IMPACT OF WATER AND CO2 ON THE MECHANICAL PROPERTIES OF LOW PERMEABLE ROCKS

Author(s):  
Anatolii A. KISLITSYN ◽  
Nikita V. Lipatov

This article features experiments on triaxial compression of low-permeable dolomite samples with different confining pressures (2-20 MPa), different pore fluids (dry air, water, CO2), and different temperatures (25-150 °C). The authors have studied the effect of confining pressure, pore fluid and temperature on the strength properties of the studied samples. The results show an increase in the strength with grwoing confining pressure. When the confining pressure increases from 2 to 20 MPa, the compressive strength increases from 86 to 370 MPa. Temperature has a significant effect on rock strength under low confining pressure conditions. With the increasing confining pressure reaching 15 MPa, increasing temperature has little effect on the strength of dolomite samples. Under an effective confining pressure of 5 MPa, the temperature weakening occurs on the dolomite specimens when the temperature exceeds 90 °C. During compression, liquid diffusion occurs in the specimens. Higher water viscosity can cause a temporary decrease in effective confining pressure, which can increase the strength of the rock. More prominent fractures are observed in the samples, and more fluid is injected under CO2 injection conditions, which may be useful for increasing the permeability of the geothermal reservoir. Two groups of experiments have been performed on the samples in this study: the first group of experiments investigated the effect of confining pressure on the fracture stress of core samples, without pore fluid injection; the second group of experiments investigated the effect of water or CO2 and temperature on the mechanical properties of core samples.

2020 ◽  
Vol 2020 ◽  
pp. 1-14
Author(s):  
Nao Shen ◽  
Qiang Zhang ◽  
Xiaochun Li ◽  
Bing Bai ◽  
Haixiang Hu

Geothermal energy is an important resource to substitute for traditional fossil fuels. The mechanical properties of reservoir rock under the conditions of water and scCO2 injection at different temperatures are crucial for the safety of Enhanced Geothermal Systems. However, the effects of working fluid on the mechanical properties of granite at in situ temperatures are still rarely reported. To reveal the impact mechanisms, conventional triaxial compression experiments were conducted on granite specimens with different confining pressures (2–20 MPa), different pore fluid (10 MPa water or CO2), and different temperatures (25–150°C) in the present study. SEM analyses were applied to the specimens to determine failure surface morphologies after the experiments. The experimental results show that the effective confining pressure, pore fluid, and temperature have significant effects on the strength of granite specimens. The strength of granite increases with the increase of effective confining pressure, with similar granite strength under the same effective confining pressure (dry, water, and CO2). Temperature strengthening of granite is limited by high confining pressure (∼15 MPa). Under the effective confining pressure of 5 MPa, temperature weakening occurs on granite specimens when temperature is higher than 90°C. There is fluid diffusion in the specimens during compression. The higher viscosity of water may cause a temporary decrease in effective confining pressure, which may increase the strength of granite. The growth or formation of cracks is mainly observed in quartz and feldspar grains without short-term chemical effects. More visible cracks are observed on the specimens and more volume of fluid is injected under CO2 injection conditions, which may be beneficial to increase the permeability of geothermal reservoir.


1994 ◽  
Vol 353 ◽  
Author(s):  
M. Umedera ◽  
A. Fujiwara ◽  
N. Yasufuku ◽  
M. Hyodo ◽  
H. Murata

AbstractA series of triaxial compression tests is being conducted under the drained condition on bentonite and sand mixtures, known as buffer, in saturated and optimum water content states to clarify the mechanical properties of the buffer.It was found that the mechanical properties of bentonite and sand mixtures are strongly influenced by water and bentonite contents: shear strength in a saturated state is less than that in an optimum water content state; shear strength decreases rapidly with increasing bentonite content. Strength properties are much dependent on confining pressure.


