Mechanical properties analysis of polyetherimide parts fabricated by fused deposition modeling

2018 ◽  
Vol 31 (1) ◽  
pp. 97-106 ◽  
Author(s):  
Shenglong Jiang ◽  
Guangxin Liao ◽  
Dingding Xu ◽  
Fenghua Liu ◽  
Wen Li ◽  
...  

Polyetherimide (PEI) is a kind of high-performance polymer, which possesses a high glass transition temperature ( Tg), excellent flame retardancy, low smoke generation, and good mechanical properties. In this article, PEI was applied in the fused deposition modeling (FDM)–based 3-D printing for the first time. The entire process from filament extrusion to printing was studied. It was observed that the filament orientation and nozzle temperature were closely related to the mechanical properties of printed samples. When the nozzle temperature is 370°C, the mean tensile strength of FDM printing parts can reach to 104 MPa, which is only 7% lower than that of injection molded parts. It can be seen that the 0° orientation set of samples show the highest storage modulus (2492 MPa) followed by the 45° samples, and the 90° orientation set of samples show the minimum storage modulus (1420 MPa) at room temperature. The above results indicated that this technique allows the production of parts with adequate mechanical performance, which does not need to be restricted to the production of mock-ups and prototypes. Our work broke the limitations of traditional FDM technology and expanded the types of material available for FDM to the high-temperature engineering plastics.

2019 ◽  
Vol 25 (7) ◽  
pp. 1145-1154 ◽  
Author(s):  
Xia Gao ◽  
Daijun Zhang ◽  
Xiangning Wen ◽  
Shunxin Qi ◽  
Yunlan Su ◽  
...  

Purpose This work aims to develop a new kind of semicrystalline polymer filament and optimize its printing parameters in the fused deposition modeling process. The purpose of this work also includes producing FDM parts with good ductility. Design/methodology/approach A new kind of semicrystalline filaments composed of long-chain polyamide (PA)1012 was prepared by controlling screw speed and pulling speed carefully. The optimal printing parameters for PA1012 filaments were explored through investigating dimensional accuracy and bonding strength of FDM parts. Furthermore, the mechanical properties of PA1012 specimens were also evaluated by varying nozzle temperatures and raster angles. Findings It is found that PA1012 filaments can accommodate for FDM process under suitable printing parameters. The print quality and mechanical properties of FDM parts highly depend on nozzle temperature and bed temperature. Even though higher temperatures facilitate stronger interlayer bonding, FDM parts with excellent tensile strength were obtained at a moderate nozzle temperature. Moreover, a bed temperature well above the glass transition temperature of PA1012 can eliminate shrinkage and distortion of FDM parts. As expected, FDM parts prepared with PA1012 filaments exhibit good ductility. Originality/value Results in this work demonstrate that the PA1012 filament allows the production of FDM parts with desired mechanical performance. This indicates the potential for overcoming the dependence on amorphous thermoplastics as a feedstock in the FDM technique. This work also provides insight into the effect of materials properties on the mechanical performance of FDM-printed parts.


2021 ◽  
pp. 089270572110530
Author(s):  
Nagarjuna Maguluri ◽  
Gamini Suresh ◽  
K Venkata Rao

Fused deposition modeling (FDM) is a fast-expanding additive manufacturing technique for fabricating various polymer components in engineering and medical applications. The mechanical properties of components printed with the FDM method are influenced by several process parameters. In the current work, the influence of nozzle temperature, infill density, and printing speed on the tensile properties of specimens printed using polylactic acid (PLA) filament was investigated. With an objective to achieve better tensile properties including elastic modulus, tensile strength, and fracture strain; Taguchi L8 array has been used for framing experimental runs, and eight experiments were conducted. The results demonstrate that the nozzle temperature significantly influences the tensile properties of the FDM printed PLA products followed by infill density. The optimum processing parameters were determined for the FDM printed PLA material at a nozzle temperature of 220°C, infill density of 100%, and printing speed of 20 mm/s.


