Determination of methane yield of cellulose using different experimental setups

2014 ◽  
Vol 70 (4) ◽  
pp. 599-604 ◽  
Author(s):  
Bing Wang ◽  
Ivo Achu Nges ◽  
Mihaela Nistor ◽  
Jing Liu
Keyword(s):  
Water Column ◽  
Test System ◽  
Methane Yield ◽  
Biochemical Methane Potential ◽  
Methane Potential ◽  
Bmp Test ◽  
Potential Test

In this work, biochemical methane potential (BMP) tests with cellulose as a model substrate were performed with the aid of three manually operated or conventional experimental setups (based on manometer, water column and gas bag) and one automated apparatus specially designed for analysis of BMP. The methane yields were 340 ± 18, 354 ± 13, 345 ± 15 and 366 ± 5 ml CH4/g VS obtained from experimental setups with manometer, water column, gas bag, and automatic methane potential test system, which corresponded to a biodegradability of 82, 85, 83 and 88% respectively. The results demonstrated that the methane yields of cellulose obtained from conventional and automatic experimental setups were comparable; however, the methane yield obtained from the automated apparatus showed greater precision. Moreover, conventional setups for the BMP test were more time- and labour-intensive compared with the automated apparatus.

Anaerobic digestion of sunflower oil cake: a current overview

2013 ◽  
Vol 67 (2) ◽  
pp. 410-417 ◽  
Author(s):  
M. A. De la Rubia ◽  
V. Fernández-Cegrí ◽  
F. Raposo ◽  
R. Borja
Keyword(s):  
Anaerobic Digestion ◽  
Sunflower Oil ◽  
Physical Structure ◽  
Methane Yield ◽  
Organic Loading Rate ◽  
Biochemical Methane Potential ◽  
In Series ◽  
Methane Potential ◽  
Bmp Test ◽  
Sunflower Oil Cake

Due to the chemical and physical structure of a lignocellulosic biomass, its anaerobic digestion (AD) is a slow and difficult process. In this paper, the results obtained from a batch biochemical methane potential (BMP) test and fed-batch mesophilic AD assays of sunflower oil cake (SuOC) are presented. Taking into account the low digestibility shown during one-stage experiments the methane yield decreased considerably after increasing the organic loading rate (OLR) from 2 to 3 g VS L−1 d−1, SuOC was subjected to a two-stage AD process (hydrolytic-acidogenic and methanogenic stages), in two separate reactors operating in series where the methanogenic stage became acidified (with >1,600 mg acetic acid L−1) at an OLR as low as 2 g VS L−1 d−1. More recently, BMP assays were carried out after mechanical, thermal, and ultrasonic pre-treatments to determine the best option on the basis of the methane yield obtained.

scholarly journals Optimisation of C:N Ratio for Co-Digested Processed Industrial Food Waste and Sewage Sludge Using the BMP Test

2011 ◽  
Vol 9 (1) ◽  
Author(s):  
Zuhaib Siddiqui ◽  
N.J. Horan ◽  
Kofi Anaman
Keyword(s):  
Sewage Sludge ◽  
Food Waste ◽  
Biogas Production ◽  
C:N Ratio ◽  
Methane Yield ◽  
Biochemical Methane Potential ◽  
Volatile Solids ◽  
Methane Potential ◽  
Biomethane Production ◽  
Bmp Test

Biomethane production from processed industrial food waste (IFW) in admixture with sewage sludge (primary and waste activated sludge: PS and WAS) was evaluated at a range of C:N ratios using a standard biochemical methane potential (BMP) test. IFW alone had a C:N of 30 whereas for WAS it was 5.4 and thus the C:N ratio of the blends fell in that range. Increasing the IFW content in mix improves the methane potential by increasing both the cumulative biogas production and the rate of methane production. Optimum methane yield 239 mL/g VSremoved occurred at a C:N ratio of 15 which was achieved with a blend containing 11 percent (w/w) IFW. As the fraction of IFW in the blend increased, volatile solids (VS) destruction was increased and this led to a reduction in methane yield and amount of production. The highest destruction of volatile solids of 93 percent was achieved at C:N of 20 followed by C:N 30 and 15. A shortened BMP test is adequate for evaluating optimum admixtures.

scholarly journals Chemical pre-treatments on oil palm empty fruit bunches: Impacts on characteristics and methane potential

