scholarly journals Mesoporous Silica MCM-41 as a Carriers Material for Nystatine Drug in Delivery System

2019 ◽  
Vol 15 (2) ◽  
pp. 34-43 ◽  
Author(s):  
Talib M. Albayati ◽  
Ali M. AlKafajy
Keyword(s):  
Historical Data ◽  
Drug Loading ◽  
Sol Gel ◽  
Weibull Model ◽  
Gravimetric Analysis ◽  
X Ray Diffraction ◽  
Combine Process ◽  
X Ray ◽  
Gel Technique ◽  
Mcm 41

In the present study, MCM-41 was synthesis as a carrier for poorly drugs soluble in water, by the sol-gel technique. Textural and chemical characterizations of MCM-41 were carried out by X-ray diffraction (XRD), Fourier transform infrared (FTIR), scanning electron microscope (SEM), and thermal gravimetric analysis (TGA). The experimental results were analyzed mesoporous carriers MCM-41. With maximum drug loading efficiency in MCM-41 determined to be 90.74%. The NYS released was prudently studied in simulated body fluid (SBF) pH 7.4 and the results proved that the release of NYS from MCM-41 was (87.79%) after 18 hr. The data of NYS released was found to be submitted a Weibull model with a correlation coefficient of (0.995). The Historical data experimental design facilitated the formulation and optimization of sustained discover the optimal formulation to loading drug, combine process variables, mixture components and categorical factors in one design.

scholarly journals Calcination Effect on Structural Trasformation of Barium Titanite Ferroelectric Ceramic by Sol-Gel Method

2019 ◽  
Vol 9 (1) ◽  
pp. 5893-5896
Keyword(s):  
Glacial Acetic Acid ◽  
Sol Gel ◽  
Ferroelectric Ceramic ◽  
Tetrabutyl Titanate ◽  
Chemical Modifier ◽  
Barium Acetate ◽  
X Ray Diffraction ◽  
X Ray ◽  
Gel Technique ◽  
Scanning Electron

High purity barium titanate BaTiO3 was successfully synthesized by using the sol-gel technique. Barium acetate Ba(CH3COO)2 and tetrabutyl titanate, Ti(C4H9O)4 was dissolved moderately in the solvent of glacial acetic acid and ethanol was added as the chemical modifier. The synthesized BaTiO3 nanoparticle was calcined at the temperature range of 700 ºC to 1100 ºC. The powders were further characterized by X-ray diffraction and scanning electron microscopy (SEM). Fined BaTiO3 powders result indicates the phase of tetragonal structures and high crystallites of BaTiO3. It was observed that the crystallinity and particle size of BaTiO3 is greatly influenced by the calcination temperature.

scholarly journals Synthesis Photocatalytic and Antibacterial Activities of Nickle Doped Tio2 Nanoparticles

2018 ◽  
Vol 34 (6) ◽  
pp. 3140-3144
Author(s):  
Ritu Vershney ◽  
Komal Chelaramani ◽  
Arpan Bhardwaj ◽  
Nayma Siddiqui ◽  
Suresh Kumar Verma
Keyword(s):  
Photocatalytic Degradation ◽  
Tio2 Nanoparticles ◽  
Sol Gel ◽  
Antibacterial Activities ◽  
X Ray Diffraction ◽  
Zone Of Inhibition ◽  
Time Duration ◽  
X Ray ◽  
Gel Technique ◽  
Doped Titania

The synthesis of Ni doped titania (TiO2) nanoparticles were achieved via simple novel sol gel technique, in which Titanium-n-butoxide and NiCl2 were taken as precursors. Effect of different wt% of dopant in TiO2 was studied on photocatalytic degradation of Aniline blue and Toluidine Blue. The study suggested the increased photocatalytic degradation with increased time duration. The synthesized samples were analyzed by surface electron microscopy (SEM) and X-ray diffraction studies. The antibacterial activity was investigated against Gram-positive Staphylococcus aureus bacteriae. Studies revealed that on increasing the dopant concentration, the diameter of zone of inhibition also increased upto 1.5 wt%.

