scholarly journals 3C-SiC Nanowires In-Situ Modified Carbon/Carbon Composites and Their Effect on Mechanical and Thermal Properties

Nanomaterials ◽  
2018 ◽  
Vol 8 (11) ◽  
pp. 894 ◽  
Author(s):  
Hongjiao Lin ◽  
Hejun Li ◽  
Qingliang Shen ◽  
Xiaohong Shi ◽  
Tao Feng ◽  
...  
Keyword(s):  
Shear Strength ◽  
Thermal Properties ◽  
Sol Gel ◽  
Interlaminar Shear Strength ◽  
Mechanical And Thermal Properties ◽  
Initial Oxidation ◽  
Sic Nanowires ◽  
Out Of Plane ◽  
Interlaminar Shear

An in-situ, catalyst-free method for synthesizing 3C-SiC ceramic nanowires (SiCNWs) inside carbon–carbon (C/C) composites was successfully achieved. Obtained samples in different stages were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), and Raman scattering spectroscopy. Results demonstrated that the combination of sol-gel impregnation and carbothermal reduction was an efficient method for in-situ SiCNW synthesis, inside C/C composites. Thermal properties and mechanical behaviors—including out-of-plane and in-plane compressive strengths, as well as interlaminar shear strength (ILLS) of SiCNW modified C/C composites—were investigated. By introducing SiCNWs, the initial oxidation temperature of C/C was increased remarkably. Meanwhile, out-of-plane and in-plane compressive strengths, as well as interlaminar shear strength (ILLS) of C/C composites were increased by 249.3%, 109.2%, and 190.0%, respectively. This significant improvement resulted from simultaneous reinforcement between the fiber/matrix (F/M) and matrix/matrix (M/M) interfaces, based on analysis of the fracture mechanism.

scholarly journals In Situ Study on Fracture Behavior of Z-Pinned Carbon Fiber-Reinforced Aluminum Matrix Composite via Scanning Electron Microscope (SEM)

Materials ◽  
2019 ◽  
Vol 12 (12) ◽  
pp. 1941
Author(s):  
Yunhe Zhang ◽  
Sian Wang ◽  
Xiwang Zhao ◽  
Fanming Wang ◽  
Gaohui Wu
Keyword(s):  
Stainless Steel ◽  
Shear Strength ◽  
Electron Microscope ◽  
Carbon Fiber ◽  
Aluminum Matrix ◽  
Aluminum Matrix Composite ◽  
Interlaminar Shear Strength ◽  
Interlaminar Shear ◽  
Scanning Electron

Inside a scanning electron microscope (SEM) chamber, we performed an in situ interlaminar shear test on a z-pinned carbon fiber-reinforced aluminum matrix composite (Cf/Al) fabricated by the pressure the infiltration method to understand its failure mechanism. Experiments show that introducing a stainless-steel z-pin increases the interlaminar shear strength of Cf/Al composite by 148%. The increase in interlaminar shear strength is attributed to the high strength of the stainless-steel z-pin and the strong bonding between the z-pin and the matrix. When the z-pin/matrix interface failed, the z-pin can still experience large shear deformation, thereby enhancing delamination resistance. The failure mechanism of composite includes interfacial debonding, aluminum plough, z-pin shear deformation, frictional sliding, and fracture. These results in this study will help us understand the interlaminar strengthening mechanism of z-pins in the delamination of metal matrix composites.

scholarly journals Enhanced Mechanical and Thermal Properties of Modified Oil Palm Fiber-Reinforced Polypropylene Composite via Multi-Objective Optimization of In Situ Silica Sol-Gel Synthesis

Polymers ◽  
2021 ◽  
Vol 13 (19) ◽  
pp. 3338
Author(s):  
Nasrullah Mat Rozi ◽  
Hamidah Abdul Hamid ◽  
Md. Sohrab Hossain ◽  
Nor Afifah Khalil ◽  
Ahmad Naim Ahmad Yahaya ◽  
...  
Keyword(s):  
Thermal Properties ◽  
Oil Palm ◽  
Sol Gel ◽  
Silica Sol ◽  
Mechanical And Thermal Properties ◽  
Fiber Reinforced ◽  
Palm Fiber ◽  
In Situ Silica ◽  
Sol Gel Process

