Rheological Characterization of Suspension of Hollow Glass Beads

SPE Journal ◽  
2017 ◽  
Vol 22 (05) ◽  
pp. 1671-1680 ◽  
Author(s):  
Simone Lumsden ◽  
John P. Singh ◽  
Ronnie G. Morgan ◽  
Gregory Hundt

Summary Hollow glass spheres (beads) are widely used as density and rheological modifiers for various oil and gas process fluids, particularly cement. One of the primary uses is to achieve lightweight slurries with good mechanical properties of the set cement. This paper discusses a concentrated, yet pumpable, suspension of these spheres for offshore cementing applications. Providing the lightweight spheres in a liquid suspension eliminates the risks associated with dry blending these materials. The development of the liquid suspension of hollow beads enables on-the-fly mixing of cement slurries with desired density profiles. Currently, the beads are premixed in the cement powder before they are shipped to offshore locations, which could result in the segregation of the beads during delivery and storage, and limits operations to the predetermined density (concentration of beads) of the slurry. This paper presents the rheological behavior of the concentrated suspension (up to 60% vol/vol) of hollow glass spheres suspended in a dilute aqueous solution of bentonite and soda ash. In addition, an attachment to the viscometer (called Fann Yield Stress Adaptor or FYSA) was used to characterize the flow behavior. A rheological model was developed to highlight the bead/bead surface interactions as a major component controlling flow behavior. Four different variants of beads were studied. These were selected to represent a range in surface area per unit volume of beads. Increasing the concentration of beads or the bentonite in solution correlated to increased yield stress and fluid viscosity at operational shear rates. In addition, a Krieger-Dougherty-type relation captured well the effect of the bead concentration, with the maximum packing fraction of beads as a function of surface area per unit volume of the beads. Overall, the Herschel-Bulkley (HB) model best described the suspension rheology with the shear-thinning exponent in the range of ≈0.8 to 1.0. Surface area of the beads linearly correlated to the yield stress of the corresponding concentrated bead solution. Results of this study and the model developed can be used to develop variants of the system with minimal experimentation, thus significantly shortening the design time.

Fluids ◽  
2021 ◽  
Vol 6 (5) ◽  
pp. 178
Author(s):  
Souhail Maazioui ◽  
Abderrahim Maazouz ◽  
Fayssal Benkhaldoun ◽  
Driss Ouazar ◽  
Khalid Lamnawar

Phosphate ore slurry is a suspension of insoluble particles of phosphate rock, the primary raw material for fertilizer and phosphoric acid, in a continuous phase of water. This suspension has a non-Newtonian flow behavior and exhibits yield stress as the shear rate tends toward zero. The suspended particles in the present study were assumed to be noncolloidal. Various grades and phosphate ore concentrations were chosen for this rheological investigation. We created some experimental protocols to determine the main characteristics of these complex fluids and established relevant rheological models with a view to simulate the numerical flow in a cylindrical pipeline. Rheograms of these slurries were obtained using a rotational rheometer and were accurately modeled with commonly used yield-pseudoplastic models. The results show that the concentration of solids in a solid–liquid mixture could be increased while maintaining a desired apparent viscosity. Finally, the design equations for the laminar pipe flow of yield pseudoplastics were investigated to highlight the role of rheological studies in this context.


1996 ◽  
Vol 36 (18) ◽  
pp. 2352-2365 ◽  
Author(s):  
H. R. Azimi ◽  
R. A. Pearson ◽  
R. W. Hertzberg

2011 ◽  
Author(s):  
Pål Løvhaugen ◽  
Balpreet S. Ahluwalia ◽  
Olav G. Hellesø

2013 ◽  
Vol 438-439 ◽  
pp. 67-71
Author(s):  
Qian Qian Zhang ◽  
Jian Zhong Liu ◽  
Jia Ping Liu

The effects of ground slag with different specific surface area on the rheology of mortar at water-binder ratio of 0.25, 0.28 and 0.30 were investigated, and the combined effects of packing density and solid surface area on the rheology of mortar were evaluated in terms of the water film thickness. The results show that with the increasing of specific surface area of slag (220 m2/kg-784 m2/kg), plastic viscosity and yield stress decrease. The correlations of yield stress and plastic viscosity to the water film thickness are basically linear with high correlation R2 values. The action of the ground slag on the rheology of mortar can be characterized by water film thickness, and with the increasing of water film thickness the rheological parameters decrease.


