Effect of Silanization on Microtensile Bond Strength of Different Resin Cements to a Lithium Disilicate Glass Ceramic

2016 ◽  
Vol 17 (2) ◽  
pp. 149-153 ◽  
Author(s):  
Cristina Parise Gré ◽  
Renan C de Ré Silveira ◽  
Shizuma Shibata ◽  
Carlo TR Lago ◽  
Luiz CC Vieira
Keyword(s):  
Bond Strength ◽  
Glass Ceramic ◽  
Hydrofluoric Acid ◽  
Lithium Disilicate ◽  
Resin Cement ◽  
Microtensile Bond Strength ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Silane Coupling ◽  
Adhesive Resin Cement

ABSTRACT Aim This study evaluated the influence of a silane-coupling agent on the bond strength of a self-adhesive cement and a conventional resin cement to a lithium disilicate glass ceramic. Materials and methods A total of eight ceramic blocks were fabricated and divided into four groups (n = 2). In groups 1 and 3, ceramic surfaces were etched with hydrofluoric acid 10% for 20 seconds, rinsed for 30 seconds, and air-dried. One layer of a silane agent was applied onto all ceramic specimens and air-dried for 30 seconds. In groups 2 and 4, ceramic surfaces were etched with hydrofluoric acid, rinsed, and air-dried without application of the silane-coupling agent. The ceramic blocks were bonded to a block of composite with a self-adhesive resin cement or with a conventional resin cement, according to the manufacturer's instructions. After 24 hours in distilled water at 37°C, the specimens were sectioned perpendicular to the bonding interface area to obtain beams with a bonding area of 0.8 mm2 and submitted to a microtensile bond strength test at a crosshead speed of 0.5 mm/min. Data were statistically analyzed with one-way analysis of variance and the Games–Howell post hoc test (p = 0.05). Fractured specimens were examined under optical microscopy at 40× magnification. Results Silanization resulted in higher microtensile bond strength compared to groups without silane. No significant differences were found between the conventional resin cement and the self-adhesive resin cement with silane agent (p = 0.983), and without silane agent (p = 0.877). Conclusion Silanization appears to be crucial for resin bonding to a lithium disilicate-based ceramic, regardless of the resin cement used. The self-adhesive resin cement performed as well as the conventional resin cement. Clinical significance Applying one layer of a silane-coupling agent after etching the ceramic surface with hydrofluoric acid 10% enhanced the bond strength between resin cements and a glass ceramic. How to cite this article Gré CP, de Ré Silveira RC, Shibata S, Lago CTR, Vieira LCC. Effect of Silanization on Microtensile Bond Strength of Different Resin Cements to a Lithium Disilicate Glass Ceramic. J Contemp Dent Pract 2016;17(2):149-153.

The Effect of Aging and Surface treatments on Micro-shear Bond Strength of Resin Nano-Ceramic Material Using Two Resin Cements

2020 ◽  
Author(s):  
Ayman Mohammed Said
Keyword(s):  
Bond Strength ◽  
Hydrofluoric Acid ◽  
Shear Bond Strength ◽  
Surface Treatments ◽  
Resin Cement ◽  
Acid Etching ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Mean Values ◽  
Adhesive Resin Cement

Purpose: To evaluate the effect of aging and different surface treatments on micro-shear bond strength of two resin cements to resin nano-ceramic composite blocks using an in-vitro study. Materials and methods: Blocks of resin nano-ceramic (Lava Ultimate, 3M, St Paul, Minnesota, USA) were used to prepare eight plates having the following dimensions: (14mm × 12mm × 2mm). After plates preparation they were assigned to two main groups according to the surface treatment applied, either hydrofluoric acid etching and silane or sandblasting and silane. Scanning electron microscope (SEM) was used to analyze the surface topography of the Lava-Ultimate plates before and after application of surface treatments. Two resin cements were used; dual cured adhesive resin cement (Bifix QM, VOCO, Cuxhafen, Germany) and dual cured self-adhesive resin cement (Bifix SE, VOCO, Cuxhafen, Germany) to create a five resin micro-cylinders received on each lava ultimate plate. Ten specimens from each subgroup were tested after 24 hours and the other ten specimens were tested after aging in saline for 6 months. Micro-shear bond strength test was applied until failure. . Multi-factorial ANOVA test and One-way ANOVA followed by pair-wise Tukey’s post-hoc tests were used to analyze the data. Results: Both resin cements showed statistically significant decrease on bond strength after aging. Before aging, both surface treatments with adhesive resin cement showed statistically significant higher micro-shear bond strength mean values than with self-adhesive resin cement. After aging sandblasting showed a statistically significant higher micro-shear bond strength mean values with adhesive resin cement, while hydrofluoric acid etching revealed a statistically non-significant higher values with adhesive resin cement than self-adhesive resin cement. Conclusion: For both surface treatments and resin cements aging had a detrimental effect on micro- shear bond strength.