2014 ◽  
Vol 501-504 ◽  
pp. 419-425
Author(s):  
Qing Xu ◽  
Jiang Da He ◽  
Hong Qiang Xie ◽  
Ming Li Xiao ◽  
Jian Feng Liu

The mechanical properties of intact rock and rock containing structural plane are very different. From the diversion tunnel of Jinping deep rock site to retrieve the complete block of marble, after a high confining pressure triaxial compression simulation tectonic movements, the formation of structural plane, it represents the mechanical properties of the original rock. On the surface of the marble structure containing triaxial compression creep tests, the results showed: at low confining pressure, the weak marble surface as micro-damage accumulation, the emergence of non-uniform partial destruction, while at high confining pressure, creep curve better continuity and integrity; different confining pressures, marble initial rheology and stability both appear rheological phase, accelerated phase rheological obvious; different confining pressures, the same stage of the axial stress steady flow rate compared with the confining pressure increases, the axial steady state flow rate becomes smaller; marble under test showed the rheological properties, the use of Nishihara model can better demonstrate the rheological properties and determine the rheological parameters for other practical engineering reference.


2019 ◽  
Vol 9 (12) ◽  
pp. 2424 ◽  
Author(s):  
Sijiang Wei ◽  
Yushun Yang ◽  
Chengdong Su ◽  
Syabilla Rachmadina Cardosh ◽  
Hao Wang

In order to study the effect of high temperature on the mechanical properties of rock, two groups of coarse sandstone samples were subjected to the uniaxial compression and triaxial compression test at room temperature of 25 °C and high temperatures of 100~1000 °C. The study comes to some conclusions: (1) With the increase of temperature, the longitudinal wave velocity gradually decreases, and the damage factor of temperature gradually increases. (2) For uniaxial compression tests at different temperatures, the high temperature action within 500 °C has a strengthening effect on the compression strength, and the high temperature effect has a weakening effect on the compression strength when temperatures exceed 500 °C; so 500 °C is the temperature threshold. (3) For triaxial compression tests at different temperatures, the rock strength is positively correlated with temperature and confining pressure when the temperature is lower than 800 °C and the confining pressure is lower than 15 MPa; the rock strength is negatively correlated with temperature and confining pressure when the temperature is over 800 °C and confining pressure is above 15 MPa, so 800 °C is the temperature threshold, and 15 MPa is the confining pressure threshold. (4) In the triaxial compression, the actual fracture angle of the sample after high temperature is basically the same as the theoretical calculation value, high temperature has little effect on the actual fracture angle of the sample, and the actual fracture angle is negatively correlated with the confining pressure.


2012 ◽  
Vol 594-597 ◽  
pp. 218-221
Author(s):  
Yu Wang ◽  
Feng Liu

Using the RMT-150C rock mechanics test system, the instantaneous triaxial compression tests for muddy siltstone were carried out under different confining pressures, and the instantaneous mechanical properties of soft rock were obtained. The results show that the strength parameters of sample have a positive linear relation with the confining pressure, and the sensitivity of peak strength on the confining pressure is higher than that of residual strength. The elastic and deformation modulus of sample linearly increase with the confining pressure going up, and the elastic modulus is more sensitive to the confining pressure. The soft rock sample shows typical ductility failure characteristic, while the damage characteristic is mainly shear failure and the shear failure angle linearly decreases with the confining pressure going up.


2021 ◽  
pp. 105678952199119
Author(s):  
Kai Yang ◽  
Qixiang Yan ◽  
Chuan Zhang ◽  
Wang Wu ◽  
Fei Wan

