Direct Magnetic Excitation of Cantilevers for Dynamic Force Microscocopy in Liquids

1999 ◽  
Vol 5 (S2) ◽  
pp. 1002-1003
Author(s):  
S.M. Lindsay
Keyword(s):  
Acoustic Excitation ◽  
Dynamic Force ◽  
Viscous Damping ◽  
Driving Frequency ◽  
Magnetic Excitation ◽  
Force Microscopy ◽  
Wide Range ◽  
Recognition Imaging ◽  
Afm Cantilever ◽  
Body Recognition

The mechanical Q-factor of an AFM cantilever immersed in fluid is reduced to a small value (ca. 3) owing to viscous damping. Thus, a large driving force is needed to excite the cantilever into bending motion in fluid. There are two common methods for exciting cantilevers for dynamic force microscopy in fluids, illustrated in Figure 1. Fig. la illustrates acoustic excitation in which a piezoelectric transducer displaces the base of the cantilever, causing bending motion of the cantilever when the driving frequency is near to a bending resonance of the cantilever. Fig. lb shows magnetic excitation. In magnetic excitation, a magnetic field is used to cause bending of a magnetic cantilever either through magnetostriction or MXB forces.Acoustic excitation has the highest amplitude at mechanical resonances of the cantilever housing, with the result that the response is dominated by these sharp features,Fig. 2a. In contrast, the response to magnetic excitation is intrinsic to the cantilever, Fig. 2b. Thus, magnetic excitation permits the cantilever to be driven over a wide range of frequencies. This is important for calibration of the amplitude and for experiments involving time and concentration dependence in tip-sample interactions, e.g., anti-body recognition imaging.

Generalized Heterodyne Configurations for Photo-induced Force Microscopy

2019 ◽  
Author(s):  
Le Wang ◽  
Devon Jakob ◽  
Haomin Wang ◽  
Alexis Apostolos ◽  
Marcos M. Pires ◽  
...  
Keyword(s):  
Spatial Resolution ◽  
Repetition Rate ◽  
Modulation Frequency ◽  
High Harmonic ◽  
Chemical Imaging ◽  
Heterodyne Detection ◽  
Force Microscopy ◽  
Wide Range ◽  
The Difference ◽  
Afm Cantilever

<div>Infrared chemical microscopy through mechanical probing of light-matter interactions by atomic force microscopy (AFM) bypasses the diffraction limit. One increasingly popular technique is photo-induced force microscopy (PiFM), which utilizes the mechanical heterodyne signal detection between cantilever mechanical resonant oscillations and the photo induced force from light-matter interaction. So far, photo induced force microscopy has been operated in only one heterodyne configuration. In this article, we generalize heterodyne configurations of photoinduced force microscopy by introducing two new schemes: harmonic heterodyne detection and sequential heterodyne detection. In harmonic heterodyne detection, the laser repetition rate matches integer fractions of the difference between the two mechanical resonant modes of the AFM cantilever. The high harmonic of the beating from the photothermal expansion mixes with the AFM cantilever oscillation to provide PiFM signal. In sequential heterodyne detection, the combination of the repetition rate of laser pulses and polarization modulation frequency matches the difference between two AFM mechanical modes, leading to detectable PiFM signals. These two generalized heterodyne configurations for photo induced force microscopy deliver new avenues for chemical imaging and broadband spectroscopy at ~10 nm spatial resolution. They are suitable for a wide range of heterogeneous materials across various disciplines: from structured polymer film, polaritonic boron nitride materials, to isolated bacterial peptidoglycan cell walls. The generalized heterodyne configurations introduce flexibility for the implementation of PiFM and related tapping mode AFM-IR, and provide possibilities for additional modulation channel in PiFM for targeted signal extraction with nanoscale spatial resolution.</div>

Experimental Investigation On Nonlinear Response of a Low-Swirl Flame to Acoustic Excitation with Large Amplitude

2021 ◽  
Author(s):  
Weijie Liu ◽  
Liang Zhang ◽  
Ranran Xue ◽  
Qian Yang ◽  
Huiru Wang
Keyword(s):  
Heat Release ◽  
Nonlinear Response ◽  
High Efficiency ◽  
Axial Direction ◽  
Limit Cycle Oscillation ◽  
Acoustic Excitation ◽  
Driving Frequency ◽  
Thermoacoustic Instability ◽  
Wide Range ◽  
Swirl Flame

Abstract Thermoacoustic instability is a major issue in developing high-efficiency low emission gas turbine combustors. In order to predict the amplitude of limit cycle oscillation, an understanding of the amplitude dependent response of the flame, i.e. the nonlinear response, to large acoustic excitation is needed. In the present study, the nonlinear response of a low-swirl CH4/air premixed flame to acoustic excitation is experimentally studied. Amplitude dependences of flame dynamic at 75 Hz and 195 Hz are discussed in detail over a wide range of excitation level. Experimental results show the gain of flame describing function of the low-swirl flame has a peak value at 65 Hz and a local minimum at 105 Hz which is caused by the destructive (out of phase) and constructive (in phase) of the axial and azimuthal velocity fluctuation. At low perturbation level, flame heat release fluctuation is in linear relationship with the normalized velocity driving level. Heat release fluctuation begins to saturate at a certain level which depends on the driving frequency. The low-swirl flame oscillates mainly in the axial direction at 75 Hz while it is in the radial direction at 195 Hz. The non-linear flame heat release response is a result of combination effect of flame rollup process and harmonic responses.