scholarly journals Does Acid Etching Morphologically and Chemically Affect Lithium Disilicate Glass Ceramic Surfaces?

2017 ◽  
Vol 15 (1) ◽  
pp. 93-100 ◽  
Author(s):  
Yukinori Maruo ◽  
Goro Nishigawa ◽  
Masao Irie ◽  
Kumiko Yoshihara ◽  
Takuya Matsumoto ◽  
...  
Keyword(s):  
Phosphoric Acid ◽  
Glass Ceramic ◽  
Hydrofluoric Acid ◽  
Lithium Disilicate ◽  
Resin Cement ◽  
Acid Etching ◽  
Adhesive Resin ◽  
Ceramic Surfaces ◽  
Bond Strengths ◽  
Adhesive Resin Cement

Background This study evaluated the surface morphology, chemical composition and adhesiveness of lithium disilicate glass ceramic after acid etching with hydrofluoric acid or phosphoric acid. Methods Lithium disilicate glass ceramic specimens polished by 600-grit silicon carbide paper were subjected to one or a combination of these surface treatments: airborne particle abrasion with 50-μm alumina (AA), etching with 5% hydrofluoric acid (HF) or 36% phosphoric acid (Phos), and application of silane coupling agent (Si). Stainless steel rods of 3.6-mm diameter and 2.0-mm height were cemented onto treated ceramic surfaces with a self-adhesive resin cement (Clearfil SA Cement). Shear bond strengths between ceramic and cement were measured after 24-hour storage in 37°C distilled water. Results SEM images of AA revealed the formation of conventional microretentive grooves, but acid etching with HF or Phos produced a porous surface. Bond strengths of AA+HF+Si (28.1 ± 6.0 MPa), AA+Phos+Si (17.5 ± 4.1 MPa) and HF+Si (21.0 ± 3.0 MPa) were significantly greater than those of non-pretreated controls with Si (9.7 ± 3.7 MPa) and without Si (4.1 ± 2.4 MPa) (p<0.05). In addition, HF etching alone (26.2 ± 7.5 MPa) had significantly higher bond strength than AA alone (11.5 ± 4.0 MPa) (p<0.05). AA+HF, AA+Phos and HF showed cohesive failures. Conclusions Etching with HF or Phos yielded higher bond strength between lithium disilicate glass ceramic and self-adhesive resin cement without microcrack formation.

Effects of Surface Treatments, Thermocycling, and Cyclic Loading on the Bond Strength of a Resin Cement Bonded to a Lithium Disilicate Glass Ceramic

2013 ◽  
Vol 38 (2) ◽  
pp. 208-217 ◽  
Author(s):  
GB Guarda ◽  
AB Correr ◽  
LS Gonçalves ◽  
AR Costa ◽  
GA Borges ◽  
...  
Keyword(s):  
Bond Strength ◽  
Glass Ceramic ◽  
Hydrofluoric Acid ◽  
Lithium Disilicate ◽  
Surface Treatments ◽  
Resin Cement ◽  
Control Group ◽  
Ceramic Surface ◽  
Microtensile Bond Strength ◽  
Ceramic Blocks

