C/SiC Composites by Electrophoretical Infiltration

Author(s):  
Rosemarie Dittrich ◽  
Eberhard Mu¨ller ◽  
Uta Popp

Due to its high thermodynamical stability carbon fiber reinforced silicon carbide is an interesting material for high temperature applications. Studies are described to find an innovative route for fabricating C/SiC composites by using electrophoresis for infiltrating carbon fiber mats with non-aqueous suspensions of mixtures of silicon carbide powders, stabilizers and sintering aids. The suitability of nano-scaled and submicron powders is discussed. Based on investigations of the interaction between the SiC particle surfaces and the carbon fibers essential technological parameters of the electrophoretic infiltration are defined. The fabrication of C/SiC composites by lamination of single infiltrated fiber mats and a subsequent thermal process is demonstrated.

2011 ◽  
Vol 462-463 ◽  
pp. 1-6 ◽  
Author(s):  
Tao Suo ◽  
Yu Long Li ◽  
Ming Shuang Liu

As Carbon-fiber-reinforced SiC-matrix (C/SiC) composites are widely used in high-temperature structural applications, its mechanical behavior at high temperature is important for the reliability of structures. In this paper, mechanical behavior of a kind of 2D C/SiC composite was investigated at temperatures ranging from room temperature (20C) to 600C under quasi-static and dynamic uniaxial compression. The results show the composite has excellent high temperature mechanical properties at the tested temperature range. Catastrophic brittle failure is not observed for the specimens tested at different strain rates. The compressive strength of the composite deceases only 10% at 600C if compared with that at room temperature. It is proposed that the decrease of compressive strength of the 2D C/SiC composite at high temperature is influenced mainly by release of thermal residual stresses in the reinforced carbon fiber and silicon carbon matrix and oxidation of the composite in high temperature atmosphere.


2018 ◽  
Vol 935 ◽  
pp. 5-10 ◽  
Author(s):  
Azamat L. Slonov ◽  
Azamat A. Zhansitov ◽  
Elena V. Rzhevskaya ◽  
Diana M. Khakulova ◽  
Elina V. Khakyasheva ◽  
...  

The effect of the length and concentration of carbon fibers on the rheological, mechanical and thermal properties of high-temperature thermoplastics – polyphenylene sulfone was investigated. As fillers fibers with a length of 0.2 and 3 mm are used.


1998 ◽  
Vol 4 (S2) ◽  
pp. 568-569
Author(s):  
K. A. Appiah ◽  
Z. L. Wang ◽  
W. J. Lackey

Silicon carbide composites are known for high-temperature strength retention, creep resistance, high elastic modulus and light weight. Laminated matrix composites (LMC's) with a matrix of alternating layers of silicon carbide (SiC) and carbon (C) with carbon fiber reinforcements possess added toughness in addition to the desirable properties of SiC composites mentioned above. The improved toughness results from both the laminated matrix, which offers a tortuous path to crack propagation, and the energy expended in fiber debonding during fracture. Microstructural analyses of LMC's are necessary to help the processing effort to achieve structures with the desired properties. In this work, a preliminary examination of the microstructure of the laminated matrix composite is undertaken using TEM.Specimens for TEM examination were prepared by cutting slices from a bulk sample of ∼ 1 mm thickness with a low-speed diamond saw. The slices were then ground to no less than 200 μm thickness to prevent the slices from breaking.


2006 ◽  
Vol 11-12 ◽  
pp. 81-84 ◽  
Author(s):  
Dong Lin Zhao ◽  
Hong Feng Yin ◽  
Fa Luo ◽  
Wan Cheng Zhou

Three dimensional textile carbon fiber reinforced silicon carbide (3D textile C/SiC) composites with pyrolytic carbon interfacial layer were fabricated by chemical vapor infiltration. The microstructure and mechanical property of 3D textile C/SiC composites were investigated. A thin pyrolysis carbon layer (0.2 ± μm) was firstly deposited on the surface of carbon fiber as the interfacial layer with C3H6 at 850°C and 0.1 MPa. Methyltrichlorosilane (CH3SiCl3 or MTS) was used for the deposition of the silicon carbide matrix. The conditions used for SiC deposition were 1100°C, a hydrogen to MTS ratio of 10 and a pressure of 0.1 MPa. The density of the composites was 2.1 g cm-3. The flexural strength of the 3D textile C/SiC composites was 438 MPa. The 3D textile C/SiC composites with pyrolytic carbon interfacial layer exhibit good mechanical properties and a typical failure behavior involving fibers pull-out and brittle fracture of sub-bundle. The real part (ε′) and imaginary part (ε″) of the complex permittivity of the 3D-C/SiC composites are 51.53-52.44 and 41.18-42.08 respectively in the frequency range from 8.2 to 12.4 GHz. The 3D-C/SiC composites would be a good candidate for microwave absorber.


2019 ◽  
Vol 967 ◽  
pp. 267-273
Author(s):  
Subaer ◽  
Abdul Haris ◽  
Noor Afifah Kharisma ◽  
Nur Akifah ◽  
Risna Zulwiyati

The main objective of this study is to investigate the thermo-mechanical properties of composite made from geopolymer/carbon fiber/TiO2 NPs. The composite was fabricated from geopolymer based on metakaolin added with carbon fibers as reinforcement and TiO2 NPs as self-cleaning agent. The thermal properties of the composite was examined by subjecting the samples to temperature up to 750OC for 4 hours. The mechanical properties of the resulting materials were measured by using flexural and tensile strength measurements. The experimental results showed that the compsite exhibited high temperature resistance and the addition of carbon fiber were increase the flexural as well as the tensile strength of the composite.


2007 ◽  
Vol 336-338 ◽  
pp. 1291-1293
Author(s):  
Xin Gui Zhou ◽  
Chang Cheng Zhou ◽  
Chang Rui Zhang ◽  
Ying Bin Cao ◽  
Shi Qin Zou

3D braided carbon fiber reinforced silicon carbide (3D-Cf/SiC) composites were fabricated by precursor infiltration and pyrolysis(PIP), with carbon coatings prepared by chemical vapor deposition (CVD) before PIP. The effect of 1873K heat treatment on the mechanical properties of Cf/SiC composites were investigated. The results showed that heat treatment before PIP can increase the density of composites and lead to excellent properties of Cf/SiC composites. The flexual strength of the Cf/SiC composites with one cycle of 1873 K heat treatment reached 571 MPa, shear strength 51 MPa, and fracture toughness 18 MPa⋅m1/2.


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