A multi-objective optimization of in situ sol-gel process was conducted in preparing oil palm fiber-reinforced polypropylene (OPF-PP) composite for an enhancement of mechanical and thermal properties. Tetraethyl orthosilicate (TEOS) and butylamine were used as precursors and catalysts for the sol-gel process. The face-centered central composite design (FCCD) experiments coupled with response surface methodology (RSM) has been utilized to optimize in situ silica sol-gel process. The optimization process showed that the drying time after the in-situ silica sol-gel process was the most influential factor on silica content, while the molar ratio of TEOS to water gave the most significant effect on silica residue. The maximum silica content of 34.1% and the silica residue of 35.9% were achieved under optimum conditions of 21.3 h soaking time, 50 min drying time, pH value of 9.26, and 1:4 molar ratio of TEOS to water. The untreated oil palm fiber (OPF) and silica sol-gel modified OPF (SiO2-OPF) were used as the reinforcing fibers, with PP as a matrix and maleic anhydride grafted polypropylene (MAgPP) as a compatibilizer for the fiber-reinforced PP matrix (SiO2-OPF-PP-MAgPP) composites preparation. The mechanical and thermal properties of OPF-PP, SiO2-OPF-PP, SiO2-OPF-PP-MAgPP composites, and pure PP were determined. It was found that the OPF-S-PP-MAgPP composite had the highest toughness and stiffness with values of tensile strength, Young’s modulus, and elongation at break of 30.9 MPa, 881.8 MPa, and 15.1%, respectively. The thermal properties analyses revealed that the OPF-S-PP-MAgPP exhibited the highest thermally stable inflection point at 477 °C as compared to pure PP and other composites formulations. The finding of the present study showed that the SiO2-OPF had the potential to use as a reinforcing agent to enhance the thermal-mechanical properties of the composites.

Mechanical properties of multiwall carbon nanotubes/unidirectional carbon fiber-reinforced epoxy hybrid nanocomposites in transverse and longitudinal fiber directions

2021 ◽  
pp. 096739112098651
Author(s):  
Saeedeh Saadatyar ◽  
Mohammad Hosain Beheshty ◽  
Razi Sahraeian
Keyword(s):  
Mechanical Properties ◽  
Shear Strength ◽  
Epoxy Resin ◽  
Interlaminar Shear Strength ◽  
Lap Shear Strength ◽  
Transverse Tensile ◽  
Lap Shear ◽  
Longitudinal Fiber ◽  
Interlaminar Shear ◽  
Multiwall Carbon

Unidirectional carbon fiber-reinforced epoxy (UCFRE) is suffering from weak transverse mechanical properties and through-thickness properties. The effect of different amount (0.1, 0.3 and 0.5 phr which is proportional to 0.09, 0.27 and 0.46 wt%, respectively) of multiwall carbon nanotube (MWCNT), on transverse tensile properties, flexural strength, fracture toughness in transverse and longitudinal fiber directions, interlaminar shear strength and lap shear strength of UCFRE has been investigated. Dicyandiamide was used as a thermal curing agent of epoxy resin. MWCNT was dispersed in the epoxy resin by ultrasonic instrument and their dispersion state was investigated by scanning electron microscopy (SEM). The curing behavior of epoxy resin and its nanocomposites was assessed by differential scanning calorimetry. Results show that transverse tensile strength, modulus and strain-at-break were increased by 28.5%, 25% and 14%, respectively by adding 0.1 phr of MWCNT. Longitudinal flexural properties of UCFRE was not changed by adding different amount of MWCNT. Although longitudinal flexural strength was increased by 5% by adding 0.1 phr of MWCNT. Fracture toughness in transverse and longitudinal fiber directions was increased by 39% and 9%, respectively at 0.3 phr of MWCNT. Results also show that interlaminar shear strength and lap shear strength were increased at 0.3 phr of MWCNT by 8% and 5%, respectively. These increases in mechanical properties were due to the good adhesion of fibers to the matrix, interlocking and toughening action of MWCNT as revealed by SEM.

Effect of consolidation force on interlaminar shear strength of CF/PEEK laminates manufactured by laser-assisted forming

2021 ◽  
Vol 266 ◽  
pp. 113779
Author(s):  
Qiuyu Miao ◽  
Zhihong Dai ◽  
Guangyi Ma ◽  
Fangyong Niu ◽  
Dongjiang Wu
Keyword(s):  
Shear Strength ◽  
Interlaminar Shear Strength ◽  
Interlaminar Shear

Surface and Composite Interface of Carbon Fiber Modified by Grafting of Diethanolamine

2009 ◽  
Vol 79-82 ◽  
pp. 497-500 ◽  
Author(s):  
Lei Chen ◽  
Zhi Wei Xu ◽  
Jia Lu Li ◽  
Xiao Qing Wu ◽  
Li Chen
Keyword(s):  
Shear Strength ◽  
Carbon Fiber ◽  
Functional Groups ◽  
Carbon Fibers ◽  
Irradiation Dose ◽  
Interlaminar Shear Strength ◽  
Epoxy Composites ◽  
Composite Interface ◽  
Γ Ray ◽  
Interlaminar Shear

The γ-ray co-irradiation method was employed to study the effect of diethanolamine modification on the surface of carbon fiber (CF) and the interfacial properties of CF/epoxy composites. Compared with the original carbon fiber, the surface of modified fibers became rougher. The amount of oxygen-containing functional groups was increased and the nitrogen element was detected after irradiation grafting. The interlaminar shear strength (ILSS) of composites reinforced by carbon fibers irradiated in diethanolamine solution was increased and then decreased as the irradiation dose increased. The ILSS of CF/epoxy composites was enhanced by 16.1% at 200kGy dose, compared with that of untreated one. The γ-ray irradiation grafting is expected to be a promising method for the industrialized modification of carbon fibers.

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