Molecular recognition imaging using tuning fork-based transverse dynamic force microscopy

2010 ◽  
Vol 110 (6) ◽  
pp. 605-611 ◽  
Author(s):  
Manuel Hofer ◽  
Stefan Adamsmaier ◽  
Thomas S. van Zanten ◽  
Lilia A. Chtcheglova ◽  
Carlo Manzo ◽  
...  
Keyword(s):  
Molecular Recognition ◽  
Tuning Fork ◽  
Dynamic Force ◽  
Force Microscopy ◽  
Transverse Dynamic ◽  
Recognition Imaging

Generalized Heterodyne Configurations for Photo-induced Force Microscopy

2019 ◽  
Author(s):  
Le Wang ◽  
Devon Jakob ◽  
Haomin Wang ◽  
Alexis Apostolos ◽  
Marcos M. Pires ◽  
...  
Keyword(s):  
Spatial Resolution ◽  
Repetition Rate ◽  
Modulation Frequency ◽  
High Harmonic ◽  
Chemical Imaging ◽  
Heterodyne Detection ◽  
Force Microscopy ◽  
Wide Range ◽  
The Difference ◽  
Afm Cantilever

<div>Infrared chemical microscopy through mechanical probing of light-matter interactions by atomic force microscopy (AFM) bypasses the diffraction limit. One increasingly popular technique is photo-induced force microscopy (PiFM), which utilizes the mechanical heterodyne signal detection between cantilever mechanical resonant oscillations and the photo induced force from light-matter interaction. So far, photo induced force microscopy has been operated in only one heterodyne configuration. In this article, we generalize heterodyne configurations of photoinduced force microscopy by introducing two new schemes: harmonic heterodyne detection and sequential heterodyne detection. In harmonic heterodyne detection, the laser repetition rate matches integer fractions of the difference between the two mechanical resonant modes of the AFM cantilever. The high harmonic of the beating from the photothermal expansion mixes with the AFM cantilever oscillation to provide PiFM signal. In sequential heterodyne detection, the combination of the repetition rate of laser pulses and polarization modulation frequency matches the difference between two AFM mechanical modes, leading to detectable PiFM signals. These two generalized heterodyne configurations for photo induced force microscopy deliver new avenues for chemical imaging and broadband spectroscopy at ~10 nm spatial resolution. They are suitable for a wide range of heterogeneous materials across various disciplines: from structured polymer film, polaritonic boron nitride materials, to isolated bacterial peptidoglycan cell walls. The generalized heterodyne configurations introduce flexibility for the implementation of PiFM and related tapping mode AFM-IR, and provide possibilities for additional modulation channel in PiFM for targeted signal extraction with nanoscale spatial resolution.</div>

Experimental Investigation on Nonlinear Response of a Low-Swirl Flame to Acoustic Excitation with Large Amplitude

2021 ◽  
Author(s):  
Weijie Liu ◽  
Liang Zhang ◽  
Ranran Xue ◽  
Qian Yang ◽  
Huiru Wang
Keyword(s):  
Heat Release ◽  
Nonlinear Response ◽  
High Efficiency ◽  
Axial Direction ◽  
Limit Cycle Oscillation ◽  
Acoustic Excitation ◽  
Driving Frequency ◽  
Thermoacoustic Instability ◽  
Wide Range ◽  
Swirl Flame

Abstract Thermoacoustic instability is a major issue in developing high-efficiency low emission gas turbine combustors. In order to predict the amplitude of limit cycle oscillation, an understanding of the amplitude dependent response of the flame, i.e. the nonlinear response, to large acoustic excitation is needed. In the present study, the nonlinear response of a low-swirl CH4/air premixed flame to acoustic excitation is experimentally studied. Amplitude dependences of flame dynamic at 75 Hz and 195 Hz are discussed in detail over a wide range of excitation level. Experimental results show the gain of flame describing function of the low-swirl flame has a peak value at 65 Hz and a local minimum at 105 Hz which is caused by the destructive (out of phase) and constructive (in phase) of the axial and azimuthal velocity fluctuation. At low perturbation level, flame heat release fluctuation is in linear relationship with the normalized velocity driving level. Heat release fluctuation begins to saturate at a certain level which depends on the driving frequency. The low-swirl flame oscillates mainly in the axial direction at 75 Hz while it is in the radial direction at 195 Hz. The non-linear flame heat release response is a result of combination effect of flame rollup process and harmonic responses.

