Influence of an Elevated Temperature Environment on the Tensile Mechanical Properties of a 3D Printed Thermoplastic Polymer

Author(s):  
Jose E. Torres ◽  
Otito N. Onwuzurike ◽  
Amber J. W. McClung ◽  
Juan D. Ocampo

Abstract The purpose of this study is to examine the effects of the environment on 3D printed Polylactic Acid (PLA), a biodegradable thermoplastic polymer. The experimental program was specifically designed to explore the influence of print temperature and aging temperature on the mechanical performance of the printed material. Printing at the elevated temperatures (30–40°C) resulted in slight mechanical property changes. In order to understand which of the changes could also be caused by simply storing the materials at the elevated temperature, samples were printed at 25°C and subsequently aged (at 30–45°C) before mechanical testing. All mechanical testing was performed in standard laboratory temperature on an MTS Criterion. All of the mechanical properties were not greatly altered by printing or aging at elevated temperatures, suggesting that printing and using in extreme weather environments could be reasonable. The yield stress is not affected by storage at elevated temperatures, but is increased (or enhanced) by printing at elevated temperatures. The maximum stress is increased (or enhanced) by both aging and printing at elevated temperatures, but is accompanied by a large reduction in strain capacity. Changes that are observed in mechanical properties will be incorporated in future material models to accurately capture material behavior.

Materials ◽  
2020 ◽  
Vol 14 (1) ◽  
pp. 21
Author(s):  
Muhammad Nasir Amin ◽  
Kaffayatullah Khan

This study investigated the effect of elevated temperatures on the mechanical properties of high-strength sustainable concrete incorporating volcanic ash (VA). For comparison, control and reference concrete specimens with fly ash (FA) were also cast along with additional specimens of VA and FA containing electric arc furnace slag (EAFS). Before thermal exposure, initial tests were performed to evaluate the mechanical properties (compressive strength, tensile strength, and elastic modulus) of cylindrical concrete specimens with aging. Additionally, 91 day moist-cured concrete specimens, after measuring their initial weight and ultrasonic pulse velocity (UPV), were exposed up to 800 °C and cooled to air temperature. Subsequently, the weight loss, residual UPV, and mechanical properties of concrete were measured with respect to exposure temperature. For all concrete specimens, test results demonstrated a higher loss of weight, UPV, and other mechanical properties under exposure to higher elevated temperature. Moreover, all the results of concrete specimens incorporating VA were observed before and after exposure to elevated temperature as either comparable to or slightly better than those of control and reference concrete with FA. According to the experimental results, a correlation was developed between residual UPV and residual compressive strength (RCS), which can be used to assess the RCS of fire-damaged concrete (up to 800 °C) incorporating VA and EAFS.


Polymers ◽  
2021 ◽  
Vol 13 (9) ◽  
pp. 1473
Author(s):  
Jun Zhao ◽  
Kang Wang ◽  
Shuaibin Wang ◽  
Zike Wang ◽  
Zhaohui Yang ◽  
...  

This paper presents results from experimental work on mechanical properties of geopolymer concrete, mortar and paste prepared using fly ash and blended slag. Compressive strength, splitting tensile strength and flexural strength tests were conducted on large sets of geopolymer and ordinary concrete, mortar and paste after exposure to elevated temperatures. From Thermogravimetric analyzer (TGA), X-ray diffraction (XRD), Scanning electron microscope (SEM) test results, the geopolymer exhibits excellent resistance to elevated temperature. Compressive strengths of C30, C40 and C50 geopolymer concrete, mortar and paste show incremental improvement then followed by a gradual reduction, and finally reach a relatively consistent value with an increase in exposure temperature. The higher slag content in the geopolymer reduces residual strength and the lower exposure temperature corresponding to peak residual strength. Resistance to elevated temperature of C40 geopolymer concrete, mortar and paste is better than that of ordinary concrete, mortar and paste at the same grade. XRD, TGA and SEM analysis suggests that the heat resistance of C–S–H produced using slag is lower than that of sulphoaluminate gel (quartz and mullite, etc.) produced using fly ash. This facilitates degradation of C30, C40 and C50 geopolymer after exposure to elevated temperatures.


2001 ◽  
Vol 10 (2) ◽  
pp. 096369350101000
Author(s):  
E. Alonso ◽  
L. Martvnez-Gomez ◽  
W. Martvnez ◽  
L. Villaseρor ◽  
V.M. Castapo

Portland cement concretes were prepared by adding different igneous materials from west central Mexico. The results of the mechanical testing of these materials show the feasibility of employing igneous minerals to produce concretes and mortars, provided a careful control of granulometry and the geochemistry involved is attained. The mechanical performance, as well as the workability of the slurries can be managed by the convenient use of commercial additives (i.e. water reducers and aging accelerators). These results open the attractive possibility of expanding the natural sources of concrete-forming elements.


