scholarly journals Monoazo disperse dyes based on 2-amino-1,3,4-thiadiazole derivatives

2002 ◽  
Vol 67 (11) ◽  
pp. 709-718 ◽  
Author(s):  
Harir Maradiya
Keyword(s):  
Spectral Properties ◽  
Visible Range ◽  
Disperse Dyes ◽  
Fastness Properties ◽  
Light Fastness ◽  
Dyeing Performance ◽  
Brown Colour ◽  
Nylon Fabric ◽  
Monoazo Disperse Dyes ◽  
Dyed Fabric

A series of monoazo disperse dyes based on 2-amino-5-mercapto-1,3,4-thiadiazole was prepared by coupling with various N-arylmaleimides. The dyeing performance of these dyes was assessed on nylon fabric. The dyes were found to give yellow to brown colour shades on dyeing with good depth and levelness on nylon fabric. The dyebath exhaustion fixation and fastness properties of the dyes were also determined. The dyed fabric showed moderate to good light fastness and very good to excellent fastness to washing, rubbing, perspiration and sublimation. The IR and visible range spectral properties of the dyes were also determined.

scholarly journals Synthesis of monoazo disperse dyes based on 2-aminoheterocycles and their dyeing performance on nylon fabrics

2000 ◽  
Vol 65 (11) ◽  
pp. 773-780 ◽  
Author(s):  
Hari Maradiya ◽  
Vithal Patel
Keyword(s):  
Absorption Spectra ◽  
Elemental Analysis ◽  
Disperse Dyes ◽  
Visible Absorption ◽  
Dyeing Performance ◽  
Nylon Fabric ◽  
Wide Range ◽  
Rf Values ◽  
Monoazo Disperse Dyes ◽  
Dyed Fabric

Novel monoazo disperse dyes based on various 2-aminoheterocycles were prepared using N-methyl-N-(2-hydroxyethyl)aniline as the coupling component. All the dyes were applied as disperse dyes on nylon fabric. These dyes have been found to give a wide range of colour shades with very good depth, brightness and levelness on nylon fabric. The visible absorption spectra, elemental analysis and Rf values were investigated. The percentage dye bath exhaustion on fabric was found to be very good. The dyed fabric showed very good to excellent fastness to light, washing, rubbing and perspiration. The sublimation fastness was found to be excellent.

scholarly journals Synthesis and application of 2-aminothiadiazole disperse dyes for nylon fabrics

2001 ◽  
Vol 66 (2) ◽  
pp. 87-93
Author(s):  
Maradiya Raghav ◽  
Vithal Patel
Keyword(s):  
Elemental Analysis ◽  
Spectral Studies ◽  
Disperse Dyes ◽  
Fastness Properties ◽  
Light Fastness ◽  
Nylon Fabric ◽  
Wide Range

Some disperse dyes based on 2-amino-5-mercapto-1,3,4-thiadiazole have been prepared by coupling with various N-arylacrylamides. The dyes were characterized by IR spectral studies and elemental analysis. All the dyes were applied as disperse dyes on nylon fabric. These dyes have been found to give a wide range of color shades with very good depth and levelness on fabrics. The percentage dye bath exhaustion and fixation on the fabric have been found to be very good. The dyied fabrics showed moderate to good light fastness and very good to excellent washing, rubbing, persperation and sublimation fastness properties.

scholarly journals Synthesis and Structural-reactivity Studies of Bifunctional MCT/SES (Monochlorotriazine/ Sulphatoethylsulphone) Azo Reactive Disperse Dyes Applied to Wool and Polyester Fabric

2019 ◽  
pp. 1-10
Author(s):  
Ishegbe Joyce Eko ◽  
Bello Kasali Ademola ◽  
Nkeonye Peter Obinna ◽  
A. A. Kogo
Keyword(s):  
Polyester Fabric ◽  
Cyanuric Chloride ◽  
Disperse Dyes ◽  
Fastness Properties ◽  
Light Fastness ◽  
Dyeing Performance ◽  
Wool Fabrics ◽  
Dyed Fabrics ◽  
Monoazo Dyes

Reactive disperse dyes containing monochlorotriazine/sulphatoethylsulphone reactive moieties were synthesized by condensing aniline with cyanuric chloride and further reacting it with a series of monoazo dyes obtained by diazotising 1-aminobenzene-4-β-sulphatoethylsulphone and coupling with various substituted 2-amino-4-phenylthiazole derivatives. The dyeing performance of the dyes was evaluated on polyester and wool fabrics. The dyes obtained gave various shades ranging from reddish to bright red colours. They had good depth and good levelling properties. They dyed fabrics showed moderate to good light fastness properties and very good to excellent fastness to washing and perspiration. The dye bath exhaustion on the polyester and wool fabrics were found to be very good and their fixation values were moderate.

scholarly journals Synthesis and dyeing performance of some amphiphilic naphthalimide azo disperse dyes on polyester fabrics