Atomic Force Microscopy (AFM) for Topography and Recognition Imaging at Single Molecule Level

2013 ◽  
pp. 102-112
Author(s):  
Memed Duman ◽  
Andreas Ebner ◽  
Christian Rankl ◽  
Jilin Tang ◽  
Lilia A. Chtcheglova ◽  
...  
Keyword(s):  
Atomic Force Microscopy ◽  
Single Molecule ◽  
Single Molecule Level ◽  
Force Microscopy ◽  
Atomic Force ◽  
Recognition Imaging

Studies of Nanomechanical Properties of Pulsed Laser Deposited NbN films on Si Using Nanoindentation

2012 ◽  
Vol 1424 ◽  
Author(s):  
M. A. Mamun ◽  
A. H. Farha ◽  
Y. Ufuktepe ◽  
H. E. Elsayed-Ali ◽  
A. A. Elmustafa
Keyword(s):  
Thin Films ◽  
Pulsed Laser ◽  
Niobium Nitride ◽  
X Ray Diffraction ◽  
Si Substrate ◽  
Force Microscopy ◽  
Atomic Force ◽  
Wide Range ◽  
Pile Up ◽  
Average Modulus

ABSTRACTNanomechanical and structural properties of pulsed laser deposited niobium nitride thin films were investigated using X-ray diffraction, atomic force microscopy, and nanoindentation. NbN film reveals cubic δ-NbN structure with the corresponding diffraction peaks from the (111), (200), and (220) planes. The NbN thin films depict highly granular structure, with a wide range of grain sizes that range from 15-40 nm with an average surface roughness of 6 nm. The average modulus of the film is 420±60 GPa, whereas for the substrate the average modulus is 180 GPa, which is considered higher than the average modulus for Si reported in the literature due to pile-up. The hardness of the film increases from an average of 12 GPa for deep indents (Si substrate) measured using XP CSM and load control (LC) modes to an average of 25 GPa measured using the DCM II head in CSM and LC modules. The average hardness of the Si substrate is 12 GPa.

SFM and TOF-SIMS Study of Novel Self-Organization phenomena in mixed LB monolayers

2002 ◽  
Vol 738 ◽  
Author(s):  
B. Pignataro ◽  
L. Sardone ◽  
A. Licciardello ◽  
G. Marletta
Keyword(s):  
Secondary Ion Mass Spectrometry ◽  
Scanning Force Microscopy ◽  
Lateral Force ◽  
Self Organization ◽  
High Mass ◽  
Molar Ratio ◽  
Force Microscopy ◽  
Tof Sims ◽  
Wide Range ◽  
Scanning Force

ABSTRACTMixed monolayers of dimyristoylphosphatidylcholine (DMPC) and quercetin palmitate (QP) in a molar ratio of 25/75 have been transferred on mica and oxygen plasma cleaned silicon by the Langmuir-Blodgett (LB) technique at different subphase temperatures. Scanning Force Microscopy (SFM) in height, phase and lateral force modes has been employed to investigate the structural and mechanical features at nanoscopic level of these samples. Although the two molecules show a wide range of miscibility at 37 °C, they give rise to phase separation at 10 °C. This last system provides a new example of nanometric scale self-organization. In particular spiral shaped domains rising from the wrapping-up of nanoscopic fiber-like structures have been observed. The high resolution achieved by the use of the dynamic scanning force microscopy operating in the net attractive regime allow to visualize characteristic nanoscopic rupture points along the supramolecular fibers. High mass resolution Time of Flight Secondary Ion Mass Spectrometry (ToF-SIMS) spectra showed DMPC- as well as QP-related peaks. The ToF-SIMS spectra from the nanostructured samples (10 °C) have been compared with those from the homogeneous ones (37 °C). The phase separated samples provides interesting secondary ions that highlight the QP supramolecular condensation within the fiber-like structures.

Thermal Response of a Viscoelastic Rod Under Cyclic Loading

1974 ◽  
Vol 41 (1) ◽  
pp. 229-233 ◽  
Author(s):  
S. Mukherjee
Keyword(s):  
Cyclic Loading ◽  
Thermal Response ◽  
Time History ◽  
Thermomechanical Coupling ◽  
Large Strains ◽  
Driving Frequency ◽  
Wide Range ◽  
History Of ◽  
Complex Young’S Modulus ◽  
Viscoelastic Rod

Thermal response of a viscoelastic rod under cyclic loading is discussed by determining the stresses and temperature in a viscoelastic rod insulated on its lateral surface and driven by a sinusoidal stress at one end. Temperature dependence of the complex Young’s modulus of the rod and the effect of thermomechanical coupling are included in the analysis. A method of finite differences is used to directly determine the steady-state stresses and temperature without obtaining the complete time history of the process. The iterative algorithm used is very efficient and converges rapidly for a wide range of driving stress amplitudes and frequencies. It is found that rapid rise of temperature to dangerous levels occurs for relatively low values of driving stress amplitudes, especially if the driving frequency is close to one of the critical frequencies of the rod. Drastic softening of the rod leads to large strains. Thus failure of the rod could occur at low values of the driving stress.

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