To explore the mechanical properties and damage evolution characteristics of carbonaceous shale with different confining pressures and water-bearing conditions, triaxial compression tests accompanied by simultaneous acoustic emission (AE) monitoring were conducted on carbonaceous shale rock specimens. The AE characteristics of carbonaceous shale were investigated, a damage assessment method based on Shannon entropy of AE was further proposed. The results suggest that the mechanical properties of carbonaceous shale intensify with increasing confining pressure and degrade with increasing water content. Moisture in rocks does not only weaken the cohesion but also reduce the internal friction angle of carbonaceous shale. It is observed that AE activities mainly occur in the post-peak stage and the strong AE activities of saturated carbonaceous shale specimens appear at a lower normalized stress level than that of natural-state specimens. The maximum AE counts and AE energy increase with water content while decrease with confining pressure. Both confining pressure and water content induce changes in the proportions of AE dominant frequency bands, but the changes caused by confining pressure are more significant than those caused by water content. The results also indicate that AE entropy can serve as an applicable index for rock damage assessment. The damage evolution process of carbonaceous shale can be divided into two main stages, including the stable damage development stage and the damage acceleration stage. The damage variable increases slowly accompanied by a few AE activities at the first stage, which is followed by a rapid growth along with intense acoustic emission activities at the damage acceleration stage. Moreover, there is a sharp rise in the damage evolution curve for the natural-state specimen at the damage acceleration stage, while the damage variable develops slowly for the saturated-state specimen.


Author(s):  
F Li ◽  
V M Puri

A medium pressure (<21 MPa) flexible boundary cubical triaxial tester was designed to measure the true three-dimensional response of powders. In this study, compression behaviour and strength of a microcrystalline cellulose powder (Avicel® PH102), a spray-dried alumina powder (A16SG), and a fluid-bed-granulated silicon nitride based powder (KY3500) were measured. To characterize the mechanical behaviour, three types of triaxial stress paths, that is, the hydrostatic triaxial compression (HTC), the conventional triaxial compression (CTC), and the constant mean pressure triaxial compression (CMPTC) tests were performed. The HTC test measured the volumetric response of the test powders under isostatic pressure from 0 to 13.79MPa, during which the three powders underwent a maximum volumetric strain of 40.8 per cent for Avicel® PH102, 30.5 per cent for A16SG, and 33.0 per cent for KY3500. The bulk modulus values increased 6.4-fold from 57 to 367MPa for Avicel® PH102, 3.7-fold from 174 to 637 MPa for A16SG, and 8.1-fold from 74 to 597MPa for KY3500, when the isotropic stress increased from 0.69 to 13.79 MPa. The CTC and CMPTC tests measured the shear response of the three powders. From 0.035 to 3.45MPa confining pressure, the shear modulus increased 28.7-fold from 1.6 to 45.9MPa for Avicel® PH102, 35-fold from 1.7 to 60.5MPa for A16SG, and 28.5-fold from 1.5 to 42.8MPa for KY3500. In addition, the failure stresses of the three powders increased from 0.129 to 4.41 MPa for Avicel® PH102, 0.082 to 3.62 MPa for A16SG, and 0.090 to 4.66MPa for KY3500, respectively, when consolidation pressure increased from 0.035 to 3.45MPa. In addition, the shear modulus and failure stress values determined from the CTC test at 2.07, 2.76, and 3.45MPa confining pressures are consistently greater than those from the CMPTC test at the same constant mean pressures. This observation demonstrates the influence of stress paths on material properties. The CTT is a useful tool for characterizing the three-dimensional response of powders and powder mixtures.


2017 ◽  
Vol 27 (8) ◽  
pp. 1131-1155 ◽  
Author(s):  
Zhiwei Zhou ◽  
Wei Ma ◽  
Shujuan Zhang ◽  
Cong Cai ◽  
Yanhu Mu ◽  
...  

A series of multistage triaxial compression, creep, and stress relaxation tests were conducted on frozen loess at the temperature of −6℃ in order to study the damage evolution and recrystallization enhancement of mechanical properties during deformation process. The effect of strain rate, confining pressure, and hydrostatic stress history in the degradation laws of mechanical properties is investigated further. The strain rate has a significant influence on the stress–strain curve which dominates the evolution trend of mechanical properties. The mechanical behaviors (strength, stiffness, and viscosity) of frozen loess all exhibit evident response for the consolidation and pressure melting phenomenon caused by the confining pressure. The multistage loading tests under different hydrostatic stresses are capable of differentiating the development characteristics of mechanical properties during axial loading and hydrostatic compression process, respectively. The testing results indicated that the recrystallization of the ice particle in the frozen soils is an important microscopic factor for enhancement behaviors of mechanical parameters during the deformation process. This strengthening degree of mechanical properties is determined by temperature, duration time, deformation degree, and stress state during the recrystallization process. The phase transformation led by pressure melting and ice recrystallization is a nonnegligible changing pattern of frozen soils microstructure, which has apparent role in the damage evolution of mechanical properties.