2014 ◽  
Vol 1004-1005 ◽  
pp. 148-153
Author(s):  
Min Hao ◽  
Ji Gang Ru ◽  
Ming Liu ◽  
Kun Zhang ◽  
Liang Wang ◽  
...  

Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) were utilized to study the microstructure and mechanical behavior of an Al-Cu-Mg alloy after tensile test at 125°C, 150°C, 175°C and 200 °C, respectively. The yield strength and ultimate tensile strength decreased with the increase of temperature, while the elongation increased firstly and then decreased. The S and S′ precipitate after tension at elevated temperatures. When the temperature was higher than 175°C, the precipitate coarsens rapidly. The alloys displayed a shear fracture features at elevated temperature. The larger S′ and S phase coarsened and dropped which forming crack in the grain boundaries and precipitate interfaces, resulting in the decrease of the elongation of the alloy.


2016 ◽  
Vol 877 ◽  
pp. 393-399
Author(s):  
Jia Zhou ◽  
Jun Ping Zhang ◽  
Ming Tu Ma

This paper presents the main achievements of a research project aimed at investigating the applicability of the hot stamping technology to non heat treatable aluminium alloys of the 5052 H32 and heat treatable aluminium alloys of the 6016 T4P after six months natural aging. The formability and mechanical properties of 5052 H32 and 6016 T4P aluminum alloy sheets after six months natural aging under different temperature conditions were studied, the processing characteristics and potential of the two aluminium alloy at room and elevated temperature were investigated. The results indicated that the 6016 aluminum alloy sheet exhibit better mechanical properties at room temperature. 5052 H32 aluminum alloy sheet shows better formability at elevated temperature, and it has higher potential to increase formability by raising the temperature.


Crystals ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1330
Author(s):  
Muhammad Farzik Ijaz ◽  
Mahmoud S. Soliman ◽  
Ahmed S. Alasmari ◽  
Adel T. Abbas ◽  
Faraz Hussain Hashmi

Unfolding the structure–property linkages between the mechanical performance and microstructural characteristics could be an attractive pathway to develop new single- and polycrystalline Al-based alloys to achieve ambitious high strength and fuel economy goals. A lot of polycrystalline as-cast Al-Cu-Mg-Ag alloy systems fabricated by conventional casting techniques have been reported to date. However, no one has reported a comparison of mechanical and microstructural properties that simultaneously incorporates the effects of both alloy chemistry and mechanical testing environments for the as-cast Al-Cu-Mg-Ag alloy systems. This preliminary prospective paper presents the examined experimental results of two alloys (denoted Alloy 1 and Alloy 2), with constant Cu content of ~3 wt.%, Cu/Mg ratios of 12.60 and 6.30, and a constant Ag of 0.65 wt.%, and correlates the synergistic comparison of mechanical properties at room and elevated temperatures. According to experimental results, the effect of the precipitation state and the mechanical properties showed strong dependence on the composition and testing environments for peak-aged, heat-treated specimens. In the room-temperature mechanical testing scenario, the higher Cu/Mg ratio alloy with Mg content of 0.23 wt.% (Alloy 1) possessed higher ultimate tensile strength when compared to the low Cu/Mg ratio with Mg content of 0.47 wt.% (Alloy 2). From phase constitution analysis, it is inferred that the increase in strength for Alloy 1 under room-temperature tensile testing is mainly ascribable to the small grain size and fine and uniform distribution of θ precipitates, which provided a barrier to slip by deaccelerating the dislocation movement in the room-temperature environment. Meanwhile, Alloy 2 showed significantly less degradation of mechanical strength under high-temperature tensile testing. Indeed, in most cases, low Cu/Mg ratios had a strong influence on the copious precipitation of thermally stable omega phase, which is known to be a major strengthening phase at elevated temperatures in the Al-Cu-Mg-Ag alloying system. Consequently, it is rationally suggested that in the high-temperature testing scenario, the improvement in mechanical and/or thermal stability in the case of the Alloy 2 specimen was mainly due to its compositional design.


