Highly efficient preparation of β-CD-based chiral monolithic column by “one-pot” hydroxymethyl polycondensation for enantioseparation in capillary liquid chromatography

2020 ◽  
Vol 1616 ◽  
pp. 460781
Author(s):  
Rongguo Chen ◽  
Chenchen Lin ◽  
Haixia Lyu ◽  
Xucong Lin ◽  
Zenghong Xie
Keyword(s):  
Liquid Chromatography ◽  
Monolithic Column ◽  
Capillary Liquid Chromatography ◽  
One Pot ◽  
Highly Efficient ◽  
Capillary Liquid

Facile one-pot preparation of an imidazolium embedded C8 hybrid monolith using polyhedral oligomeric silsesquioxane for capillary liquid chromatography

RSC Advances ◽  
2015 ◽  
Vol 5 (111) ◽  
pp. 91436-91440 ◽  
Author(s):  
Niu Zhang ◽  
Lu Zhang ◽  
Xiaoqiang Qiao ◽  
Yongli Wang ◽  
Hongyuan Yan ◽  
...  
Keyword(s):  
Liquid Chromatography ◽  
Monolithic Column ◽  
Polyhedral Oligomeric Silsesquioxane ◽  
Capillary Liquid Chromatography ◽  
One Pot ◽  
Oligomeric Silsesquioxane ◽  
Capillary Liquid ◽  
Hybrid Monolithic Column

In this study, a novel imidazolium embedded C8 hybrid monolithic column based on polyhedral oligomeric silsesquioxane (POSS) was developed.

Facile one-pot preparation of chiral monoliths with a well-defined framework based on the thiol–ene click reaction for capillary liquid chromatography

RSC Advances ◽  
2016 ◽  
Vol 6 (30) ◽  
pp. 24835-24842 ◽  
Author(s):  
Peng Zhang ◽  
Jiannan Wang ◽  
Haiguan Yang ◽  
Linjing Su ◽  
Yuhao Xiong ◽  
...  
Keyword(s):  
Liquid Chromatography ◽  
Click Reaction ◽  
Capillary Liquid Chromatography ◽  
Fused Silica ◽  
One Pot ◽  
Fused Silica Capillary ◽  
Capillary Liquid ◽  
Silica Capillary

A novel chiral cyclodextrin (CD) monolith was easily prepared via a one-pot process based on the thiol–ene click reaction of allyl-β-CD with pentaerythritol tetra-(3-mercaptopropionate) in a fused-silica capillary.

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