Effects of Strontium and Calcium on the Microstructure and Grain Size of Cast AZ91 Magnesium Alloy

2011 ◽  
Vol 264-265 ◽  
pp. 789-794
Author(s):  
A. Kiani ◽  
M. Emamy ◽  
E. Fadaei ◽  
Saber Ghannadi
Keyword(s):  
Grain Size ◽  
Electron Microscope ◽  
Magnesium Alloy ◽  
Scanning Electron Microscope ◽  
Phase Distribution ◽  
Optical Microscope ◽  
Uniform Structure ◽  
Az91 Magnesium Alloy ◽  
Az91 Magnesium ◽  
Scanning Electron

The experiments focused on the influence of strontium and calcium as additional alloying elements on the grain size and phase distribution of AZ91 magnesium alloys. For this purpose, different concentrations of Sr (0.01, 0.1, 0.4, and 0.8) and Ca (0.01, 0.1, 0.4, 0.6 and 0.78) were added. The microsturctural examination of specimens was made by an optical microscope and scanning electron microscope. From obtained results it was found that using 0.4 wt% strontium can provide a fine and uniform structure.

Effect of Casting Overheat and Rolling Temperature on Morphology of Sulfide in 30MnVS Steel

2012 ◽  
Vol 457-458 ◽  
pp. 270-273
Author(s):  
Yi You Tu ◽  
Guo Zhong Li
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Continuous Casting ◽  
Optical Microscope ◽  
Rolling Temperature ◽  
Ferrite Content ◽  
Continuous Casting Slab ◽  
Intragranular Ferrite ◽  
Sulfide Segregation ◽  
Scanning Electron

Effect of superheat and initial rolling temperature on the morphology and distribution of sulfide in non quenched and tempered free cutting steel 30MnVS has been studied by optical microscope and scanning electron microscope. Results show that proper superheat and initial rolling temperature can turn rod-shaped sulfide into massive or globular sulfide，to alleviate sulfide segregation and pro-eutectoid ferrite distribution along the boundary of pearlite clusters in 30MnVS , increase the intragranular ferrite content and optimize the structure of continuous casting slab.

Sintering Process of Nd:YAG Transparent Ceramic

2013 ◽  
Vol 281 ◽  
pp. 475-479
Author(s):  
Bo Wang ◽  
Quan Xi Cao ◽  
Guang Xu ◽  
Sen Tian
Keyword(s):  
Grain Size ◽  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Crystal Structures ◽  
Heating Rate ◽  
Optical Transmittance ◽  
Sintering Process ◽  
X Ray ◽  
Polycrystalline Ceramics ◽  
Scanning Electron

1.0at% Nd:YAG polycrystalline ceramics were sintered at 1420°C, 1500°C, 1600°C and 1730°C respectively by different heating rate (1°C/min and 5°C/min). The crystal structures were indexed by X-ray diffractometer (XRD). The microstructure and the grain size of the samples were characterized by scanning electron microscope (SEM). The optical transmittance spectra of the samples were measured using V-570 UV spectrophotometer. The sintering process of Nd:YAG ceramics and the effect of heating rate on the microstructure of samples have been investigated.

Analysis of an Axle Failure under Torsional Load

2016 ◽  
Vol 850 ◽  
pp. 101-106 ◽  
Author(s):  
Shu Mei Li ◽  
Jian Jun Yang ◽  
Wei Dong Zhang ◽  
August Chang ◽  
Cai Xia Zhang ◽  
...  
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Failure Mechanism ◽  
Field Testing ◽  
Optical Microscope ◽  
Fatigue Lifetime ◽  
Torsional Load ◽  
Torsional Fatigue ◽  
Secondary Cracks ◽  
Scanning Electron

Premature fracture of an axle under torsional load occurred after a tracked military tank had experienced field testing for only 80 kilometers. Visual metallographic examinations were performed with optical microscope (OM) and scanning electron microscope (SEM). The investigation demonstrates that the premature fracture is caused by metallurgical problems inside the axle where the primary and secondary cracks originate, propagate, and eventually result in final catastrophic rupture through torsional fatigue. The failure mechanism is summarized and improvement of the fatigue lifetime for the axle is recommended.

Study on the Properties of Doped La in BaBi4Ti4O15 Ceramic

2007 ◽  
Vol 26-28 ◽  
pp. 243-246
Author(s):  
Xing Hua Yang ◽  
Jin Liang Huang ◽  
Xiao Wang ◽  
Chun Wei Cui
Keyword(s):  
Crystal Structure ◽  
Grain Size ◽  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Sintering Temperature ◽  
Solid Phase ◽  
X Ray Diffraction ◽  
X Ray ◽  
Lanthanum Content ◽  
Scanning Electron

BaBi4-xLaxTi4O15 (BBLT) ceramics were prepared by conventional solid phase sintering ceramics processing technology. The crystal structure and the microstructure were detected by X-ray diffraction (XRD) and scanning electron microscope (SEM). The XRD analyses show that La3+ ions doping did not change the crystal structure of BBT ceramics. The sintering temperature increased from 1120°C to 1150°C with increasing Lanthanum content from 0 to 0.5, but it widened the sintering temperature range from 20°C to 50°C and refined the grain size of the BBT ceramic. Additionally, polarization treatment was performed and finally piezoelectric property was measured. As a result, the piezoelectric constant d33 of the 0.1at.% doped BBLT ceramics reached its highest value about 22pc/N at polarizing electric field of 8kV/mm and polarizing temperature of 120°C for 30min.

