Behaviour of Compacted Filtered Iron Ore Tailings–Portland Cement Blends: New Brazilian Trend for Tailings Disposal by Stacking

Failures of tailings dams, primarily due to liquefaction, have occurred in Brazil in recent years. These events have prompted the Brazilian government to place restrictions on the construction of new dams, as iron ore tailings deposited behind upstream dams by spigotting have been shown to have low in situ densities and strengths and are prone to failure. This work proposes a new trend for tailings disposal: stacking compacted filtered ore tailings–Portland cement blends. As part of the proposal, it analyses the behaviour of compacted iron ore tailings–Portland cement blends, considering the use of small amounts of Portland cement under distinct compaction degrees. With the intention of evaluating the stress–strain–strength–durability behaviour of the blends, the following tests were carried out: unconfined compression tests; pulse velocity tests; wetting–drying tests; and standard drained triaxial compression tests with internal measurement of strains. This is the first study performed to determine the strength and initial shear stiffness evolution of iron ore tailings–Portland cement blends during their curing time, as well friction angle and cohesion intercept. This manuscript postulates an analysis of original experimental results centred on the porosity/cement index (η/Civ). This index can help select the cement quantity and density for important design parameters of compacted iron ore tailings–cement blends required in geotechnical engineering projects such as the proposed compacted filtered iron ore tailings–cement blends stacking.

Microscopic Mechanism Angle of Repose in Friable Loess and Its Relationship With Slope Angle

The angle of repose in soil particles plays a key role in slope stability. There was a need for the investigation on the association between the angle of repose in loess particles and the angle of slopes. The fixed funnel methods with different particle sizes were carried out. The pressure of particle gravity weight was obtained based on the vibration stacking test. Four contact structures in loess particles were put forward including the triangular pyramid contact structure (TS), rectangular pyramid contact structure (RS), pentagonal pyramid contact structure (PS), and hexagon contact structure (HS). The particles transformed successively in four kinds of contact structures. The transformation of entropy value of the particles in different accumulation areas was discussed during the process of accumulation. The relationship between the natural angle of repose and the evolution of the contact structures was established. Combined with the existing experimental conclusion that loess particles transform in four stable states, in turn, the reason that the friction angle of uniform sand particles proposed by Shields in 1936 is 33° was explained. The formation theory of the loess angle of repose was well extended to speculate the formation process of the loess slope system. It is verified that loess slopes were mainly distributed under 30°.

Studying the Failure Behavior of Cement-fiber-treated Sand under Triaxial Direct Tension Tests

The main goal of this research is to study the failure behavior of cement-fiber-treated sand under triaxial direct tension condition tests. Thus, a new loading system and triaxial cell was designed and built for tensile loading. Samples were prepared with content cement of 3 and 5% (dry wt.) of the sand, while two types of polypropylene fibers 0.024 m in length and 23 μm and 300 μm thick were added at 0.0% and 0.5% (dry wt.) of the sand and cement mixture. After a seven-day curing period, the samples were loaded under triaxial direct tension tests under confining pressures of 100, 200, and 300 kpa in drained conditions. Stress-strain behavior, changes in volume and energy absorbed by cement-fiber reinforced sand were measured and compared with the results of other studies. Adding fibers resulted in reduced peak deviatoric stress and increased residual deviatoric stresses of the cement-fiber reinforced sand, with changes from brittle to ductile behavior. The initial stiffness and stiffness at 50% maximum tensile stress of the samples is decreased with the addition of fibers and with an increase in fiber diameter, the reduction rate of this stiffness is more evident. The absorbed energy for fibers with a thickness of 23 μm is less than fibers with a thickness of 300 μm. The effect of adding fibers to strength parameters showed that the cohesion intercept decreases, while the internal friction angle increases.

