Peculiarities of stress corrosion fracture of sensitized and neutron irradiated chromium-nickel austenitic steel

The results of SEM studies of fracture surfaces for the 12Cr18Ni9 austenitic steel ruptured under a fixedtensile load in FeCl3 water solutionand in air are presented. The samples of austenized, sensitized at 650° and irradiated with neutrons (to 1020n/cm2) steel were examined. It was shown thatirradiation hardening and sensitizing annealing increased the susceptibility of steel to intergranular cracking in corrosive solution. Structural features of formation of the strain-induced α’-martensite and its reinforcing effect on fracture in various environments are discussed.

Dryopteris Lijianxiuii (Dryopteridaceae), a New Species From China

Dryopteris lijianxiuii X. J. Li, a new species of Dryopteris Adans. from Shandong, China, is described and illustrated. It is closer to D. lacera (Thunb.) O. Kuntze for its morphological and palynological characters of LM and SEM studies but differs by a number of characters, such as, the leaves rectangular roundlanceolate, apex acuminate, and without narrow sharply; sori ornamented in the upper or middle part of 1-3 pairs of pinnaes at the base of the leaf, and densely covered with the upper and middle pinnaes back; spore perispore with tuberculiform-rugulate protrusions, and surfaces with melting ice and snow ornamentation. The sp. nov. is described with LM and SEM characters of spore and fronds, compared with that of D. lacera (Thunb.) O. Kuntze and provided with photographs. Bangladesh J. Bot. 50(3): 747-753, 2021 (September) Special

Post-thermal properties of Portland cement concrete made with copper slag as fine aggregates

Purpose The purpose of this paper is to investigate the effect of elevated temperature on mechanical and physical properties of concrete specimens obtained by substituting the river sand with copper slag (CS) at proportions of 25%, 50%, 75% and 100%. The specimens were heated in an electric furnace up to 100, 200, 300, 400, 500 and 600 C and kept at these temperatures for 2 h duration. After the specimens were cooled in the furnace, mass loss, ultrasonic pulse velocity (UPV), compressive strength, split tensile strength (STS), flexural strength (FS) and modulus of elasticity (MOE) values were determined. No spalling occurred in the specimens after subjected to elevated temperature. The surface cracks were observed only in specimens exposed to 600 C. The maximum reduction in compressive strength and STS at 600C is 50.3% and 36.39% for referral mix (NC), 18% and 16% for specimens with 100% CS (MCS4). The reduction in MOE of specimens is observed to be high as copper slag content increases with increasing temperature. Scanning electron microscopy (SEM) studies are carried out to examine the changes in micro-structures of specimens after exposed to elevated temperatures. Design/methodology/approach After casting of concrete specimens, it is cured for 28 days. After attainment of 28 days age, the concrete specimens is taken out from the curing tank and allowed to dry for 2 days to remove any moisture content in the specimens to prevent explosive spalling during the time of heating. The prepared concrete specimen is subjected to temperatures of 100°C, 200°C, 300°C, 400°C, 500°C and 600°C up to 2 h duration. The physical test, mechanical test and SEM studies are carried out after cooling of specimens to room temperature (RT). The quality of concrete specimens is measured by conducting UPV test after cooling to RT. Findings The post-thermal strength properties of concrete specimens with copper slag contents are higher than referral mix concrete. The reduction of MOE of concrete specimens is more with incremental in copper slag content with increase in temperatures. Furthermore, the quality of concrete specimens is ranging from “good to medium” up to 500C temperatures based on UPV test. Originality/value In this research work, the natural sand is fully replaced with copper slag materials in the concrete mixes. The post-thermal strength properties like residual compressive strength, residual STS, residual FS and residual MOE is higher than referral mix after subjected to elevated temperature conditions. Higher density and toughness properties of copper slag materials will contribute to concrete strength. The effect of elevated temperature is more on MOE of concrete specimens having higher copper slag contents when comparing to specimens compressive strength.