SUMMARY Objectives The aim of this present study was to investigate the effect of two surface treatments, fatigue and thermocycling, on the microtensile bond strength of a newly introduced lithium disilicate glass ceramic (IPS e.max Press, Ivoclar Vivadent) and a dual-cured resin cement. Methods A total of 18 ceramic blocks (10 mm long × 7 mm wide × 3.0 mm thick) were fabricated and divided into six groups (n=3): groups 1, 2, and 3—air particle abraded for five seconds with 50-μm aluminum oxide particles; groups 4, 5, and 6—acid etched with 10% hydrofluoric acid for 20 seconds. A silane coupling agent was applied onto all specimens and allowed to dry for five seconds, and the ceramic blocks were bonded to a block of composite Tetric N-Ceram (Ivoclar Vivadent) with RelyX ARC (3M ESPE) resin cement and placed under a 500-g static load for two minutes. The cement excess was removed with a disposable microbrush, and four periods of light activation for 40 seconds each were performed at right angles using an LED curing unit (UltraLume LED 5, Ultradent) with a final 40 second light exposure from the top surface. All of the specimens were stored in distilled water at 37°C for 24 hours. Groups 2 and 5 were submitted to 3,000 thermal cycles between 5°C and 55°C, and groups 3 and 6 were submitted to a fatigue test of 100,000 cycles at 2 Hz. Specimens were sectioned perpendicular to the bonding area to obtain beams with a cross-sectional area of 1 mm2 (30 beams per group) and submitted to a microtensile bond strength test in a testing machine (EZ Test) at a crosshead speed of 0.5 mm/min. Data were submitted to analysis of variance and Tukey post hoc test (p≤0.05). Results The microtensile bond strength values (MPa) were 26.9 ± 6.9, 22.2 ± 7.8, and 21.2 ± 9.1 for groups 1–3 and 35.0 ± 9.6, 24.3 ± 8.9, and 23.9 ± 6.3 for groups 4–6. For the control group, fatigue testing and thermocycling produced a predominance of adhesive failures. Fatigue and thermocycling significantly decreased the microtensile bond strength for both ceramic surface treatments when compared with the control groups. Etching with 10% hydrofluoric acid significantly increased the microtensile bond strength for the control group.

scholarly journals Microtensile bond strength of restorative composite bonded with self-adhesive resin cements to enamel and dentin

2013 ◽  
Vol 1 (1) ◽  
pp. 3
Author(s):  
Mohammed Al-Saleh ◽  
Omar El-Mowafy
Keyword(s):  
Bond Strength ◽  
Failure Modes ◽  
Tensile Force ◽  
Resin Cement ◽  
Microtensile Bond Strength ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Bonding Agents ◽  
Premature Failure ◽  
Adhesive Resin Cement

PURPOSE: To determine the microtensile bond strength (µTBS) of composite restorations when bonded with self-adhesive resin-cements. METHODS: Thirty caries-free extracted molars were sterilized, and divided into 5 equal groups according to adhesive used: SBMP (Scotch-Bond-Multipurpose, total-etch 3-step adhesive, 3M/ESPE), PAN (PanaviaF-2.0, resin-cement with self-etch primer, Kuraray), RXU (RelyX-Unicem, self-adhesive resin-cement, 3M/ESPE), BRZ (Breeze, self-adhesive resin-cement, Pentron) and MON (Monocem, self-adhesive resin-cement, Shofu). Each group was divided into 2 subgroups (dentin or enamel). Bonding agents, used according to manufacturers’ directions, or a thin layer of resin cement was applied onto teeth flat surfaces. Six mm-thick Filtek-Z250 (3M/ESPE) composite build up was made in three increments. Teeth were sectioned to obtain rectangular specimens which were subjected to tensile force until failure. Specimens were subjected to 1,000 thermo-cycles between 5oC-55°C. Means and standard deviation (SD) were calculated and statistically-analyzed with ANOVA and Tukey’s t-test. Specimens’ failure modes were reported. RESULTS: SBMP showed the highest µTBS results with enamel (24.6(6.1) MPa), PAN showed high µTBS with enamel (12.1(3.9)MPa) and dentin (11.6(4.7)MPa) compared to the other self-adhesive cements. Failure modes were adhesive and mixed for self-adhesive resin-cements. MON subgroups and BRZ enamel subgroup underwent premature failure. CONCLUSION: self-adhesive resin-cements showed low µTBS compared to SBMP.

