scholarly journals KARAKTERISASI DAN SIFAT KEMAGNETAN PASIR BESI EKSTRAKSI ASAL PANTAI BETAF SARMI, PAPUA

2019 ◽  
Vol 9 (2) ◽  
pp. 27-30
Author(s):  
Endang Haryati ◽  
Khaerian Dahlan ◽  
Shabri Putra Wirman
Keyword(s):  
Saturation Magnetization ◽  
Magnetic Behavior ◽  
Iron Compound ◽  
Xrd Pattern ◽  
Magnetite Fe3o4 ◽  
Coercivity Field ◽  
Behavior Test

Characterization and magnetic behavior test of extracted iron sand from Betaf beach of Sarmi Papua was studied. The purpose of the recearch was to determine minerals content, phase of iron compound, and magnetic behavior of extracted iron sand from Betaf beach of Sarmi Papua were caculate using XRF, XRD and VSM. The result showed that extrated iron sand was contained 43,81% of Iron (Fe), 25,75% of Silika (Si) and 30,44 % others. The XRD pattern showed that the highest peak was magnetite (Fe3O4) at 2= 35,65o.  The histerisis curve of VSM showed that extracted iron sand from Betaf beach of Sarmi Papua was superparamagnetic material where maximum saturation magnetization (Ms) value of 4,54 emu/gr, remanen magnetization (Mr) value of 0,371 emu/gr and coercivity field (Hc) value of 208 Oe.  

The Influence of the Soaking Process on Magnetization Saturation and Coercivity Field of the Classic Amorphous Alloy Fe61Co10Y8Nb1B20.

2018 ◽  
Vol 69 (10) ◽  
pp. 2819-2822
Author(s):  
Marcin Nabialek
Keyword(s):  
Magnetic Field ◽  
Saturation Magnetization ◽  
Coercive Field ◽  
Thermal Treatments ◽  
Solid Samples ◽  
Magnetization Saturation ◽  
Transmission Geometry ◽  
Negative Effect ◽  
Coercivity Field ◽  
The Magnetic Field

This study presents the results of Mossbauer research and magnetic properties. The tests were carried out for amorphous Fe61Co10Y8Nb1B20 alloys produced in the form of strips with a thickness of approximately 35 mm. Mossbauer spectra were measured in transmission geometry for solid samples. Measurements were taken for samples in solidified state and after two heating processes. The first process was carried out at 700K and 60 minutes, the second at 720K and 210 minutes. For the samples prepared in this way, magnetization tests were performed as a function of the magnetic field strength. The values of saturation magnetization and the value of the coercive field were determined from these matrices. It was found that the performed thermal treatments had a negative effect on the value of saturation magnetization and change in the value of the coercive field.

Structural, Morphological and Magnetic Characterization of Sm-substituted Ni-Zn Ferrite

2020 ◽  
Vol 10 (2) ◽  
pp. 152-156 ◽  
Author(s):  
Muhammad Hanif bin Zahari ◽  
Beh Hoe Guan ◽  
Lee Kean Chuan ◽  
Afiq Azri bin Zainudin
Keyword(s):  
Magnetic Properties ◽  
Rare Earth ◽  
Saturation Magnetization ◽  
Sol Gel ◽  
Magnetic Behavior ◽  
Rare Earth Ions ◽  
Ion Concentration ◽  
Zn Ferrite ◽  
Auto Combustion ◽  
Combustion Technique

