scholarly journals Characterization and source term assessments of radioactive particles from Marshall Islands using non-destructive analytical techniques

2006 ◽  
Vol 61 (8) ◽  
pp. 971-979 ◽  
Author(s):  
J. Jernström ◽  
M. Eriksson ◽  
R. Simon ◽  
G. Tamborini ◽  
O. Bildstein ◽  
...  
Keyword(s):  
Source Term ◽  
Analytical Techniques ◽  
Marshall Islands ◽  
Non Destructive

X-Ray Tomography for Electronic Packages

2000 ◽  
Author(s):  
Deepak Goyal
Keyword(s):  
3D Imaging ◽  
Development Time ◽  
Analytical Techniques ◽  
Electronic Packages ◽  
X Ray ◽  
Imaging Capability ◽  
Imaging Results ◽  
Key Drivers ◽  
Analytical Tools ◽  
Non Destructive

Abstract Next generation assembly/package development challenges are primarily increased interconnect complexity and density with ever shorter development time. The results of this trend present some distinct challenges for the analytical tools/techniques to support this technical roadmap. The key challenge in the analytical tools/techniques is the development of non-destructive imaging for improved time to information. This paper will present the key drivers for the non-destructive imaging, results of literature search and evaluation of key analytical techniques currently available. Based on these studies requirements of a 3D imaging capability will be discussed. Critical breakthroughs required for development of such a capability are also summarized.

Textile Museum Collections. SIM Method Validation for the Assessment of Pesticides

2021 ◽  
Vol 58 (3) ◽  
pp. 1-10
Author(s):  
Elena-Cornelia Mitran ◽  
Irina-Mariana Sandulache ◽  
Cristina-Mihaela Lite ◽  
Lucian Gabriel Radu
Keyword(s):  
Analytical Techniques ◽  
High Sensitivity ◽  
Pest Infestation ◽  
Accuracy And Precision ◽  
Cis And Trans Isomers ◽  
Quantitative Results ◽  
Cis And Trans ◽  
High Degree ◽  
Non Destructive ◽  
Detection And Quantification

In time the environmental conditions could damage textiles (materials/ artifacts) causing the need to develop better non-destructive or at least micro-destructive analysis techniques of the samples. There are ethnographic textile artifacts that were treated in the past with various pesticides, that have not been mentioned in any document. These are often re-treated with chemicals by museum staff as a method of preventing pest infestation. Due to the progressive use of many pesticides, this paper was focused on the detection and quantification of three pesticides: malathion, methoxychlor, and permethrin (cis- and trans- isomers). Gas chromatography is one of the most widely used analytical techniques for characterizing volatile organic compounds and therefore was the analytical method of choice for the present study. Because these analytes are found at trace levels, the detection and quantification limits of analytes are very small and it is necessary to optimize and validate a SIM method - that allows the mass spectrometer to detect specific compounds with high sensitivity. In SIM mode, the instrument is set to collect data at selected masses of interest, thus increasing the accuracy and precision of the quantitative results. The present paper is aimed to develop this type of method with specificity and selectivity, high precision (expressed in terms of repeatability and intermediate accuracy), accuracy, suitable working range and linearity, and high degree of series� homogenity.

scholarly journals Worth a Closer Look: Raman Spectra of Lead-Pipe Scale

Minerals ◽  
2021 ◽  
Vol 11 (10) ◽  
pp. 1047
Author(s):  
Jill Dill Pasteris ◽  
Yeunook Bae ◽  
Daniel E. Giammar ◽  
Sydney N. Dybing ◽  
Claude H. Yoder ◽  
...  
Keyword(s):  
Cross Sections ◽  
Water System ◽  
Analytical Techniques ◽  
Real Time Analysis ◽  
Fiber Optic Probes ◽  
Lead Pipe ◽  
Lead Pipes ◽  
Non Destructive