Development of a Cavity Disinfectant Containing Antibacterial Monomer MDPB

2016 ◽  
Vol 95 (13) ◽  
pp. 1487-1493 ◽  
Author(s):  
N. Hirose ◽  
R. Kitagawa ◽  
H. Kitagawa ◽  
H. Maezono ◽  
A. Mine ◽  
...  
Keyword(s):  
Antibacterial Activity ◽  
Bond Strength ◽  
Bacterial Species ◽  
Oral Bacteria ◽  
Resin Cement ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Significant Difference ◽  
Adhesive Resin Cement

An experimental cavity disinfectant (ACC) that is intended to be used for various direct and indirect restorations was prepared by adding an antibacterial monomer 12-methacryloyloxydodecylpyridinum bromide (MDPB) at 5% into 80% ethanol. The antibacterial effectiveness of ACC and its influences on the bonding abilities of resin cements were investigated. To examine the antibacterial activity of unpolymerized MDPB, the minimum inhibitory and bactericidal concentrations (MIC and MBC) were determined for Streptococcus mutans, Lactobacillus casei, Actinomyces naeslundii, Parvimonas micra, Enterococcus faecalis, Fusobacterium nucleatum, and Porphyromonas gingivalis. Antibacterial activities of ACC and the commercial cavity disinfectant containing 2% chlorhexidine and ethanol (CPS) were evaluated by agar disk diffusion tests through 7 bacterial species and by MIC and MBC measurement for S. mutans. The effects of ACC and CPS to kill bacteria in dentinal tubules were compared with an S. mutans–infected dentin model. Shear bond strength tests were used to examine the influences of ACC on the dentin-bonding abilities of a self-adhesive resin cement and a dual-cure resin cement used with a primer. Unpolymerized MDPB showed strong antibacterial activity against 7 oral bacteria. ACC produced inhibition zones against all bacterial species similar to CPS. For ACC and CPS, the MIC value for S. mutans was identical, and the MBC was similar with only a 1-step dilution difference (1:2). Treatment of infected dentin with ACC resulted in significantly greater bactericidal effects than CPS ( P < 0.05, analysis of variance and Tukey’s honest significant difference test). ACC showed no negative influences on the bonding abilities to dentin for both resin cements, while CPS reduced the bond strength of the self-adhesive resin cement ( P < 0.05). This study clarified that the experimental cavity disinfectant containing 5% MDPB is more effective in vitro than the commercially available chlorhexidine solution to eradicate bacteria in dentin, without causing any adverse influences on the bonding abilities of resinous luting cements.

scholarly journals The Effect of Self-adhesive and Self-etching Resin Cements on the Bond Strength of Nonmetallic Posts in Different Root Thirds

2015 ◽  
Vol 16 (2) ◽  
pp. 147-153 ◽  
Author(s):  
Mateus Rodrigues Tonetto ◽  
Rudys Rodolfo de Jesus Tavarez ◽  
Omar El-Mowafy ◽  
Matheus Coelho Bandeca ◽  
Thiago Soares Porto ◽  
...  
Keyword(s):  
Bond Strength ◽  
Resin Cement ◽  
Resin Cements ◽  
Human Teeth ◽  
Adhesive Resin ◽  
Microtensile Testing ◽  
Special Machine ◽  
Adhesive Resin Cement ◽  
The Difference ◽  
Post Space