2021 ◽  
Vol 924 (1) ◽  
pp. 012071
Author(s):  
N A Rohma ◽  
S Suhartini ◽  
I Nurika
Keyword(s):  
Lignocellulosic Biomass ◽  
Oil Palm ◽  
Biogas Production ◽  
Lignin Content ◽  
Test System ◽  
Biochemical Methane Potential ◽  
Empty Fruit Bunches ◽  
Methane Potential ◽  
Pre Treatment ◽  
Bmp Test

Abstract Production of biogas from lignocellulosic biomass by anaerobic digestion (AD) has attracted much interest. Oil palm empty fruit bunches (OPEFB), one of lignocellulosic biomass, is highly abundant in Indonesia and has potential as feedstock for bioenergy production such as biogas or methane. Yet, pre-treatments are needed to improve biogas production due to its complex crystalline structures. Chemical pre-treatments with acid or alkaline solution were reported to increase cellulose or highly reduce the lignin content of OPEFB. This study aimed to evaluate the effect of acid and alkaline pre-treatments on the characteristics of OPEFB and methane potential. The acid pre-treatment experimental design was used factor of H2SO4 concentration (1, 1.3, and 1.6 (%v/v)) and NaOH concentration (1.8, 2.8, and 3.8 (%w/v)). Methane potential evaluation was carried out using the biochemical methane potential (BMP) test with the Automatic Methane Potential Test System (AMPTS) II under mesophilic condition (37°C), operated for 28 days. The results showed that both dilute acid and alkaline pre-treatment positively impact altering the characteristics of OPEFB, hence the specific methane potential. Alkaline pre-treatment with NaOH 3.8 (%w/v) gave the highest average SMP value of 0.161 ± 0.005 m3 CH4/kgVSadded.

scholarly journals Biomethane Potential Test: Influence of Inoculum and the Digestion System

2020 ◽  
Vol 10 (7) ◽  
pp. 2589 ◽  
Author(s):  
Benedikt Hülsemann ◽  
Lijun Zhou ◽  
Wolfgang Merkle ◽  
Juli Hassa ◽  
Joachim Müller ◽  
...  
Keyword(s):  
Laboratory Tests ◽  
Methane Yield ◽  
Biochemical Methane Potential ◽  
Measurement Variability ◽  
Biogas Yield ◽  
Yield Test ◽  
Biogas Plants ◽  
Methane Potential ◽  
Bmp Test

High precision of measurement of methane potential is important for the economic operation of biogas plants in the future. The biochemical methane potential (BMP) test based on the VDI 4630 protocol is the state-of-the-art method to determine the methane potential in Germany. The coefficient of variation (CV) of methane yield was >10% in several previous inter-laboratory tests. The aim of this work was to investigate the effects of inoculum and the digestion system on the measurement variability. Methane yield and methane percentage of five substrates were investigated in a Hohenheim biogas yield test (D-HBT) by using five inocula, which were used several times in inter- laboratory tests. The same substrates and inocula were also tested in other digestion systems. To control the quality of the inocula, the effect of adding trace elements (TE) and the microbial community was investigated. Adding TE had no influence for the selected, well- supplied inocula and the community composition depended on the source of the inocula. The CV of the specific methane yield was <4.8% by using different inocula in one D-HBT (D-HBT1) and <12.8% by using different digestion systems compared to D-HBT1. Incubation time between 7 and 14 days resulted in a deviation in CV of <4.8%.

scholarly journals Methane Potential from the Digestion of Food Waste in a Batch Reactor

2018 ◽  
Vol 7 (3.23) ◽  
pp. 36 ◽  
Author(s):  
Roslinda Seswoya ◽  
Ahmad Tarmizi Abdul Karim ◽  
Nur Aiza Darnak ◽  
Muhammad Fahmi Abd Rahman
Keyword(s):  
Food Waste ◽  
Methane Production ◽  
Yield Curve ◽  
Batch Reactor ◽  
Laboratory Data ◽  
Test System ◽  
Methane Yield ◽  
Lag Phase ◽  
Methane Potential ◽  
Bmp Test

