scholarly journals Texture Evolution in Biocompatible Mg-Y-Re Alloy After Friction Stir Processing

Metals ◽  
2019 ◽  
Vol 9 (11) ◽  
pp. 1181 ◽  
Author(s):  
Kunčická ◽  
Král ◽  
Dvořák ◽  
Kocich

The presented study deals with the investigation of biocompatible WE 43 Mg-based alloy processed via the combination of rotary swaging (RS) and friction stir processing (FSP) at three different rotational speeds of 400 RPM, 800 RPM, and 1200 RPM. The structure observations primarily focused on texture development and characterizations of grain sizes and grain boundaries. The results showed that swaging plus processing at 400 RPM and 1200 RPM lead to substantial recrystallization and grain refinement. The fractions of low angle grain boundaries within the 400 RPM and 1200 RPM samples were approximately 11%, while for the 800 RPM sample exhibiting secondary recrystallization it was about 22%. The grains were also the finest in the 1200 RPM sample (average grain diameter of 1.8 µm). The processed structures exhibited a slight tendency to form the {10-10} <0001> preferential fiber texture (especially the 800 RPM sample). Tensile testing showed the FSP to have positive influence on the ultimate tensile stress, as well as ductility of all the samples; the mechanical properties improved with increasing FSP rate.

Author(s):  
MVNV Satyanarayana ◽  
Adepu Kumar

The present paper studies the influence of different cooling media (water and cryogenic media) on microstructure, mechanical, and corrosion behavior of friction stir processing of AA2014. From the electron backscattered diffraction results, it was observed that the grain size in stir zone of air-cooled friction stir processing, dry ice-cooled friction stir processing, and underwater friction stir processing are 4.9 µm, 3.5 µm, and 0.9 µm respectively, and the fraction of high angle grain boundaries are more in underwater friction stir processing sample compared to other conditions. The ultra-fine grained structure (0.9 µm) was achieved in underwater friction stir processing due to uniform heat dissipation from the processing zone to the water. Mechanical properties such as hardness and strength were improved in underwater friction stir processing compared to other conditions. The fine precipitates formed in the underwater friction stir processing sample were distributed randomly at grain boundaries, and hence corrosion resistance was improved in underwater friction stir processing sample compared to other conditions.


Materials ◽  
2019 ◽  
Vol 12 (19) ◽  
pp. 3215 ◽  
Author(s):  
Abbas Tamadon ◽  
Dirk J. Pons ◽  
Don Clucas ◽  
Kamil Sued

One of the difficulties with bobbin friction stir welding (BFSW) has been the visualisation of microstructure, particularly grain boundaries, and this is especially problematic for materials with fine grain structure, such as AA6082-T6 aluminium as here. Welds of this material were examined using optical microscopy (OM) and electron backscatter diffraction (EBSD). Results show that the grain structures that form depend on a complex set of factors. The motion of the pin and shoulder features transports material around the weld, which induces shear. The shear deformation around the pin is non-uniform with a thermal and strain gradient across the weld, and hence the dynamic recrystallisation (DRX) processes are also variable, giving a range of observed polycrystalline and grain boundary structures. Partial DRX was observed at both hourglass boundaries, and full DRX at mid-stirring zone. The grain boundary mapping showed the formation of low-angle grain boundaries (LAGBs) at regions of high shear as a consequence of thermomechanical nature of the process.


2019 ◽  
Vol 142 (2) ◽  
Author(s):  
Subhash Singh ◽  
Kaushik Pal

Abstract In this study, parent aluminum (Al), silicon carbide (SiC) reinforced Al, zirconia (ZrO2) coated SiC reinforced Al, and lithium zirconate spinel (Li2ZrO3, LZO) encapsulated SiC incorporated Al metal matrix composites were processed via friction stir processing (FSP) technique to observe the influence of grain refinement on mechanical and damping properties. Electron backscattered diffraction (EBSD) analysis were conducted for detailed and deep understanding of possible mechanism and microstructure at longitudinal cross sections of the samples. Further, the room temperature mechanical properties and thermal cyclic (−100 to 400 °C) damping performance of the friction stir processed composites were studied. The results obtained in this investigation show that storage modulus of pristine Al, SiC reinforced Al, ZrO2 coated SiC reinforced Al, and LZO coated SiC reinforced Al were improved by a factor of 1.09, 1.17, 1.09, and 1.38, respectively, after FSP. Additionally, the ultimate tensile strength (UTS) and hardness of the friction stir processed SiC/Li2ZrO3/Al composite were improved by a factor of 1.08 and 1.11, respectively, after FSP was compared with an unprocessed composite.


2020 ◽  
Vol 263 ◽  
pp. 127209 ◽  
Author(s):  
M. Mosayebi ◽  
A. Zarei-Hanzaki ◽  
H.R. Abedi ◽  
A. Ghaderi

2016 ◽  
Vol 2016 ◽  
pp. 1-6
Author(s):  
Zhi-chao Li ◽  
Ning Dang ◽  
Zhen-li Mi

OM (optical microscopy) and EBSD (electron backscatter diffraction) techniques were used to study microstructure and texture distribution during primary recrystallization under different intermediate annealing temperatures in CGO silicon steels. The effect of intermediate annealing temperature on texture distribution in 3% Si electrical steel was analyzed. The results indicate that the microstructure in primary recrystallization matrix of CGO silicon steel is comprised of equiaxed ferrite grains. Mean grain size of primary recrystallization increases with the rising of intermediate annealing temperature.γ-fiber texture is the dominant component in primary recrystallization matrix. With higher intermediate annealing temperature,111121texture and111110texture increase and111121texture is stronger than111110texture. Goss texture was observed to be decreased firstly and then increased. The content of high angle grain boundaries in primary recrystallization matrix are affected by intermediate annealing temperature. When intermediate annealing temperature is increased, high angle grain boundaries are increased firstly and then decreased. Misorientation distribution in primary recrystallized matrix is affected by primary recrystallization annealing temperature either. The content of high angle grain boundaries are increased owing to higher primary recrystallization annealing temperature, which can be a benefit to the abnormal growth of Goss grains in secondary recrystallization.


Author(s):  
Yijie Hu ◽  
Youping Sun ◽  
Jiangmei He ◽  
Dejun Fang ◽  
Jiaxin Zhu ◽  
...  

Abstract Friction stir processing is an important method for acquiring ultrafine-grained materials. In this paper, 3mm ZK60 magnesium alloy sheet was carried for friction stir processing. The best processing parameters with a small grain size and maximum mechanical properties were obtained by comparing different rotation speeds and processing speeds. Fine recrystallized grains and high-angle grain boundaries were observed in stirring zone under different processing parameters. With increasing rotation speed, the grain size and high-angle grain boundary ratio increase; while with increasing processing speed, the grain size decrease, and the ratio of high-angle grain boundaries increase. When rotation speed and processing speed are 1400 r·min-1 and 100 mm·min-1, the processing plate have the largest ultimate tensile strength are 267.52 Mpa, that reached 84.62% of the base metals, and the yield strength, elongation and grain size are 166.97 Mpa, 15.32 % and 1.12 ± 1.64 µm, respectively. The processing plate has more excellent damping performance than rolled.


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