Fabrication of Porous LSCF-SDC Carbonates Composite Cathode for Solid Oxide Fuel Cell (SOFC) Applications

2011 ◽  
Vol 471-472 ◽  
pp. 179-184 ◽  
Author(s):  
Raharjo Jarot ◽  
Andanastuti Muchtar ◽  
Wan Ramli Wan Daud ◽  
Norhamidi Muhamad ◽  
Edy Herianto Majlan
Keyword(s):  
Thermal Expansion ◽  
Sol Gel ◽  
Composite Cathode ◽  
X Ray Diffraction ◽  
X Ray ◽  
Structure Morphology ◽  
Composite Cathodes ◽  
Gel Technique ◽  
Optimum Porosity ◽  
Cold Pressed

Composite cathodes made of perovskite La0.6Sr0.4Co0.2Fe0.8O3 (LSCF) and SDC carbonates (SDC-(Li/Na)2CO3) were investigated in relation to their structure, morphology, thermal expansion coefficient and porosity. As a first step, the LSCF powder was prepared by sol-gel technique. This was followed by the preparation of the LSCF-SDC carbonates composite cathode by mixing the LSCF with SDC-(Li/Na)2CO3 electrolyte via solid state reaction in various compositions, i.e. 30, 40 and 50 wt.%, namely 70LSCF-30SDC7030, 60LSCF-40SDC7030 and 50LSCF-50SDC7030, respectively. The powder mixtures were then calcined at 680oC. The resultant powder was fine with surface area of about 3.39-7.42 m2/g and particle size of 0.56-0.66µm. The powder consists of two distinct phases, i.e. LSCF and SDC-(Li/Na)2CO3 as confirmed with x-ray diffraction. The microstructures were observed under scanning electron microscopy (SEM). Increasing the amount of the SDC-(Li/Na)2CO3 electrolyte in the composite cathode was found to bring the thermal expansion of the cathode closer to that of the electrolyte. The cathode pellets were later compacted at different pressures (27, 32 and 37 MPa) and sintered at 600oC. The optimum porosity (20.99-24.98%) was achieved for samples with SDC-(Li/Na)2CO3 content of 30-50% sintered at 600oC and cold pressed at 37 MPa.

scholarly journals ZnFe2O4-TiO2Nanoparticles within Mesoporous MCM-41

2012 ◽  
Vol 2012 ◽  
pp. 1-8 ◽  
Author(s):  
Aidong Tang ◽  
Yuehua Deng ◽  
Jiao Jin ◽  
Huaming Yang
Keyword(s):  
Sol Gel ◽  
Rutile Phase ◽  
Band Gap Energy ◽  
Molar Ratio ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Agglomeration Of Nanoparticles ◽  
Adsorption Desorption ◽  
Mcm 41

A novel nanocomposite ZnFe2O4-TiO2/MCM-41 (ZTM) was synthesized by a sol-gel method and characterized through X-ray diffraction (XRD), high-resolution transmission electron microscopy (HRTEM), N2adsorption-desorption, Raman spectroscopy, and ultraviolet visible (UV-vis) spectrophotometry. The results confirmed the incorporation of ZnFe2O4-TiO2nanoparticles inside the pores of the mesoporous MCM-41 host without destroying its integrity. ZnFe2O4nanoparticles can inhibit the transformation of anatase into rutile phase of TiO2. Incorporation of ZnFe2O4-TiO2within MCM-41 avoided the agglomeration of nanoparticles and reduced the band gap energy of TiO2to enhance its visible light photocatalytic activity. UV-vis absorption edges of ZTM nanocomposites redshifted with the increase of Zn/Ti molar ratio. The nanocomposite approach could be a potential choice for enhancing the photoactivity of TiO2, indicating an interesting application in the photodegradation and photoelectric fields.

