X-ray Diffraction Analysis of Rust Layer on a Weathering Steel Bridge with Surface Treatment Using Synchrotron Radiation

The present study presents the relevance of X-ray diffraction analysis using synchrotron light in the identification of phases with low intensity peaks. Niobium sheets were coated with monetite and then converted to hydroxyapatite in an alkali solution. Octacalcium phosphate was identified as an intermediate phase in the conversion monetite-hydroxyapatite.

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An attempt of in vivo X-ray diffraction analysis of kidney stones with the use of synchrotron radiation

Nuclear Instruments and Methods in Physics Research Section A Accelerators Spectrometers Detectors and Associated Equipment ◽

10.1016/j.nima.2005.01.245 ◽

2005 ◽

Vol 543 (1) ◽

pp. 302-305 ◽

Cited By ~ 5

Author(s):

A.I. Ancharov ◽

A.I. Nizovskii ◽

S.A. Gridnev ◽

I.V. Feofilov ◽

A.N. Vichkanov

Keyword(s):

Synchrotron Radiation ◽

Diffraction Analysis ◽

Kidney Stones ◽

X Ray Diffraction ◽

X Ray

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Self-propagating high-temperature synthesis by the method of X-ray diffraction analysis using synchrotron radiation

Combustion Explosion and Shock Waves ◽

10.1007/bf00783640 ◽

1983 ◽

Vol 19 (4) ◽

pp. 430-431 ◽

Cited By ~ 18

Author(s):

V. V. Aleksandrov ◽

M. A. Korchagin ◽

B. P. Tolochko ◽

M. A. Sheromov

Keyword(s):

High Temperature ◽

Synchrotron Radiation ◽

Diffraction Analysis ◽

X Ray Diffraction ◽

Temperature Synthesis ◽

X Ray ◽

High Temperature Synthesis

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Texture on Ground, Fractured, and Aged Y-TZP Surfaces

MRS Proceedings ◽

10.1557/proc-78-25 ◽

1986 ◽

Vol 78 ◽

Cited By ~ 7

Author(s):

Franz Reidinger ◽

Philip J. Whalen

Keyword(s):

Phase Composition ◽

Transition Temperature ◽

Diffraction Analysis ◽

Surface Treatment ◽

Tetragonal Phase ◽

Surface Region ◽

X Ray Diffraction ◽

X Ray ◽

History Of

ABSTRACTThe phase composition of Y-TZP surfaces has been shown to vary greatly depending on the thermo-mechanical history of the surface. The orientation of these different phases in the surface region is not always random. There is speculation that the alignment of the tetragonal phase before fracturing may play a part in increasing the toughness of these materials. This article deals with an X-ray diffraction analysis of various Y-TZP surfaces with special emphasis on the texture of the different phases. Surfaces which have been ground (and polished), fractured, and aged (200°C) have been examined. In all cases, the monoclinic component that was formed was strongly oriented. The tetragonal phase may or may not be oriented depending on surface treatment. Annealing above the monoclinic-tetragonal transition temperature had little effect on the tetragonal orientation in most cases. Samples fractured at 1000°C have no unusual orientation on the fracture faces.

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Synchrotron radiation X-ray diffraction analysis for Bi-based oxide superconducting wire

Diamond Light Source Proceedings ◽

10.1017/s2044820110000444 ◽

2010 ◽

Vol 1 (SRMS-7) ◽

Author(s):

S. Uemura ◽

J. Iihara ◽

Y. Saito ◽

K. Yamaguchi ◽

J. Matsumoto ◽

...

Keyword(s):

Synchrotron Radiation ◽

Diffraction Analysis ◽

Crystal Orientation ◽

Power Transmission ◽

Process Conditions ◽

X Ray Diffraction ◽

Cooling Process ◽

X Ray ◽

Superconducting Wire

The Bi-based oxide superconducting wire is one of the most promising materials for practical uses such as electric power transmission, electromagnets and so on. For the higher performances required in these applications, it is necessary to increase the critical current (Ic). We have carried out synchrotron radiation X-ray diffraction analysis to improve our manufacturing processes and thus to achieve higher Ic. We have performed in situ X-ray diffraction measurements during the sintering and cooling processes, and observed the decrease of Bi-2223(=(Bi,Pb)2Sr2Ca2Cu3Ox) phase during the cooling process. We have also evaluated the distribution of the crystal orientation in whole wire thickness, by measuring the rocking curves. We have observed that the distribution of the crystal orientation is improved by a refinement of the process conditions.

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Synchrotron radiation in situ X-ray absorption fine structure and in situ X-ray diffraction analysis of a high-performance cobalt catalyst towards the oxygen reduction reaction

Physical Chemistry Chemical Physics ◽

10.1039/c7cp05888h ◽

2017 ◽

Vol 19 (45) ◽

pp. 30749-30755

Author(s):

Haiying Qin ◽

Longxia Lin ◽

Junkang Jia ◽

Huangliang Ni ◽

Yan He ◽

...

Keyword(s):

Fine Structure ◽

Synchrotron Radiation ◽

Diffraction Analysis ◽

High Performance ◽

Cobalt Catalyst ◽

Reduction Reaction ◽

X Ray Diffraction ◽

X Ray ◽

X Ray Absorption

The evolution of metallic Co to Co(OH)2 and then to CoOOH during the ORR was revealed by in situ XRD combined with in situ XAFS tests.

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X-ray diffraction analysis of secondary phases in zirconium alloys before and after neutron irradiation at the MARS synchrotron radiation beamline

Journal of Nuclear Materials ◽

10.1016/j.jnucmat.2013.02.020 ◽

2013 ◽

Vol 437 (1-3) ◽

pp. 365-372 ◽

Cited By ~ 15

Author(s):

J.-L. Béchade ◽

D. Menut ◽

S. Doriot ◽

S. Schlutig ◽

B. Sitaud

Keyword(s):

Synchrotron Radiation ◽

Diffraction Analysis ◽

Neutron Irradiation ◽

Zirconium Alloys ◽

Secondary Phases ◽

X Ray Diffraction ◽

X Ray ◽

Before And After

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Non-Destructive X-Ray Diffraction Analysis of the Under-Film Corrosion Processes in Zinc-Coated Steel Sheets by Synchrotron Radiation

MRS Proceedings ◽

10.1557/proc-280-557 ◽

1992 ◽

Vol 280 ◽

Cited By ~ 1

Author(s):

K. Nose ◽

K. Kawasaki ◽

K. Hayashi ◽

H. Morikawa ◽

S. Sasaki

Keyword(s):

Synchrotron Radiation ◽

Diffraction Analysis ◽

Salt Spray ◽

Coated Steel ◽

X Ray Diffraction ◽

One Dimensional ◽

X Ray ◽

Steel Sheets ◽

Zinc Coated Steel ◽

Non Destructive

ABSTRACTA highly brilliant x-ray beam from a synchrotron radiation source is a powerful tool to perform non-destructive x-ray diffraction analysis of an under-film corroded region of zinc-coated steel sheets. Investigations to identify corrosion products under the outdoor salt-spray test condition and to reveal their one-dimensional distribution were carried out Simonkolleite (ZnCl2•4Zn(OH)2 ) was identified for the first time at the tip of the under-film corroded region. By the one-dimensional analysis, it was shown that the x-ray diffraction intensity of simonkolleite increased, where that of metal zinc decreased. It was suggested that simonkolleite was formed as the first corrosion product under the outdoor salt-spray test condition.

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