Background: Rare earth materials are known for its salient electrical insulation properties with high values of electrical resistivity. It is expected that the substitution of rare earth ions into spinel ferrites could significantly alter its magnetic properties. In this work, the effect of the addition of Samarium ions on the structural, morphological and magnetic properties of Ni0.5Zn0.5SmxFe2-xO4 (x=0.00, 0.02, 0.04, 0.06, 0.08, 0.10) synthesized using sol-gel auto combustion technique was investigated. Methods: A series of Samarium-substituted Ni-Zn ferrite nanoparticles (Ni0.5Zn0.5SmxFe2-xO4 where x=0.00, 0.02, 0.04, 0.06, 0.08, 0.10) were synthesized by sol-gel auto-combustion technique. Structural, morphological and magnetic properties of the samples were examined through X-Ray Diffraction (XRD), Field-Emission Scanning Electron Microscope (FESEM) and Vibrating Sample Magnetometer (VSM) measurements. Results: XRD patterns revealed single-phased samples with spinel cubic structure up to x= 0.04. The average crystallite size of the samples varied in the range of 41.8 – 85.6 nm. The prepared samples exhibited agglomerated particles with larger grain size observed in Sm-substituted Ni-Zn ferrite as compared to the unsubstituted sample. The prepared samples exhibited typical soft magnetic behavior as evidenced by the small coercivity field. The magnetic saturation, Ms values decreased as the Sm3+ concentration increases. Conclusion: The substituted Ni-Zn ferrites form agglomerated particles inching towards more uniform microstructure with each increase in Sm3+ substitution. The saturation magnetization of substituted samples decreases with the increase of samarium ion concentration. The decrease in saturation magnetization can be explained based on weak super exchange interaction between A and B sites. The difference in magnetic properties between the samples despite the slight difference in Sm3+ concentrations suggests that the properties of the NiZnFe2O4 can be ‘tuned’, depending on the present need, through the substitution of Fe3+ with rare earth ions.

scholarly journals Structural and magnetic study of metallo-organic YIG powder using 2-ethylhexanoate carboxylate-based precursors

2019 ◽  
Vol 33 (09) ◽  
pp. 1950100 ◽  
Author(s):  
S. Hosseinzadeh ◽  
P. Elahi ◽  
M. Behboudnia ◽  
M. H. Sheikhi ◽  
S. M. Mohseni
Keyword(s):  
Saturation Magnetization ◽  
Annealing Temperature ◽  
Sintering Temperature ◽  
Magnetic Behavior ◽  
Yttrium Iron ◽  
Organic Precursor ◽  
Maximum Value ◽  
Diffraction Peaks ◽  
Iron Garnet ◽  
Organic Decomposition

The crystallization and magnetic behavior of yttrium iron garnet (YIG) prepared by metallo-organic decomposition (MOD) method are discussed. The chemistry and physics related to synthesis of iron and yttrium carboxylates based on 2-ethylhexanoic acid (2EHA) are studied, since no literature was found which elucidates synthesis of metallo-organic precursor of YIG in spite of the literatures of doped YIG samples such as Bi-YIG. Typically, the metal carboxylates used in preparation of ceramic oxide materials are 2-ethylhexanoate (2EH) solvents. Herein, the synthesis, thermal behavior and solubility of yttrium and iron 2EH used in synthesis of YIG powder by MOD are reported. The crystallization and magnetic parameters, including saturation magnetization and coercivity of these samples, smoothly change as a function of the annealing temperature. It is observed that high sintering temperature of [Formula: see text] to [Formula: see text] promotes the diffraction peaks of YIG, therefore, we can conclude that the formation of YIG in MOD method increases the crystallization temperature. The maximum value of saturation magnetization and minimum value of coercivity and remanence are observed for the sample sintered at [Formula: see text] which are 13.7 emu/g, 10.38 Oe and 1.5 emu/g, respectively. This study cites the drawbacks in chemical synthesis of metallo-organic-based YIG production.

scholarly journals Synthesis and Characterization of Super Paramagnetic Magnetite Nanoparticles for Drug Delivery Application

2018 ◽  
Vol 7 (2.19) ◽  
pp. 87
Author(s):  
D BALAJ ◽  
C SARALA RUBI ◽  
N G. RENGANATHAN
Keyword(s):  
Drug Delivery ◽  
Magnetite Nanoparticles ◽  
Fe3o4 Nanoparticles ◽  
Biomedical Application ◽  
Synthesis And Characterization ◽  
Xrd Pattern ◽  
Magnetite Fe3o4 ◽  
Tumor Hyperthermia ◽  
Potential Applications

