scholarly journals In Situ Formation of a Metastable β-Ti Alloy by Laser Powder Bed Fusion (L-PBF) of Vanadium and Iron Modified Ti-6Al-4V

Metals ◽  
2018 ◽  
Vol 8 (12) ◽  
pp. 1067 ◽  
Author(s):  
Florian Huber ◽  
Thomas Papke ◽  
Christian Scheitler ◽  
Lukas Hanrieder ◽  
Marion Merklein ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Homogeneous Element ◽  
Alloy Formation ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Β Phase ◽  
Stabilizing Effect

The aim of this work is to investigate the β-Ti-phase-stabilizing effect of vanadium and iron added to Ti-6Al-4V powder by means of heterogeneous powder mixtures and in situ alloy-formation during laser powder bed fusion (L-PBF). The resulting microstructure was analyzed by metallographic methods, scanning electron microscopy (SEM), and electron backscatter diffraction (EBSD). The mechanical properties were characterized by compression tests, both prior to and after heat-treating. Energy dispersive X-ray spectroscopy showed a homogeneous element distribution, proving the feasibility of in situ alloying by LPBF. Due to the β-phase-stabilizing effect of V and Fe added to Ti-6Al-4V, instead of an α’-martensitic microstructure, an α/β-microstructure containing at least 63.8% β-phase develops. Depending on the post L-PBF heat-treatment, either an increased upsetting at failure (33.9%) compared to unmodified Ti-6Al-4V (28.8%), or an exceptional high compressive yield strength (1857 ± 35 MPa compared to 1100 MPa) were measured. The hardness of the in situ alloyed material ranges from 336 ± 7 HV0.5, in as-built condition, to 543 ± 13 HV0.5 after precipitation-hardening. Hence, the range of achievable mechanical properties in dependence of the post-L-PBF heat-treatment can be significantly expanded in comparison to unmodified Ti-6Al-4V, thus providing increased flexibility for additive manufacturing of titanium parts.

scholarly journals Laser Powder Bed Fusion (PBF-LB/M) Process Strategies for In-Situ Alloy Formation with High-Melting Elements

Metals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 336
Author(s):  
Florian Huber ◽  
Michael Rasch ◽  
Michael Schmidt
Keyword(s):  
Homogeneous Element ◽  
Alloying Elements ◽  
Complete Fusion ◽  
Alloy Formation ◽  
Powder Bed Fusion ◽  
High Melting ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Process Strategy

In-situ alloy formation by Laser Powder Bed Fusion (PBF-LB/M) from mixtures of easily available elemental powders is an appealing approach for developing and qualifying new alloys for laser based additive manufacturing of metals. However, especially when dealing with high-melting elements, like W, Ta, Mo, or Nb, it is difficult to achieve a homogeneous element distribution and a complete fusion of the powder particles. The aim of this work was to understand the effects of the PBF-LB/M process parameters (laser power, scan speed, laser spot diameter) and three different single- and double-exposure strategies on the fusion of high-melting W, Ta, Mo, and Nb particles in a Ti-matrix. For this purpose, 220 samples with 10 vol.% of the high-melting particle fraction were prepared and analyzed by optical light microscopy and automated image processing, as well as by scanning electron microscopy (SEM). The results are discussed in the context of current research on the process dynamics of PBF-LB/M. Based on that process strategies to support a complete fusion of high-melting particles during in-situ alloy formation are derived. It is shown that the number of unmolten particles can be at least decreased by a factor of ten compared to the most unfavorable parameter combination. For the lower melting elements, Nb and Mo, a complete fusion without any remaining particles visible in the microsections was achieved for certain parameter combinations. The results prove the feasibility of in-situ alloy formation with high-melting alloying elements, but they also demonstrate the necessity to adjust the PBF-LB/M process strategy to achieve a complete dissolution of the alloying elements.

scholarly journals Heat treatment possibilities for an in situ βTi-TiC composite made by laser powder bed fusion

2020 ◽  
Vol 36 ◽  
pp. 101577
Author(s):  
Sasan Dadbakhsh ◽  
Raya Mertens ◽  
Gang Ji ◽  
Bey Vrancken ◽  
Kim Vanmeensel ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed

scholarly journals Structure and Properties of Ti/Ti64 Graded Material Manufactured by Laser Powder Bed Fusion

Materials ◽  
2021 ◽  
Vol 14 (20) ◽  
pp. 6140
Author(s):  
Evgenii Borisov ◽  
Igor Polozov ◽  
Kirill Starikov ◽  
Anatoly Popovich ◽  
Vadim Sufiiarov
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Additive Manufacturing ◽  
Hot Isostatic Pressing ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Isostatic Pressing ◽  
Graded Material ◽  
Single Part

Multimaterial additive manufacturing is an attractive way of producing parts with improved functional properties by combining materials with different properties within a single part. Pure Ti provides a high ductility and an improved corrosion resistance, while the Ti64 alloy has a higher strength. The combination of these alloys within a single part using additive manufacturing can be used to produce advanced multimaterial components. This work explores the multimaterial Laser Powder Bed Fusion (L-PBF) of Ti/Ti64 graded material. The microstructure and mechanical properties of Ti/Ti64-graded samples fabricated by L-PBF with different geometries of the graded zones, as well as different effects of heat treatment and hot isostatic pressing on the microstructure of the bimetallic Ti/Ti64 samples, were investigated. The transition zone microstructure has a distinct character and does not undergo significant changes during heat treatment and hot isostatic pressing. The tensile tests of Ti/Ti64 samples showed that when the Ti64 zones were located along the sample, the ratio of cross-sections has a greater influence on the mechanical properties than their shape and location. The presented results of the investigation of the graded Ti/Ti64 samples allow tailoring properties for the possible applications of multimaterial parts.