Investigation on the Microstructure Hardness for the Hot Compressed Duplex Steel

2022 ◽  
Vol 905 ◽  
pp. 30-37
Author(s):  
Shu Lan Zhang ◽  
Xiao Dan Zhang ◽  
Hai Feng Xu ◽  
Chang Wang
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Optical Microscope ◽  
Ferrite Phase ◽  
Ferrite Formation ◽  
Average Hardness ◽  
Duplex Steel ◽  
Quench Temperature ◽  
Fluctuation Range ◽  
Scanning Electron

Effect of microstructure size and type on the hardness for the duplex steel were disclosed by using of optical microscope (OM), scanning electron microscope (SEM) and nanoindenter for the samples hot compressed under different temperature with reduction of 10%, 30%, 50% and 70%. OM and SEM were used to measure the average martensite lamellar width, space and indenter morphology. nanoindenter test characterized the microstructure hardness for the samples under different process. Experiment results show that martensite hardness for the sample hot compressed at 950°C has larger diversity than that of sample hot compressed at 1200°C. The martensite hardness fluctuation range for the sample compressed at 950°C is almost from about 7GPa to 12GPa, while, for the sample compressed at 1200°C, the fluctuation range is basically from about 9GPa to 12GPa. However, the average hardness for the samples hot compressed at 950°C is comparably smaller, which is related with lower quench temperature. The larger martensite hardness fluctuation is mainly related with induced ferrite formation and finer martensite lamellar width. For the ferrite phase, the hardness fluctuation range is lower.

CHARACTERISATION OF BIOMEDICAL TITANIUM LAYERS DEPOSITED BY A VACUUM PLASMA SPRAY PROCESS

2021 ◽  
Vol 55 (2) ◽  
pp. 231-235
Author(s):  
Mihailo Mrdak ◽  
Darko Bajić ◽  
Darko Veljić ◽  
Marko Rakin
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Hardness Test ◽  
Optical Microscope ◽  
Mechanical Tests ◽  
Test Method ◽  
Bonding Layer ◽  
Vacuum Plasma Spray ◽  
Porous Ti ◽  
Scanning Electron

In this paper we will describe the process of the deposition of thick layers of VPS-Ti coating, which is used as a bonding layer for the upper porous Ti coatings on implant substrates. In order to deposit the powder, we used HÖGANÄS Ti powder labelled as AMPERIT 154.086 -63 µm. In order to test the mechanical properties and microstructure of the VPS-Ti coating, the powder was deposited on Č.4171 (X15Cr13 EN10027) steel substrates. Mechanical tests of the microhardness of the coating were performed by the Vickers hardness test method (HV0.3) and tensile strength by measuring the force per unit area (MPa). The microhardness of the coating is 159 HV0.3, which is consistent with the microstructure. The coating was found to have a good bond strength of 68 MPa. The morphology of the powder particles was examined on a scanning electron microscope. The microstructure of the coating, both when deposited and etched, was examined with an optical microscope and a scanning electron microscope. By etching the coating layers, it was found that the structure is homogeneous and that it consists of a mixture of low-temperature and high-temperature titanium phases (α-Ti + β-Ti). Our tests have shown that the deposited layers of Ti coating can be used as a bonding layer for porous Ti coatings in the production of implants.

Clouding of Pressed Potassium Bromide Powder

1972 ◽  
Vol 26 (2) ◽  
pp. 247-251 ◽  
Author(s):  
William P. Norris ◽  
Allen L. Olsen ◽  
Richard G. Brophy
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Adsorbed Water ◽  
Optical Microscope ◽  
Potassium Bromide ◽  
Monomolecular Layer ◽  
Cloudy Region ◽  
Weak Zones ◽  
Ground Powder ◽  
Scanning Electron

The monomolecular layer of water adsorbed on KBr particles is responsible for clouding of disks pressed from finely ground powder. Cloudiness is caused by formation of a multitude of cracks in the disk. The initial cracking can be observed with a low power optical microscope and the extensive cracking in the fully cloudy region is observable with a scanning electron microscope. It is suggested that adsorbed water promotes recrystallization, generating weak zones in the workhardened, elastically stressed disk which fails by cracking.

Influence of prophylaxis on the microleakage of sealants: in vitro study

2002 ◽  
Vol 26 (4) ◽  
pp. 371-375 ◽  
Author(s):  
Ana Beatriz Alonso Chevitarese ◽  
Orlando Chevitarese ◽  
Ivete Pomarico Ribeiro de Souza ◽  
Roberto Braga de Carvalho Vianna
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
In Vitro Study ◽  
Optical Microscope ◽  
Vitro Study ◽  
Significant Difference ◽  
Group A ◽  
Group B ◽  
Scanning Electron

The aim of this study was to evaluate the influence of prophylaxis on the sealants microleakage in 30 premolars divided into: Group A, Group B and Group C. The teeth were analyzed using the optical microscope (OM) and at scanning electron microscope (SEM). There was a statitical significant difference among the groups regarding the presence of microleakage, but not with the presence of tags.

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