Influence on the temperature of the high speed steel substrate on the interface composition and adhesion of TiN hard coating deposited by cathodic arc

Vacuum ◽  
1992 ◽  
Vol 43 (5-7) ◽  
pp. 685-687 ◽  
Author(s):  
E Román ◽  
JL de Segovia ◽  
A Alberdi ◽  
J Calvo ◽  
J Laucirica
2021 ◽  
Vol 2059 (1) ◽  
pp. 012015
Author(s):  
M Sh Migranov ◽  
A M Migranov ◽  
S R Shekhtman

Abstract The paper presents the results of a study of one of the ways to increase the wear resistance of “duplex” coatings applied to cutting tools, which are due to preliminary diffusion saturation of the tool surface with nitrogen (known as ion nitriding) followed by physical deposition of a hard coating (Ti, Cr) N. The proposed coating also contains an additional layer with an impurity of ions, deposited on a preliminary nitrided surface of high speed steel before the deposition of a hard coating. Tests were carried out to evaluate the effect of these modified layers on the tool life of the HSS tool. The greatest wear resistance after "triplex" - treatment was achieved during ion implantation of titanium into a pre-nitrided surface. The coefficient of friction of the modified layer was studied at different contact temperatures. Ionic mixing contributes to the appearance of a thin surface layer with an amorphous-like structure, which prolongs the stage of normal wear, which significantly increases the tool life as a result of the self-organization process.


2019 ◽  
Vol 1393 ◽  
pp. 012084
Author(s):  
E G Grigoryev ◽  
K L Smirnov ◽  
E L Strizhakov ◽  
S V Neskoromniy

2011 ◽  
Vol 675-677 ◽  
pp. 1307-1310 ◽  
Author(s):  
Xiao Hong Yao ◽  
Bin Tang ◽  
Lin Hai Tian ◽  
Xiao Fang Li ◽  
Yong Ma

TiN coating with thickness of 2.5μm was deposited on high-speed steel (HSS) substrate by pulsed bias cathodic arc ion plating. The surface and cross-section morphologies, composition depth profile and phase structure were characterized by FESEM, GDOES and XRD, respectively. Scratch test for adhesion evaluation, microhardness test for hardness measurement, and potentiodynamic polarization for corrosion resistance test were used. The results show that the TiN coating exhibits smooth surface, dense columnar grain structure and an obviously preferred orientation of TiN(111). The adhesion of the coating to substrate is exceeded more than 100N. The hardness of the coating is about 26 GPa. The low corrosion current density (Icorr) and rather high corrosion potential (Ecorr) value imply that the TiN coating displays a good corrosion resistance in 0.5mol/l NaCl solution. However, pitting is still existed due to the defects in the coating.


2018 ◽  
Vol 437 ◽  
pp. 257-270 ◽  
Author(s):  
A.S. Chaus ◽  
P. Pokorný ◽  
Ľ. Čaplovič ◽  
M.V. Sitkevich ◽  
J. Peterka

2013 ◽  
Vol 62 (9) ◽  
pp. 096802
Author(s):  
Han Liang ◽  
Liu De-Lian ◽  
Chen Xian ◽  
Zhao Yu-Qing

MRS Advances ◽  
2018 ◽  
Vol 3 (18) ◽  
pp. 949-955
Author(s):  
Gongsheng Song ◽  
Qiang Fu ◽  
Chunxu Pan

ABSTRACTIn this paper, a multilayer CNx/TiN composite film on high-speed steel substrate was prepared by using a multi-arc assisted DC reactive magnetron sputtering system. The cross-section observations of the fracture surface reveal that the films show a pure cleavage fracture due to its super-high hardness, and the interfacial strength between the film and substrate is associates with the film thickness, i.e., 2μm is a critical thickness for the present deposition. That is to say, there is no disbonding or cracking at the interface when the film thickness is less than 2μm, while the interfacial failure is generated if the film thickness is larger than 2μm. This direct SEM observation of the fracture surface provides a distinct image for evaluating the mechanical property and also analyzing the failure mechanism of the films.


2014 ◽  
Vol 604 ◽  
pp. 67-70
Author(s):  
Leonid Kupchenko ◽  
Rauno Tali ◽  
Eron Adoberg ◽  
Valdek Mikli ◽  
Vitali Podgursky

TiN coatings with different thickness were prepared by arc ion plating (AIP) physical vapor deposition (PVD) on high speed steel (HSS) substrates. TiN coatings surface roughness was investigated by atomic force microscopy (AFM) and 3D optical profilometry and growth kinetics was described using scaling exponents β and α. The growth exponent β is 0.91-1.0 and the roughness exponent α is 0.77-0.81. Due to relatively high value of the exponent α, the surface diffusion is likely predominant smoothening mechanism of TiN growth.


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