Preparation and characterization of nickel oxide nanoparticles via solid state thermal decomposition of dinuclear nickel(II) Schiff base complex [Ni2(Brsal-1,3-ph)2] as a new precursor

2013 ◽  
Vol 41 (1) ◽  
pp. 357-363 ◽  
Author(s):  
Aliakbar Dehno Khalaji ◽  
Mahsa Nikookar ◽  
Debasis Das
Keyword(s):  
Thermal Decomposition ◽  
Schiff Base ◽  
Solid State ◽  
Nickel Oxide ◽  
Schiff Base Complex ◽  
Oxide Nanoparticles ◽  
Nickel Oxide Nanoparticles ◽  
Base Complex

Synthesis and characterization of a manganese(III) schiff base complex and exploration of Br···Br interaction in the solid state structure of the complex

2019 ◽  
Vol 72 (19-21) ◽  
pp. 3237-3247 ◽  
Author(s):  
Ipsita Mondal ◽  
Kousik Ghosh ◽  
Antonio Franconetti ◽  
Antonio Frontera ◽  
Sudipta Chatterjee ◽  
...  
Keyword(s):  
Schiff Base ◽  
Solid State ◽  
Schiff Base Complex ◽  
Synthesis And Characterization ◽  
State Structure ◽  
Base Complex ◽  
Solid State Structure

Preparation and Characterization of Copper Oxide Nanoparticles Through Solid State Thermal Decomposition of an Aqua Nitrato Copper(II) Complex with a Tridentate Schiff-base Ligand as a New Precursor

2018 ◽  
Vol 9 (1) ◽  
pp. 92-100 ◽  
Author(s):  
Niaz Monadi ◽  
Samira Saeednia ◽  
Parvaneh Iranmanesh ◽  
Mehdi H. Ardakani ◽  
Samira Sinaei
Keyword(s):  
Thermal Decomposition ◽  
Schiff Base ◽  
Solid State ◽  
Copper Oxide ◽  
Schiff Base Ligand ◽  
Copper Oxide Nanoparticles ◽  
Cuo Nanoparticles ◽  
Oxide Nanoparticles ◽  
Tridentate Schiff Base

Introduction: In this study the synthesis and characterization of copper oxide nanoparticles via solid state thermal decomposition of a recently synthesized aqua nitrato copper(II) complex with a tridentate Schiff-base ligand (1) as a new precursor are reported. Materials & Methods: The copper complexes were obtained by sonochemical and solvothermal process and characterized by Scanning Electron Microscopy (SEM), X-ray powder Diffraction (XRD) and FT-IR spectroscopy. The thermal stability of compound (1) was studied by Thermogravimetric Analysis (TGA). The amount of initial reagents and the role of reaction time on size and morphology of nanostructure compound (1) were studied. CuO nanoparticles were simply synthesized at 500 oC under air atmosphere. Results & Conclusion: The diameter of CuO nanoparticles was estimated to be about 200 and 30 nm from copper complex precursor obtained by sonochemical and solvothermal methods respectively.

scholarly journals Synthesis and characterization of a mononuclear zinc(ii) Schiff base complex: on the importance of C–H⋯π interactions

RSC Advances ◽  
2021 ◽  
Vol 11 (48) ◽  
pp. 30148-30155
Author(s):  
Tanmoy Basak ◽  
Antonio Frontera ◽  
Shouvik Chattopadhyay
Keyword(s):  
Schiff Base ◽  
Solid State ◽  
Dft Calculations ◽  
Schiff Base Complex ◽  
Synthesis And Characterization ◽  
Computational Tool ◽  
Base Complex ◽  
Π Interactions

The strength of the C–H⋯π interaction in the solid state of [ZnL(H2O)]·H2O has been evaluated using DFT calculations and also analysed using the MEP surface and NCI plot index computational tool.

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