Effect of electroplastic treatment on microstructure and texture changes of a cold rolling AZ31 strip

2009 ◽  
Vol 1170 ◽  
Author(s):  
Lei Guan ◽  
Guoyi Tang
Keyword(s):  
Cold Rolling ◽  
Light Microscopy ◽  
Static Recrystallization ◽  
Texture Evolution ◽  
Dislocation Climb ◽  
Basal Texture ◽  
X Ray Diffraction ◽  
X Ray ◽  
Electropulsing Treatment

AbstractThe effect of the electropulsing on recrystallized microstructure and on texture evolution of a cold rolling (CR) AZ31 strip was studied with the help of light microscopy and X-ray diffraction technique. It was exciting that the completed recrystallization state of sample subjected to the electropulsing treatment (EPT) could be obtained rapidly in ˜7s with the basal texture weakened. The favoring mechanism of static recrystallization (SRX) of MPT could be attributed to the coupled action of the thermal and athermal effects, thereinto, the latter one activated dislocation climb effectively.

TEXTURE EVOLUTION OF BT20 ALLOY IN BACKWARD TUBE SPINNING

2009 ◽  
Vol 23 (06n07) ◽  
pp. 914-919 ◽  
Author(s):  
GUOPING YANG ◽  
WENCHEN XU ◽  
DEBIN SHAN
Keyword(s):  
Outer Surface ◽  
Texture Evolution ◽  
Basal Texture ◽  
X Ray Diffraction ◽  
Tube Spinning ◽  
X Ray ◽  
Inner Surface ◽  
Medium Level ◽  
Spinning Process ◽  
History Of

Backward tube spinning experiment of BT20 ( Ti -6 Al -2 Zr -1 Mo -1 V ) alloy was carried out with an aim to examine texture evolution of titanium alloy in spinning process. The initial texture and the spinning texture were investigated by X-ray diffraction, and deformation history of a single-pass spinning was analyzed using finite element method. Tilt basal texture occurs when thickness reduction reaches a medium level (~ 49% for the outer surface and ~ 58% for the inner surface in the present study) and that further deformation promotes the formation of central basal texture. During early several passes basal texture in the outer surface develops more rapidly and intensely than that in the inner surface due to much larger deformation. However, the maximum intensity of texture in the inner surface reaches a higher level in subsequent passes for the following two reasons: (1) the discrepancy between equivalent deformation in the internal layer and that in the external layer reduces with increasing deformation; (2) material in the inner surface undergoes much smaller transverse shear deformation. Spinning texture is characterized by its asymmetry, which results from asymmetric spinning deformation investigated by analyzing deformation histories of material particles located in the inner and outer surface.

Effect of As-Rolled Microstructure on Static Recrystallization Characteristics and Texture Evolution during Annealing

2016 ◽  
Vol 879 ◽  
pp. 1876-1881
Author(s):  
Jing Su ◽  
Abu S.H. Kabir ◽  
Steve Yue
Keyword(s):  
Optical Microscopy ◽  
Static Recrystallization ◽  
Texture Evolution ◽  
Az31 Alloy ◽  
Rolling Speed ◽  
X Ray Diffraction ◽  
Electron Backscattered Diffraction ◽  
X Ray ◽  
Magnesium Az31

Magnesium AZ31 alloy sheets were rolled at 100 °C at a high rolling speed of 1000 m/min. After 30% reduction, the microstructure was heavily twinned and shear banded, while a partially dynamically recrystallized and twinned microstructure was seen at the reduction of 49%. The as-rolled specimens were then annealed at 500 °C for increasing times. Microstructure and texture were characterized by optical microscopy, electron backscattered diffraction (EBSD) and X-ray diffraction (XRD). Texture weakening was found during annealing of the specimens at both reductions. However, the texture weakening was more effective in the fully twinned and shear banded specimen than the partially DRXed and twinned specimen. Effects of as-rolled microstructure on static recrystallization characteristics and texture evolution during annealing were studied.