The anaerobic digestibility of a targeted substrate, measured as methane yield is conducted via biochemical methane potential (BMP). In this study, the batch BMP test was conducted using Automatic Methane Potential Test System (AMPTS II) for 25 days and focused on the methane production from the digestion of food waste (FW, in the form of raw and diluted) at inoculum to substrate ratio (I/S) ratio of 2:0 and under mesophilic temperature.  The results showed that solids (TS and VS) concentration reduced significantly due to the       dilution. The ultimate methane yields from the digestion of raw FW and diluted FW were 1891.91ml CH4/gVS and 1983.96 ml CH4/gVS respectively. This showed that the dilution significantly improved the methane yield. In addition, the lag phase of the methane yield curve for both BMP tests was less than one (1) day, showing the good biodegradability of FW. The kinetic methane production from laboratory data and Modified Gompertz modelling fitted well. However, the kinetic equation parameters such as Mo, Rm and l from the model were slightly lower based on the observation of the laboratory data. 

scholarly journals Evaluation of Biogas Production from the Co-Digestion of Municipal Food Waste and Wastewater Sludge at Refugee Camps Using an Automated Methane Potential Test System

Energies ◽  
2018 ◽  
Vol 12 (1) ◽  
pp. 32 ◽  
Author(s):  
Mohammad Al-Addous ◽  
Motasem N. Saidan ◽  
Mathhar Bdour ◽  
Mohammad Alnaief
Keyword(s):  
Food Waste ◽  
Organic Waste ◽  
Biogas Production ◽  
Test System ◽  
Wastewater Sludge ◽  
Methane Yield ◽  
Refugee Camps ◽  
Methane Potential ◽  
Municipal Food Waste ◽  
Potential Test

The potential benefits of the application of a circular economy—converting biomass at Za'atari Syrian refugee camps into energy—was investigated in this study. Representative organic waste and sludge samples were collected from the camp, mixed in different ratios, and analyzed in triplicate for potential biogas yield. Numerous calorific tests were also carried out. The tangential benefit of the co-digestion that was noticed was that it lowered the value of the total solid content in the mixture to the recommended values for wet digestion without the need for freshwater. To test the potential methane production, the automated methane potential test system (AMPTS) and the graduated tubes in the temperature-controlled climate room GB21 were utilized. Also, calorific values were determined for the organic waste and sludge on both a dry and a wet basis. The maximum biogas production from 100% organic waste and 100% sludge using AMPTS was 153 m3 ton-1 and 5.6 m3 ton-1, respectively. Methane yield reached its maximum at a Vs sub/ Vs inoculum range of 0.25–0.3. In contrast, the methane yield decreased when the Vs sub/ Vs inoculum exceeded 0.46. The optimum ratio of mixing of municipal food waste to sludge must be carefully selected to satisfy the demands of an energy production pilot plant and avoid the environmental issues associated with the sludge amount at wastewater treatment plants (WWTPs). A possible ratio to start with is 60–80% organic waste, which can produce 21–65 m3· biogas ton-1 fresh matter (FM). The co-digestion of organic waste and sludge can generate 38 Nm3/day of methane, which, in theory, can generate about 4 MW in remote refugee camps.

scholarly journals The Performance Evaluation on Co-Digestion of Domestic Sewage Sludge and Food Waste for Methane Yield and Kinetics Analysis

2021 ◽  
Vol 13 (3) ◽  
Author(s):  
Siti Mariam Sulaiman ◽  
◽  
Roslinda Seswoya ◽  
Keyword(s):  
Anaerobic Digestion ◽  
Sewage Sludge ◽  
Food Waste ◽  
Methane Production ◽  
Test System ◽  
Domestic Sewage ◽  
Methane Yield ◽  
Methane Potential ◽  
Methane Production Rate ◽  
Bmp Test

Sewage sludge and food waste; are organic wastes suitable for the anaerobic digestion. However, the digestion of sewage sludge and food waste as solely substrate is having a drawback in term of methane yield. Therefore, many researchers combined these two wastes as a co-substrate and used in co-digestion. This study focused to evaluate the anaerobic co-digestion of domestic sewage sludge (in form of primary and secondary sewage sludge) with food waste under mesophilic temperature in a batch assay. Two series of batch biochemical methane potential (BMP) test were conducted using the Automatic Methane Potential Test System (AMPTS II). Each set are labelled with BMP 1(PSS:FW) and BMP 2 (SSS:FW). The BMP tests were monitored automatically until the methane production is insignificant. Using the data observed in the laboratory, the kinetic paremeters were calculated. Also, the First-order and Modified Gompertz modeling were included to predict the anaerobic digestion performance. Finding showed that BMP 1(PSS:FW) have better performance with respect to the higher ultimate methane yield and methane production rate as compared to BMP 2 (SSS:FW). Besides, the kinetic parameters from laboratory work and modeling were slightly different. In which the kinetic paremetes from modelling is lesser. However, both modelling are well fitted to the experimental data with high correlation coefficient, R2 ranged from 0.993 to 0.997.