2017 ◽  
Vol 23 (5) ◽  
pp. 869-880 ◽  
Author(s):  
Ying-Guo Zhou ◽  
Bei Su ◽  
Lih-sheng Turng

Purpose Although the feasibility and effectiveness of the fused deposition modeling (FDM) method have been proposed and developed, studies of applying this technology to various materials are still needed for researching its applicability, especially with regard to polymer blends and composites. The purpose of this paper is to study the deposition-induced effect and the effect of compatibilizers on the mechanical properties of polypropylene and polycarbonate (PP/PC) composites. Design/methodology/approach For this purpose, three different deposition modes for PP/PC composites with or without compatibilizers were used for the FDM method and tested for tensile properties. Also, parts with the same materials were made by injection molding and used for comparison. In addition, different deposition speeds were used to investigate the different deposition-induced effects. Furthermore, the behavior of the mechanical properties was clarified with scanning electron microscope images of the fracture surfaces. Findings The research results suggest that the deposition orientation has a significant influence on the mechanical behavior of PP/PC composite FDM parts. The results also indicate that there is a close relationship between the mechanical properties and morphological structures which are deeply influenced by compatibilization. Compared with injection molded parts, the ductility of the FDM parts can be dramatically improved due to the formation of fibrils and micro-fibrils by the deposition induced during processing. Originality/value This is the first paper to investigate a PP/PC composite FDM process. The results of this paper verified the applicability of PP/PC composites to FDM technology. It is also the first time that the deposition-induced effect during FDM has been investigated and studied.


2020 ◽  
Vol 44 (1) ◽  
pp. 15-20
Author(s):  
Katarzyna Bulanda ◽  
Mariusz Oleksy ◽  
Rafał Oliwa ◽  
Grzegorz Budzik ◽  
Tadeusz Markowski

AbstractNew materials and filaments dedicated to 3D printing were obtained using the fused deposition modeling method, and the properties of the produced materials were investigated. Polylactide was used as a polymer base for the assays because of the desired properties of the polymer, mainly biodegradability, and the matrix was refilled by the addition of metallic nanofillers, such as bronze, copper, brass, and steel. For the composites obtained, mechanical properties were investigated to determine the dependence of the obtained results on the content and type of filler used and on the method of fabrication of the fittings. It was found that the additives present in the polymer matrix increased the fluidity of the material. The best results were obtained for the compositions with bronze and steel in which the mass flow rate was 72.97 and 79.99 g/10 min, respectively. The filled material that had lower hardness was measured by Rockwell and the impact strength was measured by Charpy. In addition, it was found that injection-molded parts obtained much better mechanical properties than those obtained by 3D printing.


Polymers ◽  
2021 ◽  
Vol 14 (1) ◽  
pp. 77
Author(s):  
Sasa Gao ◽  
Ruijuan Liu ◽  
Hua Xin ◽  
Haitao Liang ◽  
Yunfei Wang ◽  
...  

Additive manufacturing provides a novel and robust way to prepare medical product with anatomic matched geometry and tailored mechanical performance. In this study, the surface characteristics, microstructure, and mechanical properties of fused deposition modeling (FDM) prepared polyether-ether-ketone (PEEK) were systematically studied. During the FDM process, the crystal unit cell and thermal attribute of PEEK material remained unchanged, whereas the surface layer generally became more hydrophilic with an obvious reduction in surface hardness. Raster angle has a significant effect on the mechanical strength but not on the failure mechanism. In practice, FDM fabricated PEEK acted more like a laminate rather than a unified structure. Its main failure mechanism was correlated to the internal voids. The results show that horizontal infill orientation with 30° raster angle is promising for a better comprehensive mechanical performance, and the corresponding tensile, flexural, and shear strengths are (76.5 ± 1.4) MPa, (149.7 ± 3.0) MPa, and (55.5 ± 1.8) MPa, respectively. The findings of this study provide guidelines for FDM-PEEK to enable its realization in applications such as orthopedic implants.


Author(s):  
Saty Dev ◽  
Rajeev Srivastava

Fused deposition modeling (FDM) technology is catching the fast global market in the real-time production of polymeric parts. Process variables highly influence the performance characteristics of FDM-generated parts, so mechanical performance is not perfect for all applications. In actual conditions, parts produced by FDM are constantly subjected to loading at different temperatures. The former studies mainly concentrated on the properties of FDM products to static loading environments. There is a scope of effective investigation on the influence of FDM processing conditions on dynamic mechanical properties using artificial intelligence (AI) based techniques. The present study focused on investigation and optimization the manufacturing process parameters to evaluate the dynamic mechanical performance of FDM-produced part. The experimental runs were obtained through central composite design in Minitab software. A DMA8000 instrument was used to test the specimens for dynamic mechanical performance. The mathematical models were developed and optimized through different approaches like response surface methodology-genetic algorithm (RSM-GA) and artificial neural network-genetic algorithm (ANN-GA). The techniques for order preference by similarity to an ideal solution (TOPSIS) is employed to obtain the best parameter settings from sets of optimized solutions. The sequential use of ANN-GA and TOPSIS methods predicted the highest values of storage modulus 1619.61 MPa and loss modulus 257.38 MPa corresponding to 68.94° raster angle, 81.48% infill density, 0.10 mm layer thickness, 237.73°C nozzle temperature and 38.97 mm/s print head speed. The confirmation tests were conducted to validate the predicted result that upscale the desired properties. The RSM-GA-TOPSIS occurred with a prediction error of 2.40% and −3.31%, corresponding to storage and loss modulus. Similarly, ANN-GA-TOPSIS shows 2.17% and 2.89% prediction error corresponding to storage and loss modulus. The experimental and analytical outcome of present study will be helpful for the designers of intricate functional parts which come under thermo-mechanical loading conditions.


