scholarly journals Synthesis and characterization of composite polyaniline as hydrogen gas detector

2017 ◽  
Vol 13 (4) ◽  
pp. 559-562 ◽  
Author(s):  
Alister Genndi Willis ◽  
Saharudin Haron

Composite polymer consisting polyaniline (PANI) and zinc oxide (ZnO) were synthesized via oxidative polymerization of aniline. The composite PANI thin films were characterized by FTIR spectroscopy and their optical properties towards hydrogen gas were investigated using UV-vis spectroscopy. The FTIR spectra obtained verified the synthesis PANI/ZnO composite. From the experimental results, it was found that with increasing zinc oxide content in the composite cause the transmittance to decrease. The transmittance of the thin films slightly increased after exposed to hydrogen gas. PANI-ZnO (10%w.t.) exhibited best response compared to other composition with the highest transmittance peak difference of 11.4%. 

2019 ◽  
Vol 90 ◽  
pp. 01008
Author(s):  
Willis Alister G. ◽  
Saharudin Haron

A composite polymer consisting of polyaniline (PANI) was synthesised via oxidative polymerisation by varying concentrations of transitional metal oxides and the presence of a hydrogen dissociation catalyst, palladium (Pd). The metal oxides chosen for this study were tungsten oxide (WO3) and zinc oxide (ZnO). The composite polymer samples were characterised using Fourier transform infrared (FTIR) spectroscopy where ultraviolet-visible (UV-Vis) spectroscopy was used to observe the optical changes of the thin films due to exposure to hydrogen. The FTIR spectra obtained confirmed the synthesis of PANI composite. Based on the UV-VIS analysis, PANI-ZnO composite polymer showed the highest difference in peak intensity before and after exposure to hydrogen with 11.4% difference.


2020 ◽  
Vol 9 (5) ◽  
pp. 10624-10634
Author(s):  
Siti Nor Aliffah Mustaffa ◽  
Nurul Assikin Ariffin ◽  
Ahmed Lateef Khalaf ◽  
Mohd. Hanif Yaacob ◽  
Nizam Tamchek ◽  
...  

2018 ◽  
Vol 5 (10) ◽  
pp. 20904-20911
Author(s):  
Sachin S Bharadwaj ◽  
B.W. Shivaraj ◽  
H.N. Narasimha Murthy ◽  
M Krishna ◽  
Manjush Ganiger ◽  
...  

2005 ◽  
Vol 21 (06) ◽  
pp. 612-615
Author(s):  
CHEN Zhi-gang ◽  
◽  
TANG Yi-wen ◽  
ZHANG Li-sha ◽  
CHEN Zheng-hua ◽  
...  

2012 ◽  
Vol 121 (1) ◽  
pp. 217-220 ◽  
Author(s):  
M.S. Kim ◽  
K.G. Yim ◽  
S. Kim ◽  
G. Nam ◽  
D.Y. Lee ◽  
...  

1998 ◽  
Vol 547 ◽  
Author(s):  
A. Rougier ◽  
N. Naghavi ◽  
C. Marcel ◽  
F. Portemer ◽  
L. Dupont ◽  
...  

AbstractThin films of indium zinc oxide so called IZO were prepared with pulsed laser deposition. It was found that the crystalline structure, the composition and the morphology of the films as well as the optical and electrical properties were quite sensitive to the deposition conditions namely to the temperature and oxygen pressure. The crystallinity of the ZnkIn2O3+k (k from 1 to 5) thin films increases as the substrate temperature increases. An average transmittance of 85 % in the visible region was obtained for any k values. Optical measurements show a continuous decrease of the band gap as the zinc amount increases. The highest conductivity reported is for the ZnIn2O4, thin films deposited at 300 °C (σ = 1.2 103 S/cm). Increasing the amount of Zn (i.e. k value) was found to result in a conductivity decrease. Finally, a good correlation between the electric mobility and the optical mobility is obtained.


2008 ◽  
Vol 202 (22-23) ◽  
pp. 5467-5470 ◽  
Author(s):  
Norihiro Sakai ◽  
Yoshihiro Umeda ◽  
Fumiaki Mitsugi ◽  
Tomoaki Ikegami

2002 ◽  
Vol 14 (1) ◽  
pp. 116-121 ◽  
Author(s):  
Antonino Gulino ◽  
Ignazio Fragala
Keyword(s):  

Sign in / Sign up

Export Citation Format

Share Document