scholarly journals Biochemical Methane Potential of Cork Boiling Wastewater at Different Inoculum to Substrate Ratios

2021 ◽  
Vol 11 (7) ◽  
pp. 3064
Author(s):  
Roberta Mota-Panizio ◽  
Manuel Jesús Hermoso-Orzáez ◽  
Luis Carmo-Calado ◽  
Gonçalo Lourinho ◽  
Paulo Sérgio Duque de Brito
Keyword(s):  
Anaerobic Digestion ◽  
Biogas Production ◽  
Treatment Plant ◽  
Organic Substrates ◽  
Biochemical Methane Potential ◽  
Volatile Solids ◽  
Working Volume ◽  
Methane Potential ◽  
Bmp Test ◽  
Cork Industry

The present study evaluates the digestion of cork boiling wastewater (CBW) through a biochemical methane potential (BMP) test. BMP assays were carried out with a working volume of 600 mL at a constant mesophilic temperature (35 °C). The experiment bottles contained CBW and inoculum (digested sludge from a wastewater treatment plant (WWTP)), with a ratio of inoculum/substrate (Ino/CBW) of 1:1 and 2:1 on the basis of volatile solids (VSs); the codigestion with food waste (FW) had a ratio of 2/0.7:0.3 (Ino/CBW:FW) and the codigestion with cow manure (CM) had a ratio of 2/0.5:0.5 (Ino/CBW:CM). Biogas and methane production was proportional to the inoculum substrate ratio (ISR) used. BMP tests have proved to be valuable for inferring the adequacy of anaerobic digestion to treat wastewater from the cork industry. The results indicate that the biomethane potential of CBWs for Ino/CBW ratios 1:1 and 2:1 is very low compared to other organic substrates. For the codigestion tests, the test with the Ino/CBW:CM ratio of 2/0.7:0.3 showed better biomethane yields, being in the expected values. This demonstrated that it is possible to perform the anaerobic digestion (AD) of CBW using a cosubstrate to increase biogas production and biomethane and to improve the quality of the final digestate.

scholarly journals Optimizing anaerobic co-digestion of goat manure and cotton gin trash using biochemical methane potential (BMP) test and mathematical modeling

2021 ◽  
Vol 3 (8) ◽  
Author(s):  
Harjinder Kaur ◽  
Raghava R. Kommalapati
Keyword(s):  
Liquid Fraction ◽  
Gompertz Model ◽  
Biochemical Methane Potential ◽  
Methane Potential ◽  
Mathematical Equations ◽  
Goat Manure ◽  
Bmp Test ◽  
Batch Bioreactors ◽  
Modified Gompertz Model ◽  
Cotton Gin

AbstractAnaerobic co-digestion is widely adopted to enhance process efficacy by balancing the C/N ratio of the feedstock while converting organic wastes to biomethane. Goat manure (GM) and cotton gin trash (CGT) were anaerobically co-digested in triplicate batch bioreactors. The process was optimized and evaluated utilizing mathematical equations. The liquid fraction of the digestate was analyzed for nitrate and phosphate. The co-digestions with 10 and 20% CGT having the C/N ratios of 17.7 and 19.8 yielded the highest and statistically similar 261.4 ± 4.8 and 262.6 ± 4.2 mL/gvs biomethane, respectively. The biodegradability (BD) of GM and CGT was 94.5 ± 2.7 and 37.6 ± 0.8%, respectively. The BD decreased proportionally with an increase in CGT percentage. The co-digestion having 10% CGT yielded 80–90% of biomethane in 26–39 d. The modified Gompertz model-predicted and experimental biomethane values were similar. The highest synergistic effect index of 15.6 ± 4.7% was observed in GM/CGT; 30:70 co-digestion. The concentration of nitrate and phosphate was lower in the liquid fraction of digestate than the feedstocks, indicating that these nutrients stay in the solid fraction. The results provide important insights in agro-waste management, further studies determining the effects of effluent application on plants need to be conducted.

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