Thick PLZT Films Grown by Sol-gel for Optical Device Applications

1998 ◽  
Vol 541 ◽  
Author(s):  
M. Linnik ◽  
O. Wilson ◽  
A. Christou
Keyword(s):  
Electron Microscopy ◽  
Sol Gel ◽  
Phase Modulator ◽  
X Ray Diffraction ◽  
X Ray ◽  
Device Applications ◽  
Gel Technique ◽  
Scanning Electron

AbstractThe preparation and characterization of thick PLZT films for spatial phase modulator applications are reported. Films were fabricated on LSCO/LAO substrates by a sol-gel technique using multiple heat-treatment parameters. The crystal quality of PLZT 9/65/35 films was investigated by X-ray diffraction and scanning electron microscopy.

Synthesis and Characterization of CeO2 Doped ZrO2 Ceramics by a Simple Sol-Gel Route

2017 ◽  
Vol 907 ◽  
pp. 56-60
Author(s):  
Ummuhanı Hilal Özer ◽  
Kerim Emre Öksüz ◽  
Ali Özer
Keyword(s):  
Tetragonal Phase ◽  
Sol Gel ◽  
Lattice Parameter ◽  
X Ray Diffraction ◽  
Ceramic Powders ◽  
Zirconia Ceramics ◽  
Simple Method ◽  
X Ray ◽  
Gel Technique

It is well known that sol-gel technique is a simple method to produce nano sized ceramic powders. In this study, cerium oxide doped zirconia samples, with 10 mol%-12mol% and14mol% CeO2, were synthesized by sol-gel technique and characterized. The surface morphology, elemental composition, microstructure, and phase analysis, of the sintered CeO2 doped ZrO2 ceramics were characterized by field emission scanning electron microscopy (FE-SEM), energy dispersive X-ray (EDS) analysis, and X-ray diffraction (XRD) respectively. X-ray diffraction for samples sintered at 1550 °C for 4h revealed that the zirconia ceramics have a tetragonal phase structure. The addition of CeO2 can raise the content of the tetragonal phase, but the minor monoclinic phase exists even at the CeO2 content of 10 mol%. The effect of dopant concentration on the lattice parameter, average primary crystallite size and micro-strain was studied. Relative densities for CeO2 doped ZrO2 bulk ceramics varied between 95% and 99 %, depending on the CeO2 addition.

scholarly journals Impact of alumina particles on the morphology and mechanics of hybrid wood plastic composite materials

2019 ◽  
Vol 51 (1) ◽  
pp. 115-124 ◽  
Author(s):  
Srdjan Perisic ◽  
Marija Vuksanovic ◽  
Milos Petrovic ◽  
Andjela Radisavljevic ◽  
Aleksandar Grujic ◽  
...  
Keyword(s):  
Hybrid Composite ◽  
Moisture Absorption ◽  
Sol Gel ◽  
X Ray Diffraction ◽  
Pressing Method ◽  
X Ray ◽  
Plastic Composite ◽  
Alumina Particles ◽  
Gel Technique ◽  
The Impact

Hybrid composite panels of Wood-Plastic Composites (WPC) consisting of wood and poly (methyl methacrylate) (PMMA) were reinforced with alumina particles and made by ?hot pressing? method. Alumina-based particles were made by sol-gel technique. The particles were characterized by the X-ray diffraction (XRD). The resulting alumina particles were modified with (3mercaptopropyl) trimethoxysilane (MPTMS), in order to obtain better mechanical properties of the composite relative to the composite with unmodified alumina particles. The aim of this work was to study the influence of composite structure and the moisture absorption on bending and the impact properties of the hybrid composite. The bending and impact tests revealed that modulus of elasticity and absorbed energy of deformation increased with modification of alumina and slightly decrease after moisture absorption.

scholarly journals Enhancement of Photocatalytic Activity by Mg2+ Doped Ceria Quantum Dots