Attractive nanoparticles have been broadly considered on account of their potential applications as complexity operators in attractive reverberation imaging (MRI) of tumors, cell and DNA partition, attractively guided medication conveyance, tumor hyperthermia. Among the attractive oxides, magnetite nanoparticles are most appropriate because of their low danger and great attractive properties which may be used in drug delivery. Magnetite nanoparticles were synthesized using FeCl3 and FeSO4 as precursors and characterized for size and shape using non-contact AFM.  The formation of magnetite was confirmed by XRD pattern. The elemental composition of the obtained phase was determined using EDAX. In this work, we are aiming to develop drug loaded biopolymer Magnetite nanoparticles for biomedical application. Our main objective is to synthesize and characterize Magnetite (Fe3O4) nanoparticles.  

scholarly journals Extraction of Magnetite from Millscales Waste for Ultrafast Removal of Cadmium Ions

2019 ◽  
Vol 9 (1) ◽  
pp. 5902-5907
Keyword(s):  
Saturation Magnetization ◽  
Milling Time ◽  
Cost Effective ◽  
Xrd Analysis ◽  
High Energy ◽  
Cadmium Ions ◽  
Surface Areas ◽  
Magnetite Fe3o4 ◽  
Micron Size ◽  
20 Nm

This research was conducted to produce the magnetite (Fe3O4 ) nanoparticles extracted from the industrial millscale waste. Then, the micron size samples were extracted and grounded on the high energy ball milling (HEBM) at various milling time for 4, 8, 12, 16 and 20 h. The formation of nanosized single-phase hexagonal spinel has been observed with XRD analysis as early as 4 h milling time. The FTIR transmission spectrum shows the appearance of a Fe-O functional group for each sample. HRTEM images showed that all the samples had a small particle size of 5-20 nm with uniform distribution. The specific surface area of the 5 adsorbents increased after the 8 h milling time and it showed reduction after that. The magnetite adsorbents then utilized the adsorbent in Cadmium ions removal of the aqueous solution. Fe3O4 with 8 h milling time was able to remove 9.81 mg of cadmium ions with 1 g of adsorbents consume. The removal of the cadmium ions detected related to the particles size, surface areas and saturation magnetization. This research successfully revealed that the higher saturation magnetization contributed to high removal percentages in cadmium ions of aqueous solutions. Fe3O4 extraction from mill scales waste is cost-effective, the process is eco-friendly and thus, potentially to be applied for wastewater treatment.

Study of structural, electrical, optical and magnetic properties of Hexaferrite–Polyaniline nanocomposites

2019 ◽  
Vol 33 (13) ◽  
pp. 1950134 ◽  
Author(s):  
Muhammad Ajmal ◽  
M. U. Islam
Keyword(s):  
Saturation Magnetization ◽  
In Situ Polymerization ◽  
Sol Gel ◽  
Electric Polarization ◽  
Room Temperature Resistivity ◽  
Magnetic Studies ◽  
Xrd Pattern ◽  
Gel Technique ◽  
Pani Matrix

Y-type hexagonal ferrite (CaBaCo2Ga[Formula: see text]Fe[Formula: see text]O[Formula: see text]) was synthesized by sol–gel technique. The ferrite–polymer composites (1−x)CaBaCo2Ga[Formula: see text]Fe[Formula: see text]O[Formula: see text]+(x)polyaniline (x=0.25, 0.50, 0.75, 1) namely PF1, PF2, PF3 and polyaniline (PANI) were synthesized by in situ polymerization. The synthesized samples were characterized by XRD, SEM, electrical and dielectric measurements, optical and magnetic studies. XRD pattern reveals a broad peak of polyaniline which is an indication of amorphous nature of PANI. Room-temperature resistivity increases from 2.14 × 101 [Formula: see text]cm to 2.78 × 10[Formula: see text]cm as ferrite content increases due to resistive behavior of the ferrite particles dispersed in the PANI matrix. The value of dielectric constant decreases at fixed frequency with increasing concentration of ferrite filler which is predominantly due to exchange of electrons between Fe[Formula: see text] and Fe[Formula: see text] ions that ultimately results in enhancement of electric polarization and conductivity. The optical bandgap increases with increasing amount of ferrite in the composites. The saturation magnetization and remanence increase with the increase of ferrite filler amount in PANI matrix whereas coercivity decreases. The decrease in coercivity and increase in saturation magnetization are related to Brown’s relation. The present nanocomposite samples may be the best candidates for electromagnetic shielding.