ABSTRACT Purpose The purpose of this study was to evaluate the effect of self-adhesive and self-etching resin cements on the bond strength of nonmetallic posts in different root regions. Materials and methods Sixty single-rooted human teeth were decoronated, endodontically treated, post-space prepared, and divided into six groups. Glass-fiber (GF) posts (Exacto, Angelus) and fiber-reinforced composite (FRC) posts (EverStick, StickTeck) were cemented with self-adhesive resin cement (Breeze) (SA) (Pentral Clinical) and self-etching resin cement (Panavia-F) (SE) (Kuraray). Six 1-mm-thick rods were obtained from the cervical (C), middle (M), and apical (A) regions of the roots. The specimens were then subjected to microtensile testing in a special machine (BISCO; Schaumburg, IL, USA) at a crosshead speed of 0.5 mm/min. Microtensile bond strength data were analyzed with two-way ANOVA and Tukey's tests. Results Means (and SD) of the MPa were: GF/SA/C: 14.32 (2.84), GF/SA/M: 10.69 (2.72), GF/SA/A: 6.77 (2.17), GF/SE/C: 11.56 (4.13), GF/SE/M: 6.49 (2.54), GF/SE/A: 3.60 (1.29), FRC/SA/C: 16.89 (2.66), FRC/SA/M: 13.18 (2.19), FRC/SA/A: 8.45 (1.77), FRC/SE/C: 13.69 (3.26), FRC/SE/M: 9.58 (2.23), FRC/SE/A: 5.62 (2.12). The difference among the regions was statistically significant for all groups (p < 0.05). The selfadhesive resin cement showed better results than the selfetching resin cement when compared to each post (p < 0.05). No statistically significant differences in bond strengths of the resin cements when comparable to each post (p > 0.05). Conclusion The bond strength values were significantly affected by the resin cement and the highest values were found for self-adhesive resin cement. How to cite this article da Silva MB, de Jesus Tavarez RR, de Assis FS, Tonetto MR, Porto TS, Bhandi SH, El-Mowafy O, de Toledo Porto Neto S, Bandeca MC. The Effect of Self-adhesive and Self-etching Resin Cements on the Bond Strength of Nonmetallic Posts in Different Root Thirds. J Contemp Dent Pract 2015;16(2):147-153.

scholarly journals The Effect of Hydrofluoric Acid Concentration and Heat on the Bonding to Lithium Disilicate Glass Ceramic

2016 ◽  
Vol 27 (6) ◽  
pp. 727-733 ◽  
Author(s):  
Daniel Sundfeld ◽  
Lourenço Correr-Sobrinho ◽  
Núbia Inocêncya Pavesi Pini ◽  
Ana Rosa Costa ◽  
Renato Herman Sundfeld ◽  
...  
Keyword(s):  
Bond Strength ◽  
Glass Ceramic ◽  
Hydrofluoric Acid ◽  
Lithium Disilicate ◽  
Resin Cement ◽  
Glassy Matrix ◽  
Etching Time ◽  
Sem Images ◽  
Matrix Removal ◽  
Post Hoc

Abstract The aim of this study was to evaluate the effects of hydrofluoric acid (HF) concentration and previous heat treatment (PHT) on the surface morphology and micro-shear bond strength (mSBS) of a lithium disilicate glass ceramic (EMX) to resin cement. One hundred four EMX specimens were randomly assigned to two groups (n=52) according to the HF concentration: 5% and 10%. A new random distribution was made according to the PHTs (n=13): control (no PHT); previously heated HF (70 °C); previously heated EMX surface (85 °C); the combination of heated HF + heated EMX surface. The etching time was set at 20 s. All EMX blocks were silanated and received a thin layer of an unfilled resin. Five resin cement cylinders were made on each EMX surface using Tygon tubes as matrices, and then stored for 24 h at 37 °C. One random etched EMX sample from each group was analyzed using field-emission scanning electron microscopy (FE-SEM). The data were subjected to two-way ANOVA and multiple comparisons were performed using the Tukey post hoc test (a=0.05). For the control groups, 5% HF showed statistically lower mSBS values when compared to 10% HF (p<0.05). PHT increased the mSBS values for 5% HF, yielding statistically similar results to non-PHT 10% HF (p<0.05). FE-SEM images showed increased glassy matrix removal when PHT was applied to HF 5%, but not to the same degree as for 10% HF. PHT has the potential to improve the bond strength of 5% HF concentration on lithium disilicate glass ceramic.

Effect of temporary cements on the microtensile bond strength of self-etching and self-adhesive resin cement

2014 ◽  
Vol 72 (8) ◽  
pp. 762-769 ◽  
Author(s):  
Edilausson Moreno Carvalho ◽  
Ceci Nunes Carvalho ◽  
Alessandro Dourado Loguercio ◽  
Darlon Martins Lima ◽  
José Bauer
Keyword(s):  
Bond Strength ◽  
Resin Cement ◽  
Microtensile Bond Strength ◽  
Adhesive Resin ◽  
Adhesive Resin Cement
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