High pressure cell for small- and wide-angle x-ray scattering

1997 ◽  
Vol 68 (12) ◽  
pp. 4588-4592 ◽  
Author(s):  
K. Pressl ◽  
M. Kriechbaum ◽  
M. Steinhart ◽  
P. Laggner
Keyword(s):  
High Pressure ◽  
Wide Angle ◽  
High Pressure Cell ◽  
X Ray ◽  
Pressure Cell ◽  
X Ray Scattering ◽  
Ray Scattering

scholarly journals A high pressure cell for small angle X-ray scattering

1993 ◽  
Vol 03 (C8) ◽  
pp. C8-487-C8-490 ◽  
Author(s):  
M. LORENZEN ◽  
C. RIEKEL ◽  
A. EICHLER ◽  
D. HÄUSSERMANN
Keyword(s):  
High Pressure ◽  
Small Angle ◽  
High Pressure Cell ◽  
X Ray ◽  
Pressure Cell ◽  
X Ray Scattering ◽  
Ray Scattering

High hydrostatic pressure small-angle X-ray scattering cell for protein solution studies featuring diamond windows and disposable sample cells

2008 ◽  
Vol 41 (1) ◽  
pp. 167-175 ◽  
Author(s):  
Nozomi Ando ◽  
Pascale Chenevier ◽  
Martin Novak ◽  
Mark W. Tate ◽  
Sol M. Gruner
Keyword(s):  
High Pressure ◽  
Small Angle ◽  
Ambient Pressure ◽  
X Rays ◽  
High Pressure Cell ◽  
X Ray ◽  
Pressure Cell ◽  
X Ray Scattering ◽  
Solution Studies ◽  
Ray Scattering

A high-pressure cell for synchrotron small-angle X-ray scattering (SAXS) studies of protein solutions is described. The design was optimized for use at up to 400 MPa in liquid pressure and with 8−12 keV X-rays with particular emphasis on the ease of use. The high-pressure cell was fabricated from corrosion-resistant Inconel 725 (Special Metals Corporation, Huntington, WV, USA) and featured Poulter-type windows [Poulter (1932).Phys. Rev.40, 861–871]. Flat natural diamonds, 500 µm thick, were recycled from diamond anvil cells and were shown to perform well as high-pressure SAXS windows. For a simple and effective method of sample isolation, disposable plastic sample cells with a defined path length and reproducible parasitic scattering were designed. These sample cells enable efficient use of synchrotron time. The cells facilitate rapid and easy sample changes, eliminate the need to clean the cell between sample changes, and reduce the sample volume to as low as 12 µl. The disposable cells can also be used separately from the high-pressure cell for SAXS measurements at ambient pressure and temporary storage of samples. The performance of the apparatus is demonstrated with T4 lysozyme.

A Pressure-Induced Phase Transition in a Ternary Microemulsion with an Assembly of a New High-Pressure Cell and Small-Angle X-Ray Scattering Apparatus

1999 ◽  
Vol 38 (Part 1, No. 2A) ◽  
pp. 951-956 ◽  
Author(s):  
Hideki Seto ◽  
Daisuke Okuhara ◽  
Michihiro Nagao ◽  
Shigehiro Komura ◽  
Takayoshi Takeda
Keyword(s):  
Phase Transition ◽  
High Pressure ◽  
Small Angle ◽  
High Pressure Cell ◽  
X Ray ◽  
Pressure Cell ◽  
X Ray Scattering ◽  
Ray Scattering

scholarly journals Integrating in situ high pressure small and wide angle synchrotron x-ray scattering for exploiting new physics of nanoparticle supercrystals

2010 ◽  
Vol 81 (9) ◽  
pp. 093902 ◽  
Author(s):  
Zhongwu Wang ◽  
Ou Chen ◽  
Charles Y. Cao ◽  
Ken Finkelstein ◽  
Detlef-M. Smilgies ◽  
...  
Keyword(s):  
High Pressure ◽  
New Physics ◽  
Wide Angle ◽  
X Ray ◽  
X Ray Scattering ◽  
Ray Scattering

High-pressure cell for simultaneous small-angle x-ray scattering and laser light scattering measurements

2001 ◽  
Vol 72 (6) ◽  
pp. 2679-2685 ◽  
Author(s):  
Tadanori Koga ◽  
Shuiqin Zhou ◽  
Benjamin Chu ◽  
John L. Fulton ◽  
Shu Yang ◽  
...  
Keyword(s):  
High Pressure ◽  
Light Scattering ◽  
Small Angle ◽  
Laser Light ◽  
Laser Light Scattering ◽  
High Pressure Cell ◽  
X Ray ◽  
Pressure Cell ◽  
X Ray Scattering ◽  
Scattering Measurements

High-pressure instrument for small- and wide-angle x-ray scattering. II. Time-resolved experiments

1999 ◽  
Vol 70 (2) ◽  
pp. 1540-1545 ◽  
Author(s):  
M. Steinhart ◽  
M. Kriechbaum ◽  
K. Pressl ◽  
H. Amenitsch ◽  
P. Laggner ◽  
...  
Keyword(s):  
High Pressure ◽  
Wide Angle ◽  
Time Resolved ◽  
X Ray ◽  
X Ray Scattering ◽  
Ray Scattering

High-Pressure Solution X-ray Scattering of Protein Using a Hydrostatic Cell with Diamond Windows

1998 ◽  
Vol 5 (5) ◽  
pp. 1282-1286 ◽  
Author(s):  
Minoru Kato ◽  
Tetsuro Fujisawa
Keyword(s):  
High Pressure ◽  
Synthetic Diamond ◽  
Radius Of Gyration ◽  
Maximum Pressure ◽  
High Pressure Cell ◽  
X Ray ◽  
X Ray Scattering ◽  
Quantitative Analyses ◽  
Guinier Plot ◽  
Ray Scattering

A hydrostatic high-pressure cell (maximum pressure 700 MPa) with synthetic diamond windows is applied to measure small-angle X-ray scattering of a protein at high pressure. Use of the present cell allows an accurate solvent background correction, providing quantitative analyses. The performance of the present cell for X-ray scattering is shown by using lysozyme as a sample solution. From the Guinier plot, values of the radius of gyration of lysozyme are evaluated to be 15.31 ± 0.09 Å at 1 atm (0.10 MPa) and 14.80 ± 0.15 Å at 400 MPa.

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