Experimental Study on the Reliability of Scaling Down Techniques Used in Direct Shear Tests to Determine the Shear Strength of Rockfill and Waste Rocks

The determination of shear strength parameters for coarse granular materials such as rockfill and waste rocks is challenging due to their oversized particles and the minimum required ratio of 10 between the specimen width (W) and the maximum particle size (dmax) of tested samples for direct shear tests. To overcome this problem, a common practice is to prepare test samples by excluding the oversized particles. This method is called the scalping scaling down technique. Making further modifications on scalped samples to achieve a specific particle size distribution curve (PSDC) leads to other scaling down techniques. Until now, the parallel scaling down technique has been the most popular and most commonly applied, generally because it produces a PSDC parallel and similar to that of field material. Recently, a critical literature review performed by the authors revealed that the methodology used by previous researchers to validate or invalidate the scaling down techniques in estimating the shear strength of field materials is inappropriate. The validity of scaling down techniques remains unknown. In addition, the minimum required W/dmax ratio of 10, stipulated in ASTM D3080/D3080M-11 for direct shear tests, is not large enough to eliminate the specimen size effect (SSE). The authors’ recent experimental study showed that a minimum W/dmax ratio of 60 is necessary to avoid any SSE in direct shear tests. In this study, a series of direct shear tests were performed on samples with different dmax values, prepared by applying scalping and parallel scaling down techniques. All tested specimens had a W/dmax ratio equal to or larger than 60. The test results of the scaled down samples with dmax values smaller than those of field samples were used to establish a predictive equation between the effective internal friction angle (hereafter named “friction angle”) and dmax, which was then used to predict the friction angles of the field samples. Comparisons between the measured and predicted friction angles of field samples demonstrated that the equations based on scalping scaling down technique correctly predicted the friction angles of field samples, whereas the equations based on parallel scaling down technique failed to correctly predict the friction angles of field samples. The scalping down technique has been validated, whereas the parallel scaling down technique has been invalidated by the experimental results presented in this study.

ANALYSIS OF EMBANKMENT SLOPE STEEPNESS AND STABILITY

This paper describes the stability calculations of the most common road embankments slopes and their results using the modified Bishop method. By searching for the smallest possible effective angle of internal friction of the different slope steepness embankments, the possible different bases of the embankment, the weight of the embankment soil, the load caused by transport and the location of load application (shoulder) were evaluated. Analyzing the obtained calculation results, it was determined that at a slope of 1:2 (26.57°) steepness, to ensure slope stability, the calculated effective internal friction angle of the embankment soil should be φʹd ≥ 28.5°, and at a slope of 1:1.75 (29.74°) steepness – φʹd ≥ 29.8°. When the slope is 2:3 (33.69°) steepness, the stability of the slope cannot be guaranteed.

Experimental Study on the Effect of Freezing and Thawing on the Shear Strength of the Frozen Soil in Qinghai-Tibet Railway Embankment

The direct shear tests of different dry density and moisture content samples at different temperatures of the frozen soil in the Qinghai-Tibet Railway embankment between Tanggula South and Anduo section were carried out to analyze the influence rules of each experimental factor on the mechanical properties of frozen soil during the freeze-thaw process. The results show the following. (1) When the frozen soil temperature is below 0°C and continues to drop during the freezing and thawing process, each sample shows the law of a significant increase in cohesion and a slight decrease in the internal friction angle. In the meantime, the cohesion obtained during the thawing process of the sample at the same temperature point is higher than that obtained during the freezing process. In contrast, the internal friction angles exhibit an opposite law, where the internal friction angle during the melting process is lower than the internal friction angle during the freezing process. After freezing-thawing action, it deserves to be mentioned that the cohesion increases slightly while the internal friction angles present a slight decrease trend compared to the initial state. (2) With the decrease in temperature and the gradual increase in cohesion, the temperature curve can be divided into a fast-growing section from 0 to −2°C, a slow-growing section from −2 to −8°C, and a second fast-growing section from −8 to −10°C owing to the combined effect of the pressure-thawing action and ice-water phase change. In addition, the rate of decrease in the internal friction angle also shows a similar pattern. (3) The cohesion and the internal friction angle of samples both tend to increase first and then decrease with the rise of the initial moisture content, and the critical initial moisture content is near the optimal moisture content of 15%. (4) Both the cohesion and the internal friction angle of the samples increase with dry density growth. The growth rate of cohesion will gradually increase as the temperature decreases. Moreover, the growth rate of cohesion of low dry density samples is more susceptible to temperature, while the internal friction angle growth rate is not affected by temperature.

