Crystallization Kinetics of Fe-B Based Amorphous Alloys Studied In Situ by X-Ray Diffraction and Differential Scanning Calorimetry

2004 ◽  
Vol 453-454 ◽  
pp. 375-380
Author(s):  
P. Tomić ◽  
M. Davidović ◽  
S. Batinić
Keyword(s):  
Differential Scanning Calorimetry ◽  
Crystallization Kinetics ◽  
Amorphous Alloys ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Kinetics Of

A Model for Formation and Consumption of Transient Phase

2011 ◽  
Vol 172-174 ◽  
pp. 646-651 ◽  
Author(s):  
Gamra Tellouche ◽  
Khalid Hoummada ◽  
Dominique Mangelinck ◽  
Ivan Blum
Keyword(s):  
Differential Scanning Calorimetry ◽  
Phase Formation ◽  
Transient Phase ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Proposed Model ◽  
Transient Phases ◽  
Kinetics Of

The phase formation sequence of Ni silicide for different thicknesses is studied by in situ X ray diffraction and differential scanning calorimetry measurements. The formation of a transient phase is observed during the formation of δ-Ni2Si; transient phases grow and disappear during the growth of another phase. A possible mechanism is proposed for the transient phase formation and consumption. It is applied to the growth and consumption of θ-Ni2Si. A good accordance is found between the proposed model and in situ measurement of the kinetics of phase formation obtained by x-ray diffraction and differential scanning calorimetry for higher thickness.

scholarly journals Crystallization Kinetics of Nanocrystalline Materials by Combined X-ray Diffraction and Differential Scanning Calorimetry Experiments

2018 ◽  
Vol 18 (5) ◽  
pp. 3107-3116 ◽  
Author(s):  
Eva Gil-González ◽  
Antonio Perejón ◽  
Pedro E. Sánchez-Jiménez ◽  
Santiago Medina-Carrasco ◽  
Jaroslav Kupčík ◽  
...  
Keyword(s):  
Differential Scanning Calorimetry ◽  
Crystallization Kinetics ◽  
Nanocrystalline Materials ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Kinetics Of

Crystal formation in vanadium-doped zirconia ceramics

CrystEngComm ◽  
2018 ◽  
Vol 20 (22) ◽  
pp. 3105-3116 ◽  
Author(s):  
Roman Svoboda ◽  
Roman Bulánek ◽  
Dušan Galusek ◽  
Roghayeh Hadidimasouleh ◽  
Yadolah Ganjkhanlou
Keyword(s):  
Differential Scanning Calorimetry ◽  
Diffraction Analysis ◽  
Crystal Formation ◽  
X Ray Diffraction ◽  
Zirconia Ceramics ◽  
Scanning Calorimetry ◽  
X Ray

Differential scanning calorimetry and in situ X-ray diffraction analysis were used to study the products and mechanism of crystal formation in VOx–ZrO2 ceramics.

scholarly journals In situ probing of the crystallization kinetics of rr-P3HT on single layer graphene as a function of temperature

2017 ◽  
Vol 19 (12) ◽  
pp. 8496-8503 ◽  
Author(s):  
Nicolas Boulanger ◽  
Victor Yu ◽  
Michael Hilke ◽  
Michael F. Toney ◽  
David R. Barbero
Keyword(s):  
Diffraction Analysis ◽  
Crystallization Kinetics ◽  
Single Layer ◽  
Single Layer Graphene ◽  
X Ray Diffraction ◽  
X Ray ◽  
Layer Graphene ◽  
Kinetics Of

In situ X-ray diffraction analysis of P3HT films during cooling down on both Si and G.

In-Situ X-ray Diffraction Study of the Crystallization Kinetics of Mesoporous Titania Films

2004 ◽  
Vol 108 (34) ◽  
pp. 12698-12706 ◽  
Author(s):  
Bradley L. Kirsch ◽  
Erik K. Richman ◽  
Andrew E. Riley ◽  
Sarah H. Tolbert
Keyword(s):  
Diffraction Study ◽  
Crystallization Kinetics ◽  
Mesoporous Titania ◽  
X Ray Diffraction ◽  
X Ray ◽  
Titania Films ◽  
Kinetics Of

In-Situ Characterisation of Precipitation in AI-Cu thin films

1999 ◽  
Vol 562 ◽  
Author(s):  
J. P. Lokker ◽  
A. J. Bottger ◽  
G. C. A. M. Janssen ◽  
S. Radelaar
Keyword(s):  
Thin Films ◽  
Differential Scanning Calorimetry ◽  
Bulk Material ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Enthalpy Changes ◽  
Thin Foils ◽  
Lower Temperature

ABSTRACTThe precipitate formation occurring in Al-Cu thin foils with copper concentrations of either 1.15 at.% or 0.3 at.%, has been studied. In-situ X-ray diffraction analysis and differential scanning calorimetry are applied to determine the phases formed and the enthalpy changes in the same samples. Both X-ray diffraction and differential scanning calorimetry indicate that the precipitation behaviour of thin films (about 500 nm thickness) differs significantly from that of bulk material. In the films studied the precipitation of Al2Cu occurs at a much lower temperature than expected on the basis of the (bulk) phase diagram. Moreover, no intermediate phases are observed prior to Al2Cu precipitation. Also the amount of Cu in solid solution (0.20 at%Cu) observed by electron-probe micro-analysis after slowly cooling from 500°C to room temperature, exceeds the solubility of bulk Al-Cu.

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