Geofluids ◽  
2021 ◽  
Vol 2021 ◽  
pp. 1-13
Author(s):  
Liangbin Dou ◽  
Guanli Shu ◽  
Hui Gao ◽  
Jinqing Bao ◽  
Rui Wang

The investigation of changes in physical properties, mechanical properties, and microscopic pore structure characteristics of tight sandstone after high-temperature heat treatment provides a theoretical basis for plugging removal and stimulation techniques, such as high energy gas fracturing and explosive fracturing. In this study, core samples, taken from tight sandstone reservoirs of the Yanchang Formation in the Ordos Basin, were first heated to different temperatures (25-800°C) and then cooled separately by two distinct cooling methods—synthetic formation water cooling and natural cooling. The variations of wave velocity, permeability, tensile strength, uniaxial compressive strength, and microscopic pore structure of the core samples were analyzed. Experimental results demonstrate that, with the rise of heat treatment temperature, the wave velocity and tensile strength of tight sandstone decrease nonlinearly, yet its permeability increases nonlinearly. The tight sandstone’s peak strength and elastic modulus exhibit a trend of the first climbing and then declining sharply with increasing temperature. After being treated by heat at different temperatures, the number of small pores varies little, but the number of large pores increases obviously. Compared to natural cooling, the values of physical and mechanical properties of core samples treated by synthetic formation water cooling are apparently smaller, whereas the size and number of pores are greater. It can be explained that water cooling brings about a dramatic reduction of tight sandstone’s surface temperature, generating additional thermal stress and intensifying internal damage to the core. For different cooling methods, the higher the core temperature before cooling, the greater the thermal stress and the degree of damage caused during the cooling process. By taking into consideration of changes in physical properties, mechanical properties, and microscopic pore structure characteristics, the threshold temperature of tight sandstone is estimated in the range of 400-600°C.


Materials ◽  
2019 ◽  
Vol 12 (10) ◽  
pp. 1662 ◽  
Author(s):  
Jianguo Wang ◽  
Bowen Hu ◽  
Jia Hwei Soon

The variation of physical and mechanical properties of the lightweight bulk filling material with cement and expanded polystyrene (EPS) beads contents under different confining pressures is important to construction and geotechnical applications. In this study, a lightweight bulk filling material was firstly fabricated with Singapore marine clay, ordinary Portland cement and EPS. Then, the influences of EPS beads content, cement content, curing time and confining pressure on the mass density, stress–strain behavior and compressive strength of this lightweight bulk filling material were investigated by unconsolidated and undrained (UU) triaxial tests. In these tests, the mass ratios of EPS beads to dry clay (E/S) were 0%, 0.5%, 1%, 2%, and 4% and the mass ratios of cement to dry clay (C/S) were 10% and 15%. Thirdly, a series of UU triaxial tests were performed at a confining pressure of 0 kPa, 50 kPa, 100 kPa, and 150 kPa after three curing days, seven curing days, and 28 curing days. The results show that the mass density of this lightweight bulk filling material was mainly controlled by the E/S ratio. Its mass density decreased by 55.6% for the C/S ratio 10% and 54.9% for the C/S ratio 15% when the E/S ratio increased from 0% to 4% after three curing days. Shear failure more easily occurred in the specimens with higher cement content and lower confining pressure. The relationships between compressive strength and mass density or failure strain could be quantified by the power function. Increasing cement content and reducing EPS beads content will increase mass density and compressive strength of this lightweight bulk filling material. The compressive strength with curing time can be expressed by a logarithmic function with fitting correlation coefficient ranging from 0.83 to 0.97 for five confining pressures. These empirical formulae will be useful for the estimation of physical and mechanical properties of lightweight concretes in engineering application.


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