Microstructure and Mechanical Responses of Extruded Magnesium Alloy Sheets with Lithium Addition

2015 ◽  
Vol 816 ◽  
pp. 504-509 ◽  
Author(s):  
Qing Shan Yang ◽  
Bin Jiang ◽  
Jun Jie He ◽  
Zheng Yuan Gao ◽  
Jia Hong Dai ◽  
...  
Keyword(s):  
Magnesium Alloy ◽  
Room Temperature ◽  
Texture Evolution ◽  
Tensile Tests ◽  
Extrusion Ratio ◽  
Basal Texture ◽  
X Ray Diffraction ◽  
X Ray ◽  
Mechanical Responses ◽  
Room Temperature Ductility

After 5% lithium was added to AZ31 magnesium alloy, the alloy was extruded at 380oC with the extrusion ratio of 101. Mechanical responses and microstructure evolution were investigated. The microstructure and texture evolution were examined by electronic backscattered diffraction (EBSD) and X-ray diffraction (XRD). Tensile tests in the tensile directions of 0o, 45oand 90owere carried out at room temperature. Lithium addition brought about the strong divergence of the grain orientation and triggered the spread of the (0002) basal texture. The room temperature ductility of the extruded Mg alloy sheets was improved due to the tilted weak basal texture.

Texture Evolution during Recrystallisation of Cold Rolled TWIP Steel

2011 ◽  
Vol 702-703 ◽  
pp. 647-650
Author(s):  
Ahmed A. Saleh ◽  
Elena V. Pereloma ◽  
Azdiar A. Gazder
Keyword(s):  
Cold Rolling ◽  
Twip Steel ◽  
Texture Evolution ◽  
Rolling Texture ◽  
Austenitic Steels ◽  
X Ray Diffraction ◽  
Energy Materials ◽  
X Ray ◽  
Nucleation Sites ◽  
Cold Rolled

A TWinning Induced Plasticity (TWIP) steel was cold rolled to 42% thickness reduction followed by isochronal annealing for 300 s between 600-850 °C. Bulk texture evolution during recrystallisation was investigated by X-Ray Diffraction. While the development of the α-fibre after cold rolling is typical of low stacking fault energy materials, anomalously higher intensities were noted for the Goss ({110}) compared to Brass ({110}) orientations. Upon recrystallisation, the main rolling texture components were retained and ascribed to nucleation at orientations close to those of the deformed matrix followed by annealing twinning which leads to crystallographically identical variants. Unlike previous texture investigations on austenitic steels, the relatively homogeneous deformation microstructure and uniform distribution of subsequent nucleation sites led to the retention of the F ({111}) orientation. Moreover, the firsthand observation of the Rotated Copper ({112}) orientation in TWIP steel is attributed to the second order twinning of the A ({110}) orientation.

scholarly journals Microstructure And Texture Evolution During Cold-Rolling In The Fe-23Mn-3Si-3Al Alloy

2015 ◽  
Vol 60 (3) ◽  
pp. 1789-1794 ◽  
Author(s):  
J. Kowalska ◽  
W. Ratuszek ◽  
M. Witkowska ◽  
A. Zielińska-Lipiec ◽  
M. Kowalski
Keyword(s):  
Cold Rolling ◽  
Texture Evolution ◽  
Martensitic Transformations ◽  
Mechanical Twinning ◽  
Al Alloy ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Cold Rolled ◽  
Hot Rolled

Abstract Fe–23wt.%Mn–3wt.%Si–3wt.%Al alloy was cast, homogenized at 1150ºC, hot-rolled at temperatures between 1200ºC and 900ºC and next cold-rolled from 5% up to 40% reductions in thickness. Microstructure and texture of this alloy, which has a low stacking fault energy, were defined after cold-rolling. Investigation of transmission electron microscopy and X-ray diffraction showed that mechanical twinning and martensitic transformations (γfcc→εhcp and γfcc→εhcp→α′bcc) took place during cold-rolling. The crystallographic Shoji-Nishiyama (S-N) {00.2}ε║{111}γ, <11.0>ε ║ <110>γ and Kurdjumov-Sachs (K-S) {111}γ║{101}α’, <101>γ║<111>α’ relations between martensite (ε, α’) and austenite (γ), were found in the coldrolled material.

Microstructure and Texture Evolution in Cladded Al 3003 Aluminum Sheets

2017 ◽  
Vol 885 ◽  
pp. 159-164
Author(s):  
Adrienn Hlavacs ◽  
Márton Benke ◽  
Péter Barkóczy ◽  
Valéria Mertinger
Keyword(s):  
Cold Rolling ◽  
Texture Evolution ◽  
Base Material ◽  
Thickness Reduction ◽  
X Ray Diffraction ◽  
X Ray ◽  
Volume Fractions ◽  
Aluminum Sheets ◽  
Reduction Function ◽  
Aluminium Sheets

In the present research, the texture variation during cold rolling of cladded 3003 type aluminium sheets was examined by means of X-ray diffraction. The aluminum sheets were formed in a series of 14 rolling steps, after which texture examinations were performed on both cladded and base material sides of the sheets. After certain rolling steps, the texture was also examined by removing layers from the sheets by electropolishing to reveal the texture distribution along depth. The texture was characterised through the calculation of volume fractions of the main rolled texture components. Local drawbacks were found in the texture versus thickness reduction function. The texture was found to be higher in the middle of the sheets than at the surface.