2020 ◽  
Vol 85 (10) ◽  
pp. 1253-1264
Author(s):  
Umar Ameuru ◽  
Mohammed Yakubu ◽  
Kasali Bello ◽  
Peter Nkeonye ◽  
Azim Halimehjani
Keyword(s):  
Absorption Spectra ◽  
Electronic Absorption Spectra ◽  
Polyester Fabric ◽  
Disperse Dyes ◽  
Light Fastness ◽  
Visible Absorption ◽  
Polyester Fabrics ◽  
Dyeing Performance ◽  
Azo Disperse Dyes ◽  
Monoazo Disperse Dyes

A series of monoazo disperse dyes were synthesized by coupling diazotized 4-amino-N-dodecyl-1,8-naphthalimide with N,N-dialkyl anilines and naphthol derivatives. The synthesized intermediates and the dyes were characterized using FTIR, 1H-NMR, 13C-NMR, mass spectroscopy and elemental analysis (CHN). Visible absorption spectra of the dyes were examined in solvents of different polarities. The electronic absorption spectra cover a wavelength (?max) range of 515-535 nm in DMF at uniformly absorption intensity between 1.59-3.00?104 L mol-1 cm-1. The dyes gave deep and bright intense hues of light violet, maroon, pink and neon red on polyester fabrics. The dyes generally showed good washing and perspiration rating but poor to moderate light fastness properties on woven polyester fabric and could be recommended for commercial outlets.

Dyeing of Cotton Fabric with Natural Dye Extracted from Egyptian Cotton Leaves

2021 ◽  
Vol 8 (1) ◽  
Keyword(s):  
Natural Dye ◽  
Fastness Properties ◽  
Light Fastness ◽  
Color Strength ◽  
Cotton Variety ◽  
Dyeing Performance ◽  
Dyeing Method ◽  
Exhaust Dyeing ◽  
Egyptian Cotton ◽  
Good Price

Cotton leaves have been used to extract natural dye for dyeing of Egyptian cotton variety Giza 86 fabric and its blend with polyester 50:50, using different mordants such as iron (II) sulfate, copper (II) sulfate, and alum. The exhaust dyeing method was utilized using the pre-mordant technique. It is observed that both fabric samples can be dyed in different colors and depth of shades with Cotton leaves dye. Iron (II) sulfate ensures the best light fastness. Improved light fastness is obtained using abovementioned lower amounts of iron (II) sulfate and copper (II) sulfate. Alum is found to be less effective than iron (II) sulfate and copper (II) sulfate on the light fastness. As a novel alternative and potential natural dye, Cotton leaves extract solution can be used to get various colors and shades with satisfactory fastness properties. The mordanted and un-mordanted fabric samples were tested for their dyeing performance in terms of color parameters K/S, (L*), a*, b*, (C*) and (H*), and fastness properties (wash, perspiration, light and rubbing fastness) were studied. The samples showed high color strength, and high fastness properties. These results are very important for industrial application and with the production of a natural dye as an inexpensive source from cotton leaves as a by-product. Another objective is to increase the production of eco-textile garments with a good price for the Egyptian customers.

scholarly journals Synthesis and Application of Acid Dyes Based on 3-(4-Aminophenyl)-5-benzylidene-2-substituted phenyl-3, 5-dihydroimidazol-4-one

2008 ◽  
Vol 5 (s1) ◽  
pp. S987-S996
Author(s):  
Devang N. Wadia ◽  
Pravin M. Patel
Keyword(s):  
Wool Fabric ◽  
Spectroscopic Methods ◽  
Fastness Properties ◽  
Acid Dyes ◽  
Light Fastness ◽  
Dyeing Performance ◽  
Wool Fibers ◽  
Total Fixation ◽  
Decreasing Ph

A series of eight novel heterocyclic based monoazo acid dyes were synthesized using various substituted imidazol-4-one as diazo component and coupled with various amino-napthol sulphonic acids. The resultant dyes were characterized using standard spectroscopic methods and then dyeing performance on wool fabric was assessed. Final results concluded that exhaustion (%E) of the dyes on wool fibers increased with decreasing pH of application and that fixation (%F) of the dyes on wool fibers increased with increasing pH of application and the highest total fixation efficiency was achieved at pH 5. Wash and light fastness properties of prepared dyes showed encouraging results.

scholarly journals Microwave assisted synthesis of some azo disperse dyes part 2: Eco-friendly dyeing of polyester fabrics by using microwave irradiation

2021 ◽  
Vol 12 (1) ◽  
pp. 64-68
Author(s):  
Mohamed Osman Saleh ◽  
Morsy Ahmed El-Apasery ◽  
Abdelhaleem Mostafa Hussein ◽  
Abu-Bakr Abdelhady El-Adasy ◽  
Magda Mohamed Kamel
Keyword(s):  
Microwave Irradiation ◽  
Disperse Dyes ◽  
Microwave Assisted Synthesis ◽  
Color Intensity ◽  
Light Fastness ◽  
Polyester Fabrics ◽  
Dye Absorption ◽  
Azo Disperse Dyes ◽  
Dyed Fabric ◽  
Green Technique

This study aimed to use microwave irradiation as a green technique, not only to enhance the dyeing efficiency of disperse-colored polyester fabrics, but also to conserve resources and minimize the environmental effects. Arylazopyrazolopyrimidinones dyes 1-9 were applied to polyester fabrics at 2% shade using conventional method and microwave at 100 °C. Both the color intensity expressed as dye absorption and the fastness characteristics of the dyed fabric were investigated. The K/S values are increased by increasing the time of irradiation from 10-60 minutes. The dyed substrate displayed good light fastness, and very good fastness levels to rubbing, perspiration washing, and sublimation, respectively.