The identification and characterization of lead-bearing and associated minerals in scales on lead pipes are essential to understanding and predicting the mobilization of lead into drinking water. Despite its long-recognized usefulness in the unambiguous identification of crystalline and amorphous solids, distinguishing between polymorphic phases, and rapid and non-destructive analysis on the micrometer spatial scale, the Raman spectroscopy (RS) technique has been applied only occasionally in the analysis of scales in lead service lines (LSLs). This article illustrates multiple applications of RS not just for the identification of phases, but also compositional and structural characterization of scale materials in harvested lead pipes and experimental pipe-loop/recirculation systems. RS is shown to be a sensitive monitor of these characteristics through analyses on cross-sections of lead pipes, raw interior pipe walls, particulates captured in filters, and scrapings from pipes. RS proves to be especially sensitive to the state of crystallinity of scale phases (important to their solubility) and to the specific chemistry of phases precipitated upon the introduction of orthophosphate to the water system. It can be used effectively alone as well as in conjunction with more standard analytical techniques. By means of fiber-optic probes, RS has potential for in situ, real-time analysis within water-filled pipes.

scholarly journals Cultural Heritage Chemistry

2018 ◽  
Vol 40 (2) ◽  
pp. 58-59
Author(s):  
Daniel Rabinovich
Keyword(s):  
Analytical Chemistry ◽  
Cultural Heritage ◽  
Analytical Techniques ◽  
Profound Influence ◽  
Works Of Art ◽  
Analytical Instrumentation ◽  
Non Destructive ◽  
Modern Analytical ◽  
Destructive Methods

Abstract The tools of analytical chemistry, and the expertise and enthusiasm of many of its practitioners, have had a profound influence in the field of cultural heritage [1, 2]. Analytical techniques, especially those involving non-destructive methods of examination, have played a key role in the characterization, restoration, and preservation of an incredible range of works of art and cultural heritage, including ceramics, textiles, paintings, books, drawings, sculptures, jewelry, and a myriad of artifacts made of glass, wood, or metal. In addition, modern analytical instrumentation has been successfully applied to study the techniques used to produce heritage materials, to verify the authorship or estimate the date of pieces of art, and to detect reproductions and forgeries.

scholarly journals Polychromy on the Antonine Wall Distance Sculptures: Non-destructive Identification of Pigments on Roman Reliefs

Britannia ◽  
2020 ◽  
Vol 51 ◽  
pp. 175-201
Author(s):  
Louisa Campbell
Keyword(s):  
Material Culture ◽  
Materials Science ◽  
Analytical Techniques ◽  
Composition Analysis ◽  
Raman Spectrometry ◽  
X Ray ◽  
Wall Distance ◽  
Depositional Processes ◽  
Non Destructive

ABSTRACTNon-destructive analytical techniques are now widely and successfully employed in the fields of materials science and conservation. Portable X-ray fluorescence (pXRF) and portable Raman spectrometry have proven particularly valuable for the rapid in-situ analysis of samples, but their applicability for the analysis of archaeological artefacts for which survival of surface treatments can be negatively impacted by post-depositional processes has been underexplored. Roman relief-sculpted monumental inscriptions from the Antonine Wall, commonly referred to as ‘Distance Slabs’, have offered an excellent opportunity to deploy these non-destructive techniques to determine whether they were originally adorned with pigments and, if so, to identify the colours used. This is a revolutionary approach to identifying colours on ancient sandstone sculpture that transforms our understanding of these unique monuments. Elemental composition analysis by pXRF has confirmed evidence for pigments and this is supported by the Raman results, making it possible to develop and reconstruct a palette of colours that originally brought these monuments to life in vibrant polychrome. The research offers a new methodology for identifying pigments on sandstone sculpture and opens new avenues for investigating other classes of material culture alongside the development of bespoke analytical equipment.

Identification of purple dye from molluscs on an excavated textile by non-destructive analytical techniques

2013 ◽  
Vol 96 (3) ◽  
pp. 774-780 ◽  
Author(s):  
Christina Margariti ◽  
Stavros Protopapas ◽  
Norman Allen ◽  
Vladimir Vishnyakov
Keyword(s):  
Analytical Techniques ◽  
Non Destructive
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