Experimental Studies of Scale Effect on the Shear Strength of Coarse-Grained Soil

Shear strength is an essential index for the evaluation of soil stability. Test results of the shear strength of scaled coarse-grained soil (CGS for short) are usually not able to accurately reflect the actual properties and behaviors of in situ CGS due to the scale effect. Therefore, this study focuses on the influence of the scale effect on the shear strength of scaled CGS, which has an important theoretical significance and application for the strength estimation of CGS in high earth-rock dam engineering. According to previous studies, the main cause of the scale effect for scaled CGS is the variation of the gradation structure as well as the maximum particle size (dmax), in which the gradation structure as a characteristic parameter can be expressed by the gradation area (S). A total of 24 groups of test soil samples with different gradations were designed by changing the maximum particle size dmax and gradation area S. Direct shear tests were conducted in this study to quantitatively explore the effect of the gradation structure and the maximum particle size on the shear strength of CGS. Test results suggest that the shear strength indexes (i.e., the cohesion and internal friction angle) of CGS present an increasing trend with the improvement of the maximum particle size dmax, and thus a logarithmic function relationship among c, φ, and dmax is presented. Both cohesion (c) and internal friction angle (φ) are negatively related to the gradation area (S) in most cases. As a result, an empirical relationship between c, φ, and S is established based on the test results. Furthermore, a new prediction model of shear strength of CGS considering the scale effect is proposed, and the accuracy of this model is verified through the test results provided by relevant literature. Finally, the applicability of this model to different types of CGS is discussed.

Analytical model of bolt shear resistance considering progressive yield of surrounding material

Existing analytical models usually fail to match with the actual conditions due to ignoring the nonlinear behavior of the surrounding material reaction force, which changes progressively with the joint shear displacement from elastic stage to yield stage. To tackle this problem, this study proposes a new analytical model to describe the bolt deformation and bolt contribution from elastic stage to plastic stage. The developed model is verified by available experimental direct shear tests of bolted joints and compared with existing models. Then, based on this model, the effects of the joint dilation angle, the bolt installation angle, the friction angle, and the surrounding material strength on bolt contribution are also analyzed and its implication is further discussed. Our results show that the proposed model can precisely describe the evolution of bolt contribution from elastic stage to plastic stage. Compared with surrounding material strength, the augmentation of the joint dilation angle and friction angle is more beneficial to increase the bolt contribution and the optimal installation angle. The work presented is to attempt to provide a reference for the understanding of bolting mechanism of jointed rock mass, the development of bolting theories and the practice of bolting engineering.

Assessment of Abrasion-Induced Visual Defects in Twin Screw Wet Granulation Using Wall Friction Measurements

Starting point of the presented study were abrasion effects occurring during a twin screw wet granulation (TSG) process of a new chemical entity (NCE) formulation, resulting in gray spots on the final tablets. Several actions and systematic changes of equipment and process parameter settings of TSG process were conducted which reduced the visual defect rate of the tablets, i.e., gray spots on the surface, below the specification limit. To understand the rationale and mechanism behind these improvements, correlations of defect rates and wall friction measurements using a Schulze ring shear tester were evaluated. To check the suitability of the method, a broad range of wall materials as well as powder formulations at various moisture levels were investigated with regard to their wall friction angle. As differences in wall friction angle could be detected, further experiments were conducted using wall material samples made out of different screw materials for TSG. Evaluation of these screw wall material samples gave first hints, which screw materials should be preferred in regard of friction for TSG process. In the finally presented case study, wall friction measurements were performed using the above mentioned NCE formulation with known abrasion issues at TSG processing. The results confirmed that changes which led to a reduced visual defect rate of tablets correlated with a decreased wall friction angle. The results suggest wall friction measurements as a potent tool for equipment selection and establishment of a suitable process window prior to conducting TSG experiments. Graphical abstract