Synthesis, spectral properties and application of novel monoazo disperse dyes derived from N-ester-1,8-naphthalimide to polyester

2008 ◽  
Vol 76 (3) ◽  
pp. 684-689 ◽  
Author(s):  
Kamaladin Gharanjig ◽  
Mokhtar Arami ◽  
Hajir Bahrami ◽  
Barahman Movassagh ◽  
Niyaz Mohammad Mahmoodi ◽  
...  
Keyword(s):  
Spectral Properties ◽  
Disperse Dyes ◽  
Monoazo Disperse Dyes

High temperature dyeing of PET fabric with natural colourants extracted from annatto seeds

2019 ◽  
Vol 48 (2) ◽  
pp. 129-136 ◽  
Author(s):  
Monthon Nakpathom ◽  
Buppha Somboon ◽  
Nootsara Narumol ◽  
Rattanaphol Mongkholrattanasit
Keyword(s):  
High Temperature ◽  
Synthetic Dyes ◽  
Fastness Properties ◽  
Light Fastness ◽  
Content Type ◽  
Pet Fabric ◽  
Uv Absorber ◽  
Dyeing Method ◽  
Dyeing Parameters ◽  
Dyed Fabric

Purpose The purpose of this study is to investigate the possibility of dyeing polyester (PET) fabric with natural dye extracted from annatto seeds using high temperature dyeing method. Design/methodology/approach PET fabric was dyed with annatto extract by varying dyeing parameters (temperature, time, pH and dye concentration) to determine the optimum dyeing conditions. The influences of KAl(SO4)2, FeSO4, gallnut mordants or a commercial UV absorber on colour yield and fastness properties were further studied. Findings Optimum results were obtained when the fabric was dyed at 130°C for 30 min in a dyebath containing 15 per cent (owf) annatto dye at pH 6. The dyed fabric had an orange shade and exhibited good to excellent wash, crock, perspiration fastness and fair light fastness. Further dyeing with mordants or UV absorber mostly resulted in lower colour yield and similar fastness properties. Research limitations/implications Although the light fastness was slightly improved to moderate level for the sample with UV absorber, a noticeable colour staining on cotton portion of multi-fibre fabric occurred when subjected to standard washing test. Compared to C.I. Disperse Orange 73, the annatto dye exhibited comparable colour fastness but had inferior light fastness when dyed at approximately the same colour strength. Originality/value Natural colourants from annatto seeds can be used to dye PET fabric at high temperature without mordants, yielding deep orange shade and satisfactory fastness properties. This study provides a promising application to reduce the environmental impact of synthetic dyes.

Synthesis of 4-arylazo-2-(N-pyrazolylcarboxamido)thiophene disperse dyes for dyeing of polyester and their antibacterial evaluation

2020 ◽  
Vol 90 (23-24) ◽  
pp. 2795-2805
Author(s):  
Amal Al-Azmi ◽  
Elizabeth John
Keyword(s):  
Antibacterial Activities ◽  
Antimicrobial Activities ◽  
Disperse Dyes ◽  
Bacterial Strains ◽  
Light Fastness ◽  
Polyester Fabrics ◽  
Nuclear Magnetic Resonance Spectra ◽  
Current Article ◽  
Dyed Fabrics ◽  
Dyed Fabric

The current article aims to synthesize some new arylazo-thiophenes for dyeing polyester fabrics and screen their antimicrobial activities. The new 4-arylazo-2-( N-pyrazolylcarboxamido)-thiophene dyes 4a–e were prepared by the reaction of 2-acetyl-2-arylazo-thioacetanilide derivative 1 with 2-chloro- N-(3-methyl-1 H-pyrazol-5-yl)acetamide derivative 2. The structures of these prepared analogues were established via Fourier-transform infrared and 1H/13C nuclear magnetic resonance spectra. The synthesized dyestuffs were applied to polyester fabrics after establishing the optimal dyeing conditions at 130 ºC, high pressure, 3% shade, and liquor ratio 20:1 at pH 5. Furthermore, the dyed fabrics obtained under these optimal conditions resulted in proper colorfastness toward washing, rubbing, sublimation and perspiration, and were adequate for light fastness. They showed respectable antibacterial effectiveness against two bacterial strains, Staphylococcus aureus (Gram-positive) and Salmonella typhimurium (Gram-negative) bacteria. The dyed fabric with dye 4d displayed the best antibacterial activities with percentage reduction of 88% and 76% against S. aureus and S. typhimurium bacteria, respectively.

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