scholarly journals The new neutron grating interferometer at the ANTARES beamline: design, principles and applications

2016 ◽  
Vol 49 (5) ◽  
pp. 1488-1500 ◽  
Author(s):  
Tommy Reimann ◽  
Sebastian Mühlbauer ◽  
Michael Horisberger ◽  
Benedikt Betz ◽  
Peter Böni ◽  
...  

Neutron grating interferometry is an advanced method in neutron imaging that allows the simultaneous recording of the transmission, the differential phase and the dark-field image. The latter in particular has recently been the subject of much interest because of its unique contrast mechanism which marks ultra-small-angle neutron scattering within the sample. Hence, in neutron grating interferometry, an imaging contrast is generated by scattering of neutrons off micrometre-sized inhomogeneities. Although the scatterer cannot be resolved, it leads to a measurable local decoherence of the beam. Here, a report is given on the design considerations, principles and applications of a new neutron grating interferometer which has recently been implemented at the ANTARES beamline at the Heinz Maier-Leibnitz Zentrum. Its highly flexible design allows users to perform experiments such as directional and quantitative dark-field imaging which provide spatially resolved information on the anisotropy and shape of the microstructure of the sample. A comprehensive overview of the neutron grating interferometer principle is given, followed by theoretical considerations to optimize the setup performance for different applications. Furthermore, an extensive characterization of the setup is presented and its abilities are demonstrated using selected case studies: (i) dark-field imaging for material differentiation, (ii) directional dark-field imaging to mark and quantify micrometre anisotropies within the sample, and (iii) quantitative dark-field imaging, providing additional size information on the sample's microstructure by probing its autocorrelation function.

2016 ◽  
Vol 49 (2) ◽  
pp. 569-573 ◽  
Author(s):  
M. Strobl ◽  
B. Betz ◽  
R. P. Harti ◽  
A. Hilger ◽  
N. Kardjilov ◽  
...  

Dark-field imaging using grating interferometers has been proven to have a high potential for applications in engineering, magnetism, and soft matter and biophysics, as well as in medicine with both neutrons and X-rays. The access to spatially resolved small-angle scattering information in neutron dark-field imaging provides information about structures beyond direct spatial image resolution. The dark-field contrast modality is hence a valuable tool for materials science based on neutron imaging. This is underlined by the success of the method, despite its current limitation to qualitative scattering information. Here it is demonstrated how a wavelength-dispersive approach allows such drawbacks to be overcome by providing quantitative structure size information and hence can introduce novel possibilities and insights for materials science.


2019 ◽  
Author(s):  
Daniel Hussey ◽  
Adam J Brooks ◽  
Jacob LaManna ◽  
David Jacobson ◽  
Leslie Butler

A novel imaging mode, neutron dark field imaging, extends the capability of neutron imaging to enable one to measure the microstructure, that is length scales from the nm to µm. The dark field is a measure of the pair correlation function, which is linked to conventional small angle. Neutron dark field images of lithium-ion batteries provide spatially resolved measurements (with resolution ~100 µm) of the particle distribution along the path of the neutron beam. We applied neutron dark-field imaging to commercial lithium-ion batteries with different capacities, states of charge, and wear. The images probed length scales from 100 nm to 3 µm. We observed a uniform dark field signal across the fresh battery in both charge states which is contrasted with the worn batteries, which show clear inhomogeneities in the dark field signal, which indicates that the underlying electrode structures have changed in a non-uniform fashion.


2011 ◽  
Vol 110 (10) ◽  
pp. 109902 ◽  
Author(s):  
Michael Chabior ◽  
Tilman Donath ◽  
Christian David ◽  
Manfred Schuster ◽  
Christian Schroer ◽  
...  

2011 ◽  
Vol 110 (5) ◽  
pp. 053105 ◽  
Author(s):  
Michael Chabior ◽  
Tilman Donath ◽  
Christian David ◽  
Manfred Schuster ◽  
Christian Schroer ◽  
...  

2008 ◽  
Vol 7 (2) ◽  
pp. 134-137 ◽  
Author(s):  
F. Pfeiffer ◽  
M. Bech ◽  
O. Bunk ◽  
P. Kraft ◽  
E. F. Eikenberry ◽  
...  

2010 ◽  
Vol 20 (1) ◽  
pp. 7-16 ◽  
Author(s):  
Martin Bech ◽  
Torben H. Jensen ◽  
Oliver Bunk ◽  
Tilman Donath ◽  
Christian David ◽  
...  

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