scholarly journals Temperature Calibration Measurements based on Laser-Induced Phosphorescence Technique for Combustion Applications

2015 ◽  
Vol 10 (1) ◽  
Keyword(s):  
Laser Radiation ◽  
Laser Beam ◽  
Intensity Ratio ◽  
Laser Power ◽  
Room Temperature ◽  
Pulsed Laser ◽  
Temperature Calibration ◽  
Phosphor Powder ◽  
Calibration Methods

Phosphor powder and phosphor-binder mixtures are successfully employed for temperature calibration measurements by using laser-induced phosphorescence (LIP) technique with an emphasis on higher precisions and accuracies than other non-intrusive methods. The phosphorescence intensities are used to perform these calibrations in three different strategies. The influence of laser power regular changes on particles heating and the calibration analyses is also carried out. A pulsed laser at 355 nm was used for exciting specimens of the phosphor powder as well as the phosphor-binder mixtures. The laser beam was directed onto the specimens and varied in three laser power levels (LPLs). The samples were kept in an oven with temperatures ranging from room temperature up to 1800 °C. The three strategies which are expressed in terms of non-dimensional intensity versus wavelength (NDI-W), normalised intensity (NI) and intensity ratio (IR) were used for the calibration assessments. A modified IR was compared with two different IRs. A precision of around ± (0.50-1.41)% was attained for different calibration methods. This research confirmed that these calibrations are possible using three different strategies, given high precisions and accuracies. The laser power alternations influenced the NI and do affect neither the NDI-W nor the IR curves. The laser radiation does not play any role for heating the particles of the studied powder.

Laser Annealing of 8YSZ Powders

2014 ◽  
Vol 1036 ◽  
pp. 168-171
Author(s):  
Andrzej Grabowski ◽  
Grzegorz Moskal ◽  
Mirosława Kępińska
Keyword(s):  
Laser Radiation ◽  
Absorption Coefficient ◽  
Laser Beam ◽  
Laser Power ◽  
Laser Annealing ◽  
Experimental Investigations ◽  
Stabilized Zirconia ◽  
Absorption Coefficients ◽  
Radiation Annealing ◽  
Power Densities

In the article are presented investigations of the reflectance and the absorption coefficient of yttrium partially stabilized zirconia (YPSZ), for 10,6μm wavelength electromagnetic radiation as well as for the wavelengths in the range of 0,5-1,1μm. Based on an experimentally obtained absorption coefficients, the amount of laser power densities absorbed within YPSZ was calculated. Also, experimental investigations with Disk laser and CO2 laser radiation annealing were conducted. It was shown that for different lasers wavelengths and for the same laser beam intensities the microstructural changes in YPSZ are different.

Lasers

2015 ◽  
Author(s):  
Harry Moseley
Keyword(s):  
Laser Radiation ◽  
Laser Beam ◽  
Pulsed Laser ◽  
Expert Advice ◽  
Laser Safety ◽  
Extended Sources ◽  
New Challenges ◽  
Modes Of Interaction

The rapid increase in the use of lasers in healthcare has introduced new challenges. The hazards depend on the characteristics of the laser and the different modes of interaction with tissue. If the laser beam were to strike the unprotected eye, serious damage could occur, the site of damage depending on the wavelength of the laser radiation. The risk is reduced in the case of extended sources but, potentially, may be increased when a repetitively pulsed laser is used. These concepts are all discussed in addition to summarizing current legislation and standards. The laser protection adviser (LPA) is someone who is knowledgeable in the evaluation of risk associated with the use of lasers and has responsibility for provision of expert advice to the user. This chapter contains much useful information for the LPA and others interested in understanding the principles of laser safety.

TEM sample preparation of wear-tested room-temperature pulsed-laser-deposited thin films of MoS2 by ultramicrotomy

1993 ◽  
Vol 51 ◽  
pp. 1118-1119
Author(s):  
Pamela F. Lloyd ◽  
Scott D. Walck
Keyword(s):  
Thin Films ◽  
Sample Preparation ◽  
Room Temperature ◽  
High Vacuum ◽  
Pulsed Laser ◽  
Ultra High Vacuum ◽  
Wear Testing ◽  
Preparation Technique ◽  
Cross Sectional ◽  
Aerospace Applications

Pulsed laser deposition (PLD) is a novel technique for the deposition of tribological thin films. MoS2 is the archetypical solid lubricant material for aerospace applications. It provides a low coefficient of friction from cryogenic temperatures to about 350°C and can be used in ultra high vacuum environments. The TEM is ideally suited for studying the microstructural and tribo-chemical changes that occur during wear. The normal cross sectional TEM sample preparation method does not work well because the material’s lubricity causes the sandwich to separate. Walck et al. deposited MoS2 through a mesh mask which gave suitable results for as-deposited films, but the discontinuous nature of the film is unsuitable for wear-testing. To investigate wear-tested, room temperature (RT) PLD MoS2 films, the sample preparation technique of Heuer and Howitt was adapted.Two 300 run thick films were deposited on single crystal NaCl substrates. One was wear-tested on a ball-on-disk tribometer using a 30 gm load at 150 rpm for one minute, and subsequently coated with a heavy layer of evaporated gold.

