scholarly journals Recent Trends in the Microwave-Assisted Synthesis of Metal Oxide Nanoparticles Supported on Carbon Nanotubes and Their Applications

2012 ◽  
Vol 2012 ◽  
pp. 1-15 ◽  
Author(s):  
Sarah C. Motshekga ◽  
Sreejarani K. Pillai ◽  
Suprakas Sinha Ray ◽  
Kalala Jalama ◽  
Rui. W. M. Krause

The study of coating carbon nanotubes with metal/oxides nanoparticles is now becoming a promising and challenging area of research. To optimize the use of carbon nanotubes in various applications, it is necessary to attach functional groups or other nanostructures to their surface. The combination of the distinctive properties of carbon nanotubes and metal/oxides is expected to be applied in field emission displays, nanoelectronic devices, novel catalysts, and polymer or ceramic reinforcement. The synthesis of these composites is still largely based on conventional techniques, such as wet impregnation followed by chemical reduction of the metal nanoparticle precursors. These techniques based on thermal heating can be time consuming and often lack control of particle size and morphology. Hence, there is interest in microwave technology recently, where using microwaves represents an alternative way of power input into chemical reactions through dielectric heating. This paper covers the synthesis and applications of carbon-nanotube-coated metal/oxides nanoparticles prepared by a microwave-assisted method. The reviewed studies show that the microwave-assisted synthesis of the composites allows processes to be completed within a shorter reaction time with uniform and well-dispersed nanoparticle formation.

2017 ◽  
Vol 63 (6) ◽  
pp. 341-374 ◽  
Author(s):  
Markus B. Schütz ◽  
Lisong Xiao ◽  
Thomas Lehnen ◽  
Thomas Fischer ◽  
Sanjay Mathur

RSC Advances ◽  
2016 ◽  
Vol 6 (116) ◽  
pp. 115317-115325 ◽  
Author(s):  
Yaru Yan ◽  
Qitong Huang ◽  
Chan Wei ◽  
Shirong Hu ◽  
Hanqiang Zhang ◽  
...  

Cyclic voltammetry of HQ and CC recorded on Nafion/CDs–ZnO/MWCNTs/GCE.


2016 ◽  
Vol 40 (9) ◽  
pp. 7986-7995 ◽  
Author(s):  
Zohre Zarnegar ◽  
Javad Safari

The microwave-assisted synthesis of the first ionic liquid stabilized CNTs–Fe3O4as a novel nanocatalyst for the synthesis of 2-amino-chromenesviaa multicomponent reaction is reported.


RSC Advances ◽  
2014 ◽  
Vol 4 (27) ◽  
pp. 14149-14156 ◽  
Author(s):  
Michael T. Kessler ◽  
Maria K. Hentschel ◽  
Christina Heinrichs ◽  
Stefan Roitsch ◽  
Martin H. G. Prechtl

Herein we present a general approach to metal and metal oxide nanoparticles using simple metal salts as starting materials.


2017 ◽  
Vol 730 ◽  
pp. 167-171 ◽  
Author(s):  
Ekarat Detsri ◽  
Kanrayasiri Kamhom ◽  
Chatsuda Detsri

Unmodified gold nanoparticles (AuNPs) have been successfully synthesized by the chemical reduction of tetrachloride gold (III) ions ([AuCl4]-) in the presence of sodium citrate based on the rapid microwave−assisted approach. The diameter of the synthesized nanoparticles was found in the range of 16.50±2.75 nm. The AuNPs were characterized using UV−vis spectrophotometer, zeta potential analyzer and transmission electron microscope (TEM). The sodium citrate protected AuNPs were found to be selective and sensitive for the detection of dopamine. It was based on the aggregation change of the nanoparticles from random coil to hairpin structure upon the addition of dopamine concentration. The red shift of the plasmonic peak wavelength of AuNPs could be used for the detection of dopamine. The response to dopamine allows for a linear range from 10 to 125 mg⋅L-1 (R2 = 0.9804) with a limit of detection (LOD) at a signal to noise ratio of 3 of 12.85±1.38 mg⋅L-1. The colorimetric sensor was evaluated with 98.0−99.9% recovery of added dopamine in urine sample. The proposed sensor was successfully applied to the determination of dopamine in biological samples.


MRS Advances ◽  
2018 ◽  
Vol 3 (1-2) ◽  
pp. 121-126
Author(s):  
Patsy Y. Arquieta Guillén ◽  
Alena Borisovna Kharissova ◽  
Beatriz Ortega García ◽  
Oxana V. Kharissova

ABSTRACTNowadays, carbon nanotubes have a lot of applications in daily life, being applied in the fabrication of cellphones, computers, nanotransistors, among many others. Currently, their new applications in biotechnology area are in research, in particular in order to find new biosensors with fluorescent properties applying on the basis of multi-wall carbon nanotubes (MWCNTs). In this work, the obtaining of carbon nanoparticles having fluorescent properties via spray pyrolysis is presented. Synthesis, properties, structural peculiarities, and applications of nanobuds and related nanostructures are discussed. MWCNTs, decorated with strontium aluminate SrAl12O19 and doped with rare-earth elements, were synthetized from distinct organic precursors and the corresponding metal oxides. The metal oxides used were Samarium (Sm), Europium (Eu), Neodymium (Nd), Lanthanum (La), Cerium (Ce) and some their combinations.The synthesis was carried out on the surface of optical fibres to obtain a uniform growth of forest-like MWCNTs, adding to metal oxide nanoparticles to their surface. The preparation of composites was carried out by spray pyrolysis techniques in dry nitrogen atmosphere in the temperature range from 780 to 850°C. The formed products were characterized by Scanning Electron Microscopy (SEM), Transmission Electron Microscopy (TEM), FTIR spectroscopy, Raman spectroscopy and UV/visible spectroscopies. The analysis of the obtained data shows that the deposited nanoparticles are in the range of size 20-60 nm being uniformly distributed on the surface of MWCNTs. The samples, obtained at different temperatures and with doping metal oxides added to SrAl12O19, show different fluorescence behavior. The best results were observed with lanthanum oxide as a dopant. Possible applications as persistently luminescent phosphors for the formed MWCNTs-supported luminescent materials are proposed.


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