Weak anion-exchange mixed-mode materials to selectively extract acidic compounds by stir bar sorptive extraction from environmental waters

2021 ◽  
pp. 462748
Author(s):  
Joan Carles Nadal ◽  
Mónica Catalá-Icardo ◽  
Francesc Borrull ◽  
José Manuel Herrero-Martínez ◽  
Rosa Maria Marcé ◽  
...  
2015 ◽  
Vol 30 (1) ◽  
pp. 162-171 ◽  
Author(s):  
Xiangju Mao ◽  
Wenying Fan ◽  
Man He ◽  
Beibei Chen ◽  
Bin Hu

A simple, rapid and sensitive method of C18-SBSE-HPLC-ICP-MS for the speciation of butyltins in environmental waters and sediments.


Author(s):  
Yamile Pérez-Padilla ◽  
Saúl Ariel Medina Cetina ◽  
Alejandro Ávila-Ortega ◽  
Jesús Alberto Barrón-Zambrano ◽  
Alfredo Rafael Vilchis-Néstor ◽  
...  

Analytical pretreatment has become environmental-friendly because of material science assistance. In stir bar sorptive extraction (SBSE), a coating is typically used to isolate and preconcentrate organic compounds in aqueous samples. Here, a translucent coating based on polydimethylsiloxane and phenyltriethoxysilane was prepared by a sol-gel method. Characterization tests showed that the coating was homogeneous, relatively polar, and both thermally (< 400 °C) and chemically stable. Coated stir bars were evaluated in the SBSE experiments. Benzene derivatives were successfully extracted/preconcentrated from aqueous solutions and environmental waters. Furanic derivatives and antibiotics were moderately extracted from water, but they were extracted from isooctane.


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