Cocrystallization and Phase Segregation of Polyethylene Blends between the D and H Species. 7. Time-Resolved Synchrotron-Source Small-Angle X-ray Scattering Measurements for Studying the Isothermal Crystallization Kinetics: Comparison with the FTIR Data

1995 ◽  
Vol 28 (25) ◽  
pp. 8477-8483 ◽  
Author(s):  
Kohji Tashiro ◽  
Kouji Imanishi ◽  
Yoshinobu Izumi ◽  
Masamichi Kobayashi ◽  
Katsumi Kobayashi ◽  
...  
Keyword(s):  
Small Angle ◽  
Isothermal Crystallization ◽  
Phase Segregation ◽  
Time Resolved ◽  
Synchrotron Source ◽  
Isothermal Crystallization Kinetics ◽  
X Ray ◽  
Polyethylene Blends ◽  
X Ray Scattering ◽  
Scattering Measurements

Time-resolved isothermal crystallization of absorbable PGA-co-PLA copolymer by synchrotron small-angle X-ray scattering and wide-angle X-ray diffraction

Polymer ◽  
2001 ◽  
Vol 42 (21) ◽  
pp. 8965-8973 ◽  
Author(s):  
Zhi-Gang Wang ◽  
Xuehui Wang ◽  
Benjamin S. Hsiao ◽  
Saša Andjelić ◽  
Dennis Jamiolkowski ◽  
...  
Keyword(s):  
Small Angle ◽  
Isothermal Crystallization ◽  
Wide Angle ◽  
X Ray Diffraction ◽  
Time Resolved ◽  
X Ray ◽  
X Ray Scattering ◽  
Ray Scattering

Time-resolved small-angle x-ray scattering measurements of a polymer bicontinuous microemulsion structure factor under shear

2002 ◽  
Vol 66 (4) ◽  
Author(s):  
Franklin E. Caputo ◽  
Wesley R. Burghardt ◽  
Kasiraman Krishnan ◽  
Frank S. Bates ◽  
Timothy P. Lodge
Keyword(s):  
Small Angle ◽  
Structure Factor ◽  
Time Resolved ◽  
X Ray ◽  
X Ray Scattering ◽  
Bicontinuous Microemulsion ◽  
Scattering Measurements ◽  
Ray Scattering

First performance assessment of the small-angle X-ray scattering beamline at ELETTRA

1998 ◽  
Vol 5 (3) ◽  
pp. 506-508 ◽  
Author(s):  
H. Amenitsch ◽  
M. Rappolt ◽  
M. Kriechbaum ◽  
H. Mio ◽  
P. Laggner ◽  
...  
Keyword(s):  
Small Angle ◽  
Wide Angle ◽  
Fibrous Materials ◽  
Time Resolved ◽  
X Ray ◽  
X Ray Scattering ◽  
Angle Scattering ◽  
Scattering Measurements ◽  
Double Focusing ◽  
Ray Scattering

The double-focusing high-flux wiggler beamline dedicated to small-angle X-ray scattering (SAXS) and wide-angle X-ray scattering (WAXS) at ELETTRA has gone into user operation recently. It has been designed specifically for time-resolved studies of non-crystalline and fibrous materials in the submillisecond time scale, and has been optimized for small-angle scattering measurements. An overview of the beamline status and of some representative results, highlighting the performance of the SAXS beamline, are given.

The stopped-drop method: a novel setup for containment-free and time-resolved measurements

2016 ◽  
Vol 23 (2) ◽  
pp. 545-550 ◽  
Author(s):  
Andreas Schiener ◽  
Soenke Seifert ◽  
Andreas Magerl
Keyword(s):  
Time Evolution ◽  
Small Angle ◽  
Dead Time ◽  
Hanging Drop ◽  
Time Resolved ◽  
Synchrotron Source ◽  
X Ray ◽  
X Ray Scattering ◽  
Laboratory Source ◽  
Scattering Study

A novel setup for containment-free time-resolved experiments at a free-hanging drop is reported. Within a dead-time of 100 ms a drop of mixed reactant solutions is formed and the time evolution of a reaction can be followed from thereon by various techniques. As an example, a small-angle X-ray scattering study on the formation mechanism of EDTA-stabilized CdS both at a synchrotron and a laboratory X-ray source is presented here. While the evolution can be followed with one drop only at a synchrotron source, a stroboscopic mode with many drops is preferable for the laboratory source.

Correlation of nanostructural parameters and macromechanical behaviour of hyperbranched-modified polypropylene using time-resolved small-angle X-ray scattering measurements

2012 ◽  
Vol 62 (7) ◽  
pp. 1101-1111 ◽  
Author(s):  
Morteza Ganjaee Sari ◽  
Norbert Stribeck ◽  
Siamak Moradian ◽  
Ahmad Zeinolebadi ◽  
Saeed Bastani ◽  
...  
Keyword(s):  
Small Angle ◽  
Time Resolved ◽  
X Ray ◽  
X Ray Scattering ◽  
Scattering Measurements ◽  
Ray Scattering

Performance and First Results of the ELETTRA High-Flux Beamline for Small-Angle X-ray Scattering

1997 ◽  
Vol 30 (5) ◽  
pp. 872-876 ◽  
Author(s):  
H. Amenitsch ◽  
S. Bernstorff ◽  
M. Kriechbaum ◽  
D. Lombardo ◽  
H. Mio ◽  
...  
Keyword(s):  
Small Angle ◽  
Small Angle Scattering ◽  
Design Parameters ◽  
High Flux ◽  
Time Resolved ◽  
X Ray ◽  
X Ray Scattering ◽  
Angle Scattering ◽  
Scattering Measurements ◽  
Ray Scattering

A new beamline for small-angle X-ray scattering (SAXS) has recently been constructed and is presently under final commissioning at the 2 GeV storage ring ELETTRA. It has been designed specifically for time-resolved studies of non-crystalline and fibrous materials and has been optimized for small-angle scattering measurements. The beamline operates with a SAXS resolution between 10 and about 1400 Å in d spacing (at 8 keV) and has been optimized with respect to high flux at the sample [of the order of 1013 photons s−1 for 8 keV photons (2 GeV, 400 mA)]. Soon it will be possible to perform simultaneously wide-angle diffraction measurements in the d-spacing range 1.2–8 Å (at 8 keV). In order to allow time-resolved (resolution ~1 ms) small-angle scattering measurements, a high-power 57-pole wiggler is used as the beamline source. From its beam, one of three discrete energies, 5.4, 8 and 16 keV, can be selected with a double-crystal monochromator, which contains three pairs of asymmetrically cut plane Si(111) crystals. Downstream, the beam is focused horizontally and vertically by a toroidal mirror. Commissioning tests of this new SAXS beamline showed that all design parameters have been realized.

Sign in / Sign up

Export Citation Format

Share Document