2017 ◽  
Vol 2 (1) ◽  
Keyword(s):  
Quantum Dots ◽  
Photocatalytic Activity ◽  
Quantum Dot ◽  
Sol Gel ◽  
Lattice Parameter ◽  
Doped Ceria ◽  
X Ray Diffraction ◽  
X Ray ◽  
Gel Technique ◽  
Cubic Structure

The pure and Mg2+ doped CeO2 quantum dot were synthesized by sol-gel technique. The prepared quantum dots were characterized using X-ray diffraction pattern (XRD), Scanning electron microscope (SEM-EDX). The XRD results show cubic structure of the CeO2 quantum dots. The crystalline size (D), microstrain (ε), dislocation density (δ) and lattice parameter (α) were calculated and analyzed. SEM-EDX analysis shows the morphology and the presence of elements. The photocatalytic activity of the synthesized quantum dot was evaluated based on the photodegradation of methylene blue (MB) by UV-Vis spectrometry.

scholarly journals Synthesis and Characterizations of LaMnO3 Perovskite Powders Using Sol-Gel Method 

2021 ◽  
Author(s):  
Deniz ÇOBAN ÖZKAN ◽  
Ahmet Türk ◽  
Erdal Celik
Keyword(s):  
Photoelectron Spectroscopy ◽  
Sol Gel ◽  
Dye Sensitized Solar Cells ◽  
Ammonium Hydroxide ◽  
X Ray Diffraction ◽  
X Ray ◽  
Dye Sensitized ◽  
Gel Technique ◽  
Sensitized Solar Cells

Abstract The present research demonstrates the synthesis and characterization of LaMnO3 perovskite powders using the sol-gel technique for dye-sensitive solar cell applications. With this respect, transparent solutions were prepared from La and Mn based precursors, distilled water and citric acid monohydrate. Ammonium hydroxide was incorporated into the La-Mn solution in order to neutralize/precipitate at 24oC for 1 hour in the air. The solution was allowed to evaporate on a hot plate device at 90 °C in the air. The obtained solutions were dried at 90 oC for 24 hours to form a xerogel structure, dried at 200 oC for 2 hours and consequently annealed at 500 and 850 oC for 2 hours in the air. Thermal, structural, microstructural, optical and magnetic properties of the powders were characterized through differential thermal analysis-thermogravimetry (DTA-TG), Fourier transform infrared (FTIR), X-ray diffraction (XRD), X-ray Photoelectron Spectroscopy (XPS), scanning electron microscopy (SEM), Malvern zeta sizer (PSD), UV-vis spectrometer and vibrating sample magnetometer (VSM). The obtained results indicate promise, especially the low band range, that LaMnO3 powders can be used in dye-sensitized solar cells and can positively affect performance and efficiency.

Characterization of Sol-Gel Derived (Pb,Ba)(Zr,Ti,Nb)O3 Thin Films for Optical Waveguide Development

1994 ◽  
Vol 343 ◽  
Author(s):  
P. F. Baude ◽  
J. S. Wright ◽  
C. Ye ◽  
L. F. Francis ◽  
D. L. Polla
Keyword(s):  
Thin Films ◽  
Sol Gel ◽  
Silicon Substrates ◽  
X Ray Diffraction ◽  
X Ray ◽  
Sapphire Substrates ◽  
Solution Preparation ◽  
Transmission Measurements ◽  
Gel Technique

ABSTRACT(PbBa)(ZrTiNb)03 thin films and powders have been prepared using the sol-gel technique. Solutions were synthesized in 2-methoxyethanol based upon our previous PZT solution preparation. Three different approaches were used for incorporating barium into PZT alkoxide solutions. Thermal analysis and x-ray diffraction results indicated that barium methoxypropoxide gave the best results. PBZTN (71% Pb and 71% Zr) was deposited onto sapphire substrates as well as oxidized silicon substrates. Optical transmission measurements showed greater than 80% transmission for wavelengths longer than 400 nm. Films with thickness of 3000 Å on sapphire exhibited a refractive index of 2.19 at λ=633 nm.

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