scholarly journals Multi-Laser Powder Bed Fusion Benchmarking—Initial Trials with Inconel 625

2019 ◽  
Vol 105 (7-8) ◽  
pp. 2891-2906 ◽  
Author(s):  
H. Wong ◽  
K. Dawson ◽  
G. A. Ravi ◽  
L. Howlett ◽  
R. O. Jones ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Production Rate ◽  
Single Mode ◽  
Inconel 625 ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Single Laser ◽  
Stress Relieving

Abstract Production rate is an increasingly important factor in the deployment of metal additive manufacturing (AM) throughout industry. To address the perceived low production rate of metal AM systems based on single-laser powder bed fusion (L-PBF), several companies now offer systems in which melting has been parallelised by the introduction of multiple, independently controlled laser beams. Nevertheless, a full set of studies is yet to be conducted to benchmark the efficiency of multi-laser systems and, at the same time, to verify if the mechanical properties of components are compromised due to the increase in build rate. This study addresses the described technology gaps and presents a 4-beam L-PBF system operating in “single multi” (SM) mode (SM-L-PBF) where each of the four lasers is controlled so that it melts all of a particular components’ layers and produces specimens for comparison with standard L-PBF specimens from the same machine. That is all four lasers making all of some of the parts were compared to a single-laser manufacturing all of the parts. Build parameters were kept constant throughout the manufacturing process and the material used was Inconel 625 (IN625). Stress-relieving heat treatment was conducted on As-built (AB) specimens. Both AB and heat-treated (HT) specimen sets were tested for density, microstructure, tensile strength and hardness. Results indicate that the stress-relieving heat treatment increases specimen ductility without compromising other mechanical properties. SM-L-PBF has achieved a build rate of 14 cm3/h when four 200 W lasers were used to process IN625 at a layer thickness of 30 μm. An increase in the build rate of 2.74 times (build time reduction: 63%) has been demonstrated when compared to that of L-PBF, with little to no compromises in specimen mechanical properties. The observed tensile properties exceed the American Society for Testing Materials (ASTM) requirements for IN625 (by a margin of 22 to 26% in the 0.2% offset yield strength). Average specimen hardness and grain size are in the same order as that reported in literatures. The study has demonstrated that a multi-laser AM system opens up opportunities to tackle the impasse of low build rate in L-PBF in an industrial setting and that at least when operating in single mode there is no detectable degradation in the mechanical and crystallographic characteristics of the components produced.

scholarly journals Influence of Powder Bed Temperature on the Microstructure and Mechanical Properties of Ti-6Al-4V Alloy Fabricated via Laser Powder Bed Fusion

Materials ◽  
2021 ◽  
Vol 14 (9) ◽  
pp. 2278
Author(s):  
Lei-Lei Xing ◽  
Wen-Jing Zhang ◽  
Cong-Cong Zhao ◽  
Wen-Qiang Gao ◽  
Zhi-Jian Shen ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
High Strength ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Β Phase ◽  
Phase Precipitate ◽  
Bed Temperature ◽  
Martensitic Microstructure ◽  
Increasing Temperature

Laser powder bed fusion (LPBF) is being increasingly used in the fabrication of complex-shaped structure parts with high precision. It is easy to form martensitic microstructure in Ti-6Al-4V alloy during manufacturing. Pre-heating the powder bed can enhance the thermal field produced by cyclic laser heating during LPBF, which can tailor the microstructure and further improve the mechanical properties. In the present study, all the Ti-6Al-4V alloy samples manufactured by LPBF at different powder bed temperatures exhibit a near-full densification state, with the densification ratio of above 99.4%. When the powder bed temperature is lower than 400 °C, the specimens are composed of a single α′ martensite. As the temperature elevates to higher than 400 °C, the α and β phase precipitate at the α′ martensite boundaries by the diffusion and redistribution of V element. In addition, the α/α′ lath coarsening is presented with the increasing powder bed temperature. The specimens manufactured at the temperature lower than 400 °C exhibit high strength but bad ductility. Moreover, the ultimate tensile strength and yield strength reduce slightly, whereas the ductility is improved dramatically with the increasing temperature, when it is higher than 400 °C.

scholarly journals In Situ Alloying of a Modified Inconel 625 via Laser Powder Bed Fusion: Microstructure and Mechanical Properties

Metals ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 988
Author(s):  
Giulio Marchese ◽  
Margherita Beretta ◽  
Alberta Aversa ◽  
Sara Biamino
Keyword(s):  
Mechanical Properties ◽  
Base Alloy ◽  
Heat Treatments ◽  
Inconel 625 ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Melt Pool ◽  
Composition Modification

This study investigates the in situ alloying of a Ni-based superalloy processed by means of laser powder bed fusion (LPBF). For this purpose, Inconel 625 powder is mixed with 1 wt.% of Ti6Al4V powder. The modified alloy is characterized by densification levels similar to the base alloy, with relative density superior to 99.8%. The material exhibits Ti-rich segregations along the melt pool contours. Moreover, Ti tends to be entrapped in the interdendritic areas during solidification in the as-built state. After heat treatments, the modified Inconel 625 version presents greater hardness and tensile strengths than the base alloy in the same heat-treated conditions. For the solution annealed state, this is mainly attributed to the elimination of the segregations into the interdendritic structures, thus triggering solute strengthening. Finally, for the aged state, the further increment of mechanical properties can be attributed to a more intense formation of phases than the base alloy, due to elevated precipitation strengthening ability under heat treatments. It is interesting to note how slight chemical composition modification can directly develop new alloys by the LPBF process.

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