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2020 ◽  
Vol 71 (6) ◽  
pp. 368-377
Author(s):  
Valeriu Robert Badescu ◽  
Olga Tiron ◽  
Gabriela Geanina Vasile ◽  
Laurentiu Razvan Dinu

The research aimed to provide an optimized method for the determination of iodides concentration in groundwater and surface water sources using ion chromatography technique. The analyses were conducted by using a conductivity detector, with a 35 mM KOH mobile phase, at a flow rate of 1 mL/min, the temperature in the detector chamber and the intensity of the suppressor current being set at 350C and 87 mA, respectively. The interferences given by other ions were also investigated, and the performance parameters were determined such as detection limit, quantification limit, accuracy, and recovery.


2016 ◽  
Vol 19 (4) ◽  
pp. 126-130
Author(s):  
Thanh Thien Tran ◽  
Tao Van Chau ◽  
Laurent Ferreux ◽  
Marie Christine Lépy

This paper describes a simple method to reduce the radon background component applied in environmental studies using gamma spectrometry. The radon component can be reduced by introducing either nitrogen gas or clean air into the detector chamber in order to create a positive pressure and further minimize radon intrusion from outside. This method shows that we can minimize the influence of radon daughter background such as 214Pb, 214Bi and 210Pb (from 238U), 212Pb, 212Bi and 208Tl (from 232Th). By the way, the detection limit of the gamma spectrometry is discussed.


2013 ◽  
Vol 79 (5) ◽  
pp. 489-507 ◽  
Author(s):  
R. MILLS ◽  
R. BOOKER ◽  
Y. LU

AbstractUnder a study contracted by GEN3 Partners, spectra of high current pinch discharges in pure hydrogen and helium were recorded in the extreme ultraviolet radiation region at the Harvard Smithsonian Center for Astrophysics (CfA) in an attempt to reproduce experimental results published by BlackLight Power, Inc. (BLP) showing predicted continuum radiation due to hydrogen in the 10–30 nm region (Mills, R. L. and Lu, Y. 2010 Hydrino continuum transitions with cutoffs at 22.8 nm and 10.1 nm. Int. J. Hydrog. Energy35, 8446–8456, doi:10.1016?j.ijhydene.2010.05.098). Alternative explanations were considered to the claimed interpretation of the continuum radiation as being that emitted during transitions of H to lower-energy states (hydrinos). Continuum radiation was observed at CfA in the 10–30 nm region that matched BLP's results. Considering the low energy of 5.2 J per pulse, the observed radiation in the energy range of about 120–40 eV, reference experiments and analysis of plasma gases, cryofiltration to remove contaminants, and spectra of the electrode metal, no conventional explanation was found in the prior or present work to be plausible including contaminants, electrode metal emission, and Bremsstrahlung, ion recombination, molecular or molecular ion band radiation, and instrument artifacts involving radicals and energetic ions reacting at the charge-coupled device and H2 re-radiation at the detector chamber. Moreover, predicted selective extraordinarily high-kinetic energy H was observed by the corresponding Doppler broadening of the Balmer α line.


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