2016 ◽  
Vol 22 (6) ◽  
pp. 887-894 ◽  
Author(s):  
Eunseob Kim ◽  
Yong-Jun Shin ◽  
Sung-Hoon Ahn

Purpose This paper aims to investigate the water absorption behaviors and mechanical properties, according to water absorption and temperature, of components fabricated by fused deposition modeling (FDM) and injection molding. The mechanical properties of FDM and injection molded parts were studied under several environmental conditions. Design/methodology/approach FDM components can be used as load-carrying elements under a range of moisture and temperature conditions. FDM parts show anisotropic mechanical properties according to build orientation. Components were fabricated from acrylonitrile-butadiene-styrene in three different orientations. The mechanical properties of parts fabricated by FDM were compared to injection molded components made from the same material. Water absorption tests were conducted in distilled water between 20 and 60°C to identify the maximum water absorption rate. Both moisture and temperature were considered as environmental variables in the tensile tests, which were conducted under various conditions to measure the effects on mechanical properties. Findings The water absorption behavior of FDM components obeyed Fickian diffusion theory, irrespective of the temperature. High temperatures accelerated the diffusion rate, although the maximum water absorption rate was not affected. The tensile strength of FDM parts under dry, room temperature conditions, was approximately 26-56 per cent that of injection molded parts, depending on build orientation. Increased temperature and water absorption had a more significant effect on FDM parts than injection molded components. The tensile strength was decreased by 67-71 per cent in hot, wet environments compared with dry, room temperature conditions. Originality/value The water absorption behavior of FDM components was investigated. The quantitative effects of temperature and moisture on tensile strength, modulus and strain were also measured. These results will contribute to the design of FDM parts for use under various environmental conditions.


Author(s):  
Steffany N. Cerda-Avila ◽  
Hugo I. Medellín-Castillo ◽  
Dirk F. de Lange

The prediction of the structural performance of additive manufacturing (AM) parts has become one of the main challenges to boost the use of AM in industry. The structural properties of AM are very important in order to design and fabricate parts not only of any geometrical shape but also with variable or customized mechanical properties. While AM experimental studies are common in the literature, a limited number of investigations have focused on the analysis and prediction of the mechanical properties of AM parts using theoretical and numerical approaches, such as the finite element method (FEM); however, their results have been not accurate yet. Thus, more research work is needed in order to develop reliable prediction models able to estimate the mechanical performance of AM parts before fabrication. In this paper, the analysis and numerical simulation of the structural performance of fused deposition modeling (FDM) samples with variable infill values is presented. The aim is to predict the mechanical performance of FDM components using numerical models. Thus, several standard tensile test specimens were fabricated in an FDM system using different infill values, a constant layer thickness, one shell perimeter, and polylactic acid (PLA) material. These samples were measured and modeled in a computer-aided design (CAD) system before performing the experimental tensile tests. Numerical models and simulations based on the FEM method were then developed and carried out in order to predict the structural performance of the specimens. Finally, the experimental and numerical results were compared and conclusions drawn.


2021 ◽  
Vol 13 (2) ◽  
pp. 34-38
Author(s):  
Sabit Hasçelik ◽  
◽  
Ömer T. Öztürk ◽  
Sezer Özerinç ◽  
◽  
...  

Fused deposition modeling (FDM) is a widely used additive manufacturing technique for producing polymeric parts. While most commonly used FDM filaments are PLA and ABS, nylon is a widely used thermoplastic polymer in industry. This study investigated the mechanical properties of FDM-produced specimens made of nylon and quantified the effect of process parameters such as raster orientation and nozzle temperature on the mechanical properties. As the nozzle temperature increases, specimens become stronger with higher elongations at the break. This is mainly due to the improved fusion between the layers, provided by an expansion of the heat-affected zone. On the other hand, specimens with diagonal raster orientation exhibit higher elongations than those with perpendicular and parallel raster. The findings also emphasize the synergistic effects between nozzle temperature and printing orientation, showing that optimization should consider the two parameters together. Overall, FDM can produce strong nylon parts with adequate ductility suitable for load-bearing applications. However, achieving such results requires a detailed optimization of process parameters.


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