt pool length during single track laser scans on nickel alloy 625 substrates. Scans are made using a commercial laser powder bed fusion machine while measurements of the radiation from the surface are made using a high speed (1800 frames per second) infrared camera. The melt pool length measurement is based on the detection of the liquidus-solidus transition that is evident in the temperature profile. Seven different combinations of programmed laser power (49 W to 195 W) and scan speed (200 mm/s to 800 mm/s) are investigated and numerous replications using a variety of scan lengths (4 mm to 12 mm) are performed. Results show that the melt pool length reaches steady state within 2 mm of the start of each scan. Melt pool length increases with laser power, but its relationship with scan speed is less obvious because there is no significant difference between cases performed at the highest laser power of 195 W. Although keyholing appears to affect the anticipated trends in melt pool length, further research is required.


2019 ◽  
Vol 164 ◽  
pp. 107534 ◽  
Author(s):  
Hahn Choo ◽  
Kin-Ling Sham ◽  
John Bohling ◽  
Austin Ngo ◽  
Xianghui Xiao ◽  
...  

Materials ◽  
2022 ◽  
Vol 15 (2) ◽  
pp. 450
Author(s):  
Johan Lindwall ◽  
Andreas Lundbäck ◽  
Jithin James Marattukalam ◽  
Anders Ericsson

The development of process parameters and scanning strategies for bulk metallic glass formation during additive manufacturing is time-consuming and costly. It typically involves trials with varying settings and destructive testing to evaluate the final phase structure of the experimental samples. In this study, we present an alternative method by modelling to predict the influence of the process parameters on the crystalline phase evolution during laser-based powder bed fusion (PBF-LB). The methodology is demonstrated by performing simulations, varying the following parameters: laser power, hatch spacing and hatch length. The results are compared in terms of crystalline volume fraction, crystal number density and mean crystal radius after scanning five consecutive layers. The result from the simulation shows an identical trend for the predicted crystalline phase fraction compared to the experimental estimates. It is shown that a low laser power, large hatch spacing and long hatch lengths are beneficial for glass formation during PBF-LB. The absolute values show an offset though, over-predicted by the numerical model. The method can indicate favourable parameter settings and be a complementary tool in the development of scanning strategies and processing parameters for additive manufacturing of bulk metallic glass.


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