Influence of Continuous and Pulsed Laser Radiation on Optical and Thermal Properties of Biological Tissues

2014 ◽  
Vol 59 (12) ◽  
pp. 1149-1154
Author(s):  
A.D. Mamuta ◽  
◽  
V.S. Voitsekhovich ◽  
N.M. Kachalova ◽  
L.F. Golovko ◽  
...  
Keyword(s):  
Thermal Properties ◽  
Laser Radiation ◽  
Pulsed Laser ◽  
Biological Tissues ◽  
Pulsed Laser Radiation

scholarly journals Annealing Condition Effects on the Structural Properties of FePt Nanoparticles Embedded in MgO via Pulsed Laser Deposition

Nanomaterials ◽  
2021 ◽  
Vol 11 (1) ◽  
pp. 131
Author(s):  
Tingting Xiao ◽  
Qi Yang ◽  
Jian Yu ◽  
Zhengwei Xiong ◽  
Weidong Wu
Keyword(s):  
Pulsed Laser Deposition ◽  
Room Temperature ◽  
High Vacuum ◽  
Pulsed Laser ◽  
Annealing Process ◽  
Ultra High Vacuum ◽  
Laser Deposition ◽  
Fept Nanoparticles ◽  
Annealing Conditions ◽  
Vacuum Atmosphere

FePt nanoparticles (NPs) were embedded into a single-crystal MgO host by pulsed laser deposition (PLD). It was found that its phase, microstructures and physical properties were strongly dependent on annealing conditions. Annealing induced a remarkable morphology variation in order to decrease its total free energy. H2/Ar (95% Ar + 5% H2) significantly improved the L10 ordering of FePt NPs, making magnetic coercivity reach 37 KOe at room temperature. However, the samples annealing at H2/Ar, O2, and vacuum all showed the presence of iron oxide even with the coverage of MgO. MgO matrix could restrain the particles’ coalescence effectively but can hardly avoid the oxidation of Fe since it is extremely sensitive to oxygen under the high-temperature annealing process. This study demonstrated that it is essential to anneal FePt in a high-purity reducing or ultra-high vacuum atmosphere in order to eliminate the influence of oxygen.

scholarly journals Laser Superficial Fusion of Gold Nanoparticles with PEEK Polymer for Cardiovascular Application

Materials ◽  
2021 ◽  
Vol 14 (4) ◽  
pp. 971
Author(s):  
Oktawian Bialas ◽  
Mateusz Lis ◽  
Anna Woźniak ◽  
Marcin Adamiak
Keyword(s):  
Particle Size ◽  
Laser Beam ◽  
Gold Particle ◽  
Laser Power ◽  
Biomedical Application ◽  
Parameters Optimization ◽  
Size Reduction ◽  
Particle Size Reduction ◽  
Nano Gold ◽  
Gold Particle Size

This paper analyses the possibility of obtaining surface-infused nano gold particles with the polyether ether ketone (PEEK) using picosecond laser treatment. To fuse particles into polymer, the raw surface of PEEK was sputtered with 99.99% Au and micromachined by an A-355 laser device for gold particle size reduction. Biomimetic pattern and parameters optimization were key properties of the design for biomedical application. The structures were investigated by employing surface topography in the presence of micron and sub-micron features. The energy of the laser beam stating the presence of polymer bond thermalisation with remelting due to high temperature was also taken into the account. The process was suited to avoid intensive surface modification that could compromise the mechanical properties of fragile cardiovascular devices. The initial material analysis was conducted by power–depth dependence using confocal microscopy. The evaluation of gold particle size reduction was performed with scanning electron microscopy (SEM), secondary electron (SE) and quadrant backscatter electron detector (QBSD) and energy dispersive spectroscopy (EDS) analysis. The visibility of the constituted coating was checked by a commercial grade X-ray that is commonly used in hospitals. Attempts to reduce deposited gold coating to the size of Au nanoparticles (Au NPs) and to fuse them into the groove using a laser beam have been successfully completed. The relationship between the laser power and the characteristics of the particles remaining in the laser irradiation area has been established. A significant increase in quantity was achieved using laser power with a minimum power of 15 mW. The obtained results allowed for the continuation of the pilot study for augmented research and material properties analysis.

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