scholarly journals Influence of α-Phase Field Heat Treatment on the Tensile and Primary Creep Resistance of a Powder Metallurgical Processed Ti-45Al-5Nb-0.2B-0.2C Titanium Aluminide Alloy

2017 ◽  
Vol 899 ◽  
pp. 418-423
Author(s):  
Rafael Paiotti Marcondes Guimarães ◽  
Juliano Soyama ◽  
Thomas Ebel ◽  
Márcio C. Fredel ◽  
Florian Pyczak

In powder metallurgical processing the sintering process, as well as heat treatments, can drastically influence microstructure formation. In the case of γ-titanium aluminides, it is critical to achieve certain microstructure parameters, such as colony size, porosity and grain boundary morphology in order to obtain appropriate mechanical properties. In this study, the effect of a heat treatment implemented after sintering with the objective of varying the colony size was investigated. Specimens of Ti-45Al-5Nb-0.2B-0.2C prepared by metal injection moulding and uniaxial pressing of feedstock were used to evaluate the tensile and creep properties. Heat treatments conducted at 1350 and 1400 °C for 3 h led to colony sizes of approximately 100 and 200 μm, respectively. Classically, there is an inverse relationship between grain size and creep resistance, nonetheless, for γ-titanium aluminides, the morphology of the colony boundaries was also found to play a role. The larger colony sizes achieved with the heat treatments did not improve the primary creep resistance, which was explained by the change in the morphology of the colony boundaries as they became larger.

1996 ◽  
Vol 460 ◽  
Author(s):  
F. Herrouin ◽  
P. Bowen ◽  
I. P. Jones

ABSTRACTA complex two phase γ-TiAl alloy, Ti-47Al-lCr-1Mn-2Ta-0.2Si (at.%) in a fully lamellar condition, has been creep tested at a stress of 200MPa and a temperature of 700°C. This simulates the in-service operating conditions for several potential gas turbine aero engine applications where creep resistance is a design limiting material property. The results have indicate that reduction in lamellae thickness and avoidance of feathery type microstructures contribute to improved creep resistance.


2014 ◽  
Vol 657 ◽  
pp. 311-315 ◽  
Author(s):  
Mihai Trifănescu ◽  
Alexandra Banu ◽  
Aurelian Vişan ◽  
Nicolae Ionescu ◽  
Alexandru Paraschiv ◽  
...  

Currently there is a continuous extension of application areas of titanium aluminides but their processing encounters a number of difficulties such as the precision of machining and modifying the properties of the surface layer. In the specialist literature [1, 2, 4, 7] different authors address the processing of these materials by conventional methods. In this context, this paper aims at finding the optimal regimes for the electrical discharge machining (EDM) of titanium aluminides Ti-40Al-5NB-3V and provides the analysis of the process parameters effect on cutting through wire EDM technological characteristics. In the case of wire EDM a relatively good output has been obtained as well as very good roughness of the processed surfaces. On the contrary, when considering the die sinking edm, due to very small output, several experimental measurements were performed on three machines – Sodick, ONA and ELER. Based on the experimental data, it has been established that the best output is to be obtained by reverse polarity machining.


2011 ◽  
Vol 690 ◽  
pp. 210-213 ◽  
Author(s):  
Serge Gavras ◽  
Su Ming Zhu ◽  
Mark A. Easton ◽  
Mark A. Gibson ◽  
Jian Feng Nie

In this study effects of heat treatments on the creep resistance at 177°C/90MPa of a high-pressure die-cast Mg-2.70La-1.50Y (wt.%) alloy were examined. It was found that ageing at 160°C for 24 h (T5) or a solution treatment at 520°C for 1 h (T4) improved creep resistance and caused no blistering on the surface or dimensional changes to the die-cast specimens. TEM was used to characterize the microstructures of heat-treated samples. Improvements to creep resistance might be attributed to the pinning or otherwise retarding of dislocation motion by precipitates and/or solute atoms during creep.


1996 ◽  
Vol 460 ◽  
Author(s):  
F. Appel ◽  
U. Christoph ◽  
R. Wagner

ABSTRACTA two-phase titanium aluminide alloy was systematically doped with carbon to improve its high temperature strength. Solid solutions and precipitates of carbon were formed by different thermal treatments. A fine dispersion of perovskite precipitates was found to be very effective for improving the high temperature strength and creep resistance of the material. The strengthening mechanisms were characterized by flow stresses and activation parameters. The investigations were accompanied by electron microscope observation of the defect structure which was generated during deformation. Special attention was paid on the interaction mechanisms of perfect and twinning dislocations with the carbide precipitates.