2021 ◽  
Author(s):  
Karolina E. Mazur ◽  
Aleksandra Borucka ◽  
Paulina Kaczor ◽  
Szymon Gądek ◽  
Stanislaw Kuciel

Abstract In the study, polylactide-based (PLA) composites modified with natural particles (wood, bamboo, and cork) and with different levels of infilling (100%, 80%, and 60%) obtained by additive methods were tested. The effect of type fiber, infill level and crystallization rate on the mechanical properties were investigated by using tensile, flexural, and impact tests. The materials were subjected to mechanical tests carried out at 23 and 80 °C. Furthermore, hydrothermal degradation was performed, and its effect on the properties was analyzed. The addition of natural fillers and different level of infilling result in a similar level of reduction in the properties. Composites made of PLA are more sensitive to high temperature than to water. The decrease in Young's modulus of PLA at 80 °C was 90%, while after 28 days of hydrodegradation ~ 9%. The addition of fibers reduced this decrease at elevated temperatures. Moreover, the impact strength has been improved by 50% for composites with cork particles and for other lignocellulosic composites remained at the same level as for resin.


2019 ◽  
Vol 54 (13) ◽  
pp. 1705-1715
Author(s):  
MHR Jen ◽  
GT Kuo ◽  
YH Wu ◽  
YJ Chen

The mechanical properties and fatigue responses of Ti/APC-2 neat and nanocomposites with inclined single-edged cracks due to tensile and cyclic tests at elevated temperature were investigated. Two types of composite laminates [Ti/(0/90)s/Ti] were fabricated with and without (W/WO) nanoparticles SiO2 of optimal 1 wt.%. The geometry and dimensions of specimens were L × W × t = 240 × 25 × 1.55 mm3. The cracks were of constant length 3 mm and width 0.3 mm. The inclined angles were 0°, 45°, and 60°. Both the tensile and cyclic tests were conducted at elevated temperatures 25℃ (RT), 100℃, 125℃, and 150℃. From the tensile tests we obtained the load vs. displacement curves for both types of laminates with varied inclinations at elevated temperatures. Next, we received the applied load vs. cycles curves for the same laminates with inclined cracks at the corresponding temperature due to cyclic tests. According to the experimental data of both tensile and cyclic tests the mechanical properties, such as strength, stiffness, and life, decreased as the temperature rises. The greater the inclined angles were, the greater the strength and stiffness were. Similarly, the fatigue life was in the same trend. However, the effect of inclined angle on mechanical properties was more strong than those of temperature. The mechanical properties of nanocomposite laminates were higher than those of neat composite laminates, but not significant. The main reason was that the enhancement of spreading nano-powder silica on the laminate interfaces did not effectively eliminate the stress intensity at the crack tip locally.


2020 ◽  
Vol 2020 ◽  
pp. 1-18
Author(s):  
Zhen Nie ◽  
Yuanqi Li ◽  
Yehua Wang

It is highly important to clarify the high-temperature mechanical properties in the design of cold-formed steel (CFS) structures under fire conditions due to the unique deterioration feature in material properties under fire environment and associated reduction to the mechanical performance of members. This paper presents the mechanical properties of widely used steels for cold-formed steel structures at elevated temperatures. The coupons were extracted from original coils of proposed full annealed steels (S350 and S420, with nominal yielding strengths 280 MPa and 350 MPa) and proposed stress relieving annealed steels (G500, with nominal yielding strength 500 MPa) for CFS structures with thickness of 1.0 mm and 1.2 mm, and a total of nearly 50 tensile tests were carried out by steady-state test method for temperatures ranging from 20 to 700°C. Based on the tests, material properties including the yield strengths, ultimate strengths, the elasticity modulus, and the stress-strain curve were obtained. Meanwhile, the ductility of steels for CFS structures was discussed. Then, the temperature-dependent retention factors of yield strengths and elasticity modulus were compared to those provided by design codes and former researchers. Finally, a set of prediction equations of the mechanical properties for steels for CFS structures at elevated temperatures was proposed depending on existing tests data.


Materials ◽  
2020 ◽  
Vol 13 (22) ◽  
pp. 5264
Author(s):  
Bharat Yelamanchi ◽  
Eric MacDonald ◽  
Nancy G. Gonzalez-Canche ◽  
Jose G. Carrillo ◽  
Pedro Cortes

The production and mechanical properties of fiber metal laminates (FMLs) based on 3D printed composites have been investigated in this study. FMLs are structures constituting an alternating arrangement of metal and composite materials that are used in the aerospace sector due to their unique mechanical performance. 3D printing technology in FMLs could allow the production of structures with customized configuration and performance. A series of continuous carbon fiber reinforced composites were printed on a Markforged system and placed between layers of aluminum alloy to manufacture a novel breed of FMLs in this study. These laminates were subjected to tensile, low velocity and high velocity impact tests. The results show that the tensile strength of the FMLs falls between the strength of their constituent materials, while the low and high velocity impact performance of the FMLs is superior to those observed for the plain aluminum and the composite material. This mechanism is related to the energy absorption process displayed by the plastic deformation, and interfacial delamination within the laminates. The present work expects to provide an initial research platform for considering 3D printing in the manufacturing process of hybrid laminates.


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