Texture Evolution Under Fast Heating and Cooling Rates of Zirconium Alloys Studied In-Situ by Synchrotron X-Ray Diffraction

2020 ◽  
Author(s):  
Chi-Toan Nguyen ◽  
Alistair Garner ◽  
Javier Romero ◽  
Antoine Ambard ◽  
Michael Preuss ◽  
...  
Keyword(s):  
Texture Evolution ◽  
Zirconium Alloys ◽  
X Ray Diffraction ◽  
Fast Heating ◽  
Cooling Rates ◽  
X Ray ◽  
Heating And Cooling

scholarly journals Study of the High Temperature Phase of 1,16-Hexadecanediol by Polarized Light Microscopy and Glancing Incidence X-Ray Diffraction

2018 ◽  
Vol 24 (S1) ◽  
pp. 2248-2249
Author(s):  
M. Ramírez-Cardona ◽  
M.P. Falcón-León ◽  
G. Luis-Raya ◽  
G. Mejía-Hernández ◽  
R. Arceo ◽  
...  
Keyword(s):  
High Temperature ◽  
Light Microscopy ◽  
Polarized Light ◽  
High Temperature Phase ◽  
Polarized Light Microscopy ◽  
Temperature Phase ◽  
X Ray Diffraction ◽  
X Ray

A Study of Recrystallization Texture Formation in Cold Rolled Iron Sheets with X-Ray Diffraction Techniques

1970 ◽  
Vol 14 ◽  
pp. 214-230 ◽  
Author(s):  
M. Matsuo ◽  
S. Hayami ◽  
S. Nagashima
Keyword(s):  
Cold Rolling ◽  
Recrystallization Texture ◽  
High Energy ◽  
Orientation Dependence ◽  
Primary Recrystallization ◽  
Texture Formation ◽  
X Ray Diffraction ◽  
X Ray ◽  
Stable Orientation ◽  
Rotational Orientation

AbstractThe possibility that primary recrystallization textures are influenced by local inhomogeneities of deformation induced in the regions of grain boundaries has been confirmed by comparing the cold rolling and the annealing textures of polycrystalline pure irons which were different in the grain size prior to cold rolling. Analyses were made for the effects of deformation on crystals, namely storage of lattice strain and orientation spread, with application of X-ray diffraction techniques, in order to elucidate the role of in homogeneities of deformation on recrystallization texture formation. Apparent correspondence was found between the orientation dependence of stored strain energy and the textural change on recrystallization. This is a scribed to oriented nucleation in high energy blocks, in the case of originally large-grain material in which the effects of inhomogeneities of deformation are small. But discrepancies arise on this basis in originally small - grain material in which the effects of inhomogeneities of deformation are thought to be considerable. The discrepancy is inferred to arise as an effect of local inhomogeneities of deformation, from the change in the trend of rotational orientation spreads from, a stable orientation and the extent of development of potential nuclei of recrystallization at high energy blocks in the orientation spreads. The change is considered to give rise to the variation in amount of microstrain distribution, which is expressed in recovery characteristics of lattice strains and in the dependence of microstrains on the column length as analyzed by following the procedure of Warren-Averbach.

Detection of Intermetallic Compounds in a Mg-5Al-3Ca-0.7Sr-0.2Mn Magnesium Alloy

2013 ◽  
Vol 197 ◽  
pp. 137-142 ◽  
Author(s):  
Tomasz Rzychoń ◽  
Janusz Szala ◽  
Tomasz Kukiełka
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Magnesium Alloy ◽  
Light Microscopy ◽  
Diffraction Analysis ◽  
Intermetallic Compounds ◽  
Intermetallic Phases ◽  
X Ray Diffraction ◽  
X Ray ◽  
Scanning Electron

In this paper the results of microstructural investigations and methodology of detection of intermetallic compounds were reported. The microstructural investigations included the light microscopy, scanning electron microscopy, chemical microanalysis and X-ray diffraction analysis. It was found that the microstructure of Mg-5Al-3Ca-0.7Sr-0.2Mn alloy consists of α-Mg, (Mg,Al)2Ca, Al3Mg13(Sr,Ca), Mg2Ca and Al2Ca intermetallic phases. The correct detection of these phases requires the high magnifications and a large number of measurements fields.

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