scholarly journals On the Strain Rate Sensitivity of Fused Filament Fabrication (FFF) Processed PLA, ABS, PETG, PA6, and PP Thermoplastic Polymers

Polymers ◽  
2020 ◽  
Vol 12 (12) ◽  
pp. 2924
Author(s):  
Nectarios Vidakis ◽  
Markos Petousis ◽  
Emmanouil Velidakis ◽  
Marco Liebscher ◽  
Viktor Mechtcherine ◽  
...  
Keyword(s):  
Strain Rate ◽  
Strain Rate Sensitivity ◽  
Mechanical Response ◽  
Rate Sensitivity ◽  
Polymeric Materials ◽  
Applied Strain ◽  
Sensitivity Index ◽  
Strain Rates ◽  
Thermoplastic Polymers ◽  
Fused Filament Fabrication

In this study, the strain rate sensitivity of five different thermoplastic polymers processed via Fused Filament Fabrication (FFF) Additive Manufacturing (AM) is reported. Namely, Polylactic Acid (PLA), Acrylonitrile-Butadiene-Styrene (ABS), Polyethylene Terephthalate Glycol (PETG), Polyamide 6 (PA6), and Polypropylene (PP) were thoroughly investigated under static tensile loading conditions at different strain rates. Strain rates have been selected representing the most common applications of polymeric materials manufactured by Three-Dimensional (3D) Printing. Each polymer was exposed to five different strain rates in order to elucidate the dependency and sensitivity of the tensile properties, i.e., stiffness, strength, and toughness on the applied strain rate. Scanning Electron Microscopy (SEM) was employed to investigate the 3D printed samples’ fractured surfaces, as a means to derive important information regarding the fracture process, the type of fracture (brittle or ductile), as well as correlate the fractured surface characteristics with the mechanical response under certain strain rate conditions. An Expectation–Maximization (EM) analysis was carried out. Finally, a comparison is presented calculating the strain rate sensitivity index “m” and toughness of all materials at the different applied strain rates.

scholarly journals Strain Rate Sensitivity of Polycarbonate and Thermoplastic Polyurethane for Various 3D Printing Temperatures and Layer Heights

Polymers ◽  
2021 ◽  
Vol 13 (16) ◽  
pp. 2752
Author(s):  
Nectarios Vidakis ◽  
Markos Petousis ◽  
Apostolos Korlos ◽  
Emmanouil Velidakis ◽  
Nikolaos Mountakis ◽  
...  
Keyword(s):  
Strain Rate ◽  
Strain Rate Sensitivity ◽  
Mechanical Response ◽  
Thermoplastic Polyurethane ◽  
Temperature Response ◽  
Tensile Modulus ◽  
Rate Sensitivity ◽  
Sensitivity Index ◽  
Strain Rates ◽  
Fused Filament Fabrication

In this work, strain rate sensitivity was studied for 3D-printed polycarbonate (PC) and thermoplastic polyurethane (TPU) materials. Specimens were fabricated through fused filament fabrication (FFF) additive manufacturing (AM) technology and were tested at various strain rates. The effects of two FFF process parameters, i.e., nozzle temperature and layer thickness, were also investigated. A wide analysis for the tensile strength (MPa), the tensile modulus of elasticity (MPa), the toughness (MJ/m3) and the strain rate sensitivity index ‘m’ was conducted. Additionally, a morphological analysis was conducted using scanning electron microscopy (SEM) on the side and the fracture area of the specimens. Results from the different strain rates for each material were analyzed, in conjunction with the two FFF parameters tested, to determine their effect on the mechanical response of the two materials. PC and TPU materials exhibited similarities regarding their temperature response at different strain rates, while differences in layer height emerged regarding the appropriate choice for the FFF process. Overall, strain rate had a significant effect on the mechanical response of both materials.

Mechanical behaviour and superplastic forming capabilities of extra-low interstitial grade Ti-6Al-4V wire alloy with numerical verification

2007 ◽  
Vol 221 (3) ◽  
pp. 165-174 ◽  
Author(s):  
M D Naughton ◽  
P Tiernan
Keyword(s):  
Flow Stress ◽  
Strain Rate ◽  
Strain Rate Sensitivity ◽  
Rate Sensitivity ◽  
Superplastic Forming ◽  
Effect Of Temperature ◽  
Sensitivity Index ◽  
Numerical Verification ◽  
Strain Rates ◽  
Strain Rate Sensitivity Index

In this paper, the behaviour of extra-low interstitial (ELI) grade Ti-6Al-4V wire alloy has been extensively studied at varying strain rates in the range of 10-5-102 s-1 at temperatures ranging between 750 °C and 1050 °C using processing maps and experimental data to determine the material's mechanical and superplastic forming capabilities. From the slope of a log plot of strain rate versus flow stress, the