ChemInform Abstract: A POLYMERIC OXALATE (2,2′-BIPYRIDINE)IRON COMPOUND WITH INTERESTING MAGNETIC BEHAVIOR

1985 ◽  
Vol 16 (16) ◽  
Author(s):  
M. BENEDIX ◽  
R. BENEDIX ◽  
C. MICHALK ◽  
J. SUWALSKI
Keyword(s):  
Magnetic Behavior ◽  
Iron Compound

scholarly journals Modification of the Magnetic Properties of Co2Y Hexaferrites by Divalent and Trivalent Metal Substitutions

2015 ◽  
Vol 241 ◽  
pp. 93-125 ◽  
Author(s):  
Sami H. Mahmood ◽  
Muna D. Zaqsaw ◽  
Osama E. Mohsen ◽  
Ahmad Awadallah ◽  
Ibrahim Bsoul ◽  
...  
Keyword(s):  
Magnetic Properties ◽  
Saturation Magnetization ◽  
Exchange Interactions ◽  
High Coercivity ◽  
Xrd Pattern ◽  
A Value ◽  
Type Phase ◽  
Ball Milling Technique ◽  
Xrd Patterns

The present study is concerned with the fabrication and characterization of Me2Y substituted hexaferrites, Ba2Me2Fe12-xTxO22(Me = Co2+, Mg2+, and Cr2+, and T = Fe3+, and Ga3+). The samples were prepared by the conventional ball milling technique and sintering at 1200° C. The effect of the choices of Me and T ions on the structural and magnetic properties of the hexaferrites were investigated. XRD patterns, magnetic parameters, and Mössbauer spectra of the Co2Y were consistent with a single phase Y-type hexaferrite. However, the CoCr-Y sample was found to be dominated by the Y-type hexaferrite, and M-type and BaCrO4minority phases were observed in the XRD pattern of the sample. The small increase in saturation magnetization from about 34 emu/g up to 37.5 emu/g was therefore attributed to the development of the M-type phase. On the other hand, XRD pattern of the Cr2Y sample indicated the dominance of the M-type phase in this sample. The high coercivity (1445 Oe) of this sample is evidence of the transformation of the material from a typically soft magnetic material (Y-type) to a hard magnet (M-type). The Ga-substitution for Fe in Co2Y did not affect the saturation magnetization significantly, but the coercivity was reduced. However, the sample Ba2CoMgFe11GaO22exhibited a significant reduction of the saturation magnetization down to a value 26.6 emu/g, which could be due to the attenuation of the super-exchange interactions induced by the Mg2+substitution.

Magnetization Evolution with Hole Doping Level in (Sr2-xNax)FeMoO6

2011 ◽  
Vol 239-242 ◽  
pp. 3165-3168
Author(s):  
Qin Zhang ◽  
Chang Li ◽  
Zhen Feng Xu ◽  
Ke Yan Wang
Keyword(s):  
Crystal Structure ◽  
Saturation Magnetization ◽  
Doping Level ◽  
Single Phase ◽  
Sol Gel ◽  
Double Perovskite ◽  
Hole Doping ◽  
Cation Ordering ◽  
Xrd Pattern ◽  
Method Effects

Hole doped double perovskite compounds (Sr, Na)2FeMoO6 with the Na content of x = 0, 0.02, 0.03, 0.07 and 0.17 have been synthesized by sol-gel method. Effects of hole doping on the crystal structure and magnetic properties of Sr2FeMoO6 have been investigated. XRD pattern indicates that all the samples are of single phase and belong to the space group I4/m. The degree of cation ordering in the Na-doped Sr2FeMoO6 compounds shows a non-monotonic variation with the doping level. The saturation magnetization of the compound increases with x for x<0.17. Similar to the electron doped Sr2FeMoO6, provided that the doped hole enters selectively the spin-down band, the variation of the saturation magnetization can be explained in light of the ferrimagnetic model (FIM).

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