2006 ◽  
Vol 514-516 ◽  
pp. 1333-1337 ◽  
Author(s):  
Anibal Guedes ◽  
Ana Maria Pires Pinto ◽  
Manuel F. Vieira ◽  
Filomena Viana

The heat treatment of γ-TiAl alloy (Ti-47Al-2Cr-2Nb (at.%)) diffusion brazed joints was investigated. Joining was performed using a Ti/Ni/Ti clad-laminated braze alloy foil at 1050 and 1150°C with a dwell time of 10 minutes. The joints were subsequently heat treated at 1250 and 1350°C for 240 and 30 minutes, respectively. The microstructure and the chemical composition of the interfaces were analysed by scanning electron microscopy (SEM) and by energy dispersive X-ray spectroscopy (EDS), respectively. Microhardness tests performed across the interface were used to roughly predict the mechanical behaviour of the as-diffusion brazed and of the heat treated joints. Diffusion brazing produced interfaces with two distinct layers essentially composed of α2-Ti3Al and of TiNiAl; γ-TiAl was also detected for joining at 1150°C. After heat treating, the as-diffusion brazed microstructure of the interface was completely replaced by a mixture essentially composed of γ-TiAl and α2–Ti3Al single phase grains and of (α2 + γ) lamellar grains. Microhardness tests showed that the hardness of the as-diffusion brazed interfaces, which ranges from 567 to 844 HV (15 gf), is significantly higher than that of the titanium aluminide alloy (272 HV). All post-joining heat treatments lowered substantially the hardness of the interface, as the hardness of the main phases detected at the interfacial zone after heat treating the joints is comprised between 296 and 414 HV.


Author(s):  
Dominique A. Shepherd ◽  
Vijay K. Vasudevan

The effect of molybdenum additions on the creep properties of two orthorhombic titanium aluminide materials, Ti-22Al-26Nb and Ti-22Al-24.5Nb-1.5Mo (% atomic fraction), has been investigated. Heat treatments below the beta transus temperature followed by a 16-hour ageing treatment produced similar microstructures. Using the similar microstructures (consisting of O laths in a B2 matrix with α2 dispersed at B2 grain boundaries) for the two compositions, tensile creep testing was conducted under stresses of 68 MPa, 160 MPa, and 197 MPa at temperatures of 590 °C and 760 °C. The creep results demonstrated the favorable effects of Mo on creep resistance in these orthorhombic titanium aluminides. Due to similar microstructures, results also suggested that improvements have been substructural, rather than purely microstructural, in nature.


1994 ◽  
Vol 351 ◽  
Author(s):  
S.T. Schwab ◽  
P.P. Paul ◽  
Y-M. Pan

ABSTRACTAlthough plagued by a lack of ductility, titanium aluminides are among the most promising intermetallics under development. Significant improvements in ductility may be obtained from nanostructured intermetallics. Nanosize particles of TiAl3 have been prepared by heat-treatment of chemically synthesized precursor (compound 1). Nanosized TiAl3 has been characterized by chemical analysis, XRD, EDS, NMR, and HREM.


1998 ◽  
Vol 5 (2) ◽  
pp. 86-89 ◽  
Author(s):  
Yong Liu ◽  
Baiyun Huang ◽  
Yuehui He ◽  
Zhongyong Deng

Author(s):  
G. S. Wang ◽  
K. Liu ◽  
S. L. Wang

Present work has systematically investigated the evolution of dispersoid and elevated-temperature properties including the strength and creep resistance during the various multi-step heat treatments in Al-Mn-Mg 3004 alloys. Results show that only α-Al(MnFe)Si dispersoid is observed in the studied temperature range (up to 625°C) and it coarsens with increasing temperature to 500°C but dissolves at 625°C. The evolution of elevated-temperature strength and creep resistance is greatly related to the temperature of each step during the multi-step heat treatments. Generally, lower temperature at the first-step heat treatment leads to higher properties while the properties decrease with increasing temperature of last-step heat treatment. Suitable models have been introduced to explain the evolution of strength and the creep threshold stress at elevated-temperature during the various heat treatments.


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