2015 ◽  
Vol 7 (3) ◽  
pp. 21-31 ◽  
Author(s):  
D. R. Kuiry ◽  
S. Bahadur

The steady flow behavior of a viscous, incompressible and electrically conducting fluid between two parallel infinite insulated horizontal porous plates with heat transfer is investigated along with the effect of an external uniform transverse magnetic field, the action of inflow normal to the plates, the pressure gradient on the flow and temperature. The fluid viscosity is supposed to vary exponentially with the temperature. A numerical solution for the governing equations for both the momentum transfer and energy transfer has been developed using the finite difference method. The velocity and temperature distribution graphs have been presented under the influence of different values of magnetic inclination, fluid pressure gradient, inflow acting perpendicularly on the plates, temperature dependent viscosity and the Hartmann number. In our study viscosity is shown to affect the velocity graph. The flow parameters such as viscosity, pressure and injection of fluid normal to the plate can cause reverse flow. For highly viscous fluid, reverse flow is observed. The effect of magnetic force helps to restrain this reverse flow.


2010 ◽  
Vol 44-47 ◽  
pp. 2872-2876
Author(s):  
Pei Li Haw ◽  
Norhamidi Muhamad ◽  
Hadi Murthadha

The rheological behaviors of the Micro Metal Injection Molding feedstock are important for the stability of the feedstock during micro injection molding process and quality of the final micro-components. Homogeneous feedstocks are preferable for MIM process to ensure the dimensional consistency of molded components and prevent the defects of powder-binder separation or particle segregation. In this work, feedstocks with various formulations of 316L stainless steel and binder system were prepared by using Brabender Plastograph EC Plus mixer. The binder system comprises of palm stearin, polyethelene (PE) and stearic acid. In order to obtain the viscosity, activation energy, flow behavior and mold ability index, the rheological characterization of the feedstocks were investigated in numerous conditions by using Shimadzu 500-D capillary rheometer The study showed that all of the 316L stainless steel feedstocks are homogenous with pseudo-plastic behaviors.


Author(s):  
Bahri Kutlu ◽  
Evren M. Ozbayoglu ◽  
Stefan Z. Miska ◽  
Nicholas Takach ◽  
Mengjiao Yu ◽  
...  

This study concentrates on the use of materials known as hollow glass spheres, also known as glass bubbles, to reduce the drilling fluid density below the base fluid density without introducing a compressible phase to the wellbore. Four types of lightweight glass spheres with different physical properties were tested for their impact on rheological behavior, density reduction effect, survival ratio at elevated pressures and hydraulic drag reduction effect when mixed with water based fluids. A Fann75 HPHT viscometer and a flow loop were used for the experiments. Results show that glass spheres successfully reduce the density of the base drilling fluid while maintaining an average of 0.93 survival ratio, the rheological behavior of the tested fluids at elevated concentrations of glass bubbles is similar to the rheological behavior of conventional drilling fluids and hydraulic drag reduction is present up to certain concentrations. All results were integrated into hydraulics calculations for a wellbore scenario that accounts for the effect of temperature and pressure on rheological properties, as well as the effect of glass bubble concentration on mud temperature distribution along the wellbore. The effect of drag reduction was also considered in the calculations.


2020 ◽  
Vol 39 (1) ◽  
pp. 27-39 ◽  
Author(s):  
Sophie Kendall ◽  
Felix Gradstein ◽  
Christopher Jones ◽  
Oliver T. Lord ◽  
Daniela N. Schmidt

Abstract. Changes in morphology during ontogeny can have profound impacts on the physiology and biology of a species. Studies of ontogenetic disparity through time are rare because of the lack of preservation of developmental stages in the fossil record. As they grow by incremental chamber accretion and retain evidence of growth in their shell, planktic foraminifera are an ideal group for the study ontogenetic disparity through the evolution of a higher taxon. Here, we quantify different developmental stages in Jurassic foraminifers and infer the evolutionary implications of the shape of these earliest representatives of the group. Using a Zeiss Xradia micro-CT scanner, the development of Globuligerina bathoniana and Globuligerina oxfordiana from the Bathonian sediments of Gnaszyn, Poland, and Globuligerina balakhmatovae and Globuligerina tojeiraensis from the Kimmeridgian Tojeira Formation of Portugal was reconstructed. Disparity is low through the early evolution of planktic foraminifers. The number of chambers and range in surface area per unit volume are lower than in modern specimens. We interpret this morphology as an indication of opportunistic behaviour. The low morphological plasticity during the juvenile stage suggests that strong constraints on the juveniles, described in the modern ocean, were already acting on Jurassic specimens. The high surface area per unit volume in these developmental stages points towards the need to satisfy a higher metabolic demand than in the adult specimens. We are interpreting the lower chamber numbers as indicative of short life cycles and potentially rapid reproduction, both of which may have allowed these species to exploit the nutrient-rich waters of the Jurassic Tethys Ocean.


Sign in / Sign up

Export Citation Format

Share Document