scholarly journals Review on Dynamic Recrystallization of Martensitic Stainless Steels during Hot Deformation: Part I—Experimental Study

Metals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 572
Author(s):  
Hamed Aghajani Derazkola ◽  
Eduardo García Gil ◽  
Alberto Murillo-Marrodán ◽  
Damien Méresse

The evolution of the microstructure changes during hot deformation of high-chromium content of stainless steels (martensitic stainless steels) is reviewed. The microstructural changes taking place under high-temperature conditions and the associated mechanical behaviors are presented. During the continuous dynamic recrystallization (cDRX), the new grains nucleate and growth in materials with high stacking fault energies (SFE). On the other hand, new ultrafine grains could be produced in stainless steel material irrespective of the SFE employing high deformation and temperatures. The gradual transformation results from the dislocation of sub-boundaries created at low strains into ultrafine grains with high angle boundaries at large strains. There is limited information about flow stress and monitoring microstructure changes during the hot forming of martensitic stainless steels. For this reason, continuous dynamic recrystallization (cDRX) is still not entirely understood for these types of metals. Recent studies of the deformation behavior of martensitic stainless steels under thermomechanical conditions investigated the relationship between the microstructural changes and mechanical properties. In this review, grain formation under thermomechanical conditions and dynamic recrystallization behavior of this type of steel during the deformation phase is discussed.

2004 ◽  
Vol 467-470 ◽  
pp. 1229-1236 ◽  
Author(s):  
Tarcisio R. Oliveira ◽  
Frank Montheillet

The study was carried out to understand the mechanisms occurring during dynamic recrystallization of hot deformed 11% chromium stabilized ferritic stainless steels and to compare the behaviour induced by various types of stabilization. It was observed that continuous dynamic recrystallization (CDRX) operates in all materials starting at the onset of straining. Niobium has a more pronounced influence on hardening than titanium during hot deformation, which is due to solid solution strengthening and also to the reduction or stopping of grain boundary migration by solute drag effect. The D2 component, { 2 1 1 }<111>, was found as the major texture component at the steady state for the torsion tests carried along the negative shear direction. It was likely to be formed by the combination of straining and growth of the grains exhibiting both low stored energy and low rotation rate of the crystallographic axes.


Materials ◽  
2018 ◽  
Vol 11 (8) ◽  
pp. 1443 ◽  
Author(s):  
Lei Liu ◽  
Yunxin Wu ◽  
Hai Gong ◽  
Shuang Li ◽  
A. S. Ahmad

The isothermal compression tests of the 2219 Al alloy were conducted at the temperature and the strain rate ranges of 623–773 K and 0.01–10 s−1, respectively, and the deformed microstructures were observed. The flow curves of the 2219 Al alloy obtained show that flow stress decreases with the increase in temperature and/or the decrease in strain rate. The physically based constitutive model is applied to describe the flow behavior during hot deformation. In this model, Young’s modulus and lattice diffusion coefficient are temperature-dependent, and the creep exponent is regarded as a variable. The predicted values calculated by the constitutive model are in good agreement with the experimental results. In addition, it is confirmed that the main softening mechanism of the 2219 Al alloy during hot deformation is dynamic recovery and incomplete continuous dynamic recrystallization (CDRX) by the analysis of electron backscattered diffraction (EBSD) micrographs. Moreover, CDRX can readily occur under the condition of high temperatures, low strain rates, and large strains. Meanwhile, the recrystallization grain size will also be larger.


Materials ◽  
2020 ◽  
Vol 13 (20) ◽  
pp. 4553
Author(s):  
Shaomin Lv ◽  
Jinbin Chen ◽  
Xinbo He ◽  
Chonglin Jia ◽  
Kang Wei ◽  
...  

Sub-solvus dynamic recrystallization (DRX) mechanisms in an advanced γ-γ’ nickel-based superalloy GH4151 were investigated by isothermal compression experiments at 1040 °C with a strain rate of 0.1 s−1 and various true strain of 0.1, 0.3, 0.5, and 0.7, respectively. This has not been reported in literature before. The electron backscatter diffraction (EBSD) and transmission electron microscope (TEM) technology were used for the observation of microstructure evolution and the confirmation of DRX mechanisms. The results indicate that a new dynamic recrystallization mechanism occurs during hot deformation of the hot-extruded GH4151 alloy. The nucleation mechanism can be described as such a feature, that is a primary γ’ (Ni3(Al, Ti, Nb)) precipitate embedded in a recrystallized grain existed the same crystallographic orientation, which is defined as heteroepitaxial dynamic recrystallization (HDRX). Meanwhile, the conventional DRX mechanisms, such as the discontinuous dynamic recrystallization (DDRX) characterized by bulging grain boundary and continuous dynamic recrystallization (CDRX) operated through progressive sub-grain merging and rotation, also take place during the hot deformation of the hot-extruded GH4151 alloy. In addition, the step-shaped structures can be observed at grain boundaries, which ensure the low-energy surface state during the DRX process.


2004 ◽  
Vol 467-470 ◽  
pp. 1151-1156 ◽  
Author(s):  
Cédric Chauvy ◽  
Pierre Barbéris ◽  
Frank Montheillet

Compression tests were used to simulate simple deformation paths within the upper a-range of Zircaloy-4 (i.e. 500°C-750°C). The mechanical behaviour reveals two different domains : at low temperatures and large strain rates, strain hardening takes place before flow softening, whereas this first stage disappears at lower flow stress levels. Strain rate sensitivity and activation energy were determined for both domains. Dynamic recrystallization was investigated using the Electron BackScattering Diffraction (EBSD) technique. It appears that the mechanism involved here is continuous dynamic recrystallization (CDRX), based on the increasing misorientation of subgrain boundaries and their progressive transformation into large angle boundaries. At low strains (e £ 0.3), CDRX kinetics are similar whatever the deformation conditions, while higher temperatures and lower strain rates promote recrystallization at large strains.


2018 ◽  
Vol 941 ◽  
pp. 1443-1449 ◽  
Author(s):  
María Cecilia Poletti ◽  
Ricardo Buzolin ◽  
Sanjev Kumar ◽  
Peng Wang ◽  
Thierry Franz Jules Simonet-Fotso

This work deals with the analysis and modelling of the microstructural evolution of the metastable titanium alloy Ti-5Al-5V-5Mo-3Cr during hot deformation up to moderate and large strains. Experimental flow curves and deformed samples are obtained by hot compression and hot torsion tests using a Gleeble ® 3800 device. The samples are deformed above and below the beta transus temperature and in a wide range of strain rates. Microstructures are characterized after deformation and in-situ water quenching using light optical and scanning electron microscopy and electron back scattered diffraction (EBSD). Dynamic recovery of the beta phase is found to be the main deformation mechanism up to moderated strains. By increasing the strain, continuous dynamic recrystallization (cDRX) is confirmed by the progressive conversion of low angle boundaries into high-angle boundaries. Alpha phase plays a secondary role in the deformation of the material by pinning the movement of beta high angle grain boundaries (HAGB). The evolution of the microstructure is modelled using dislocation density as internal variable in the single β field.


2004 ◽  
Vol 467-470 ◽  
pp. 1199-1204 ◽  
Author(s):  
Rustam Kaibyshev ◽  
I. Mazurina ◽  
Oleg Sitdikov

The mechanism of new grain evolution during equal channel angular extrusion (ECAE) up to a total strain of ~12 in an Al-Cu-Mn-Zr alloy at a temperature of 475oC (0.75Tm) was examined. It was shown that the new grains with an average size of about 15 µm result from a specific process of geometric dynamic recrystallization (GRX) which can be considered as a type of continuous dynamic recrystallization (CDRX). This process involves three elementary mechanisms. At moderate strains, extensive elongation of initial grains takes place; old grain boundaries become progressively serrated. Upon further ECAE processing, transverse low-angle boundaries (LAB) with misorientation ranging from 5 to 15o are evolved between grain boundary irregularities subdividing the initial elongated grains on crystallites with essentially equiaxed shape. The misorientation of these transverse subboundaries rapidly increases with increasing strain, resulting in the formation of true recrystallized grains outlined by high-angle boundaries from all sides. In the same time, the average misorientation of deformation-induced boundaries remains essentially unchanged during ECAE. It is caused by the fact that the evolution of LABs with misorientation less than 4o occurs continuously during severe plastic deformation. The mechanism maintaining the stability of the transverse subboundaries that is a prerequisite condition for their further transformation into highangle boundaries (HABs) is discussed.


2005 ◽  
Vol 488-489 ◽  
pp. 223-226 ◽  
Author(s):  
Xu Yue Yang ◽  
Masayoshi Sanada ◽  
Hiromi Miura ◽  
Taku Sakai

Hot deformation and associated structural changes were studied in compression of a magnesium alloy AZ31 with initial grain sizes (D0) of 22 µm and 90 µm at a temperature of 573K. D0 influences significantly the flow curve and the kinetics of grain refinement during hot deformation. For D0 = 22 µm, grain fragmentation takes place due to frequent formation of kink bands initially at corrugated grain boundaries and then in grain interiors in low strain, followed by full development of new fine grains in high strain. For D0 = 90 µm, in contrast, twinning takes place in coarser original grains, and then kink bands and new fine grains are formed mainly in finer ones at low strains. Then new grains are formed in necklace along the boundaries of coarse original grains, followed by their development into the grain interiors. Grain refinement in the Mg alloy can be concluded to result from a series of deformation-induced continuous reactions, they are essentially similar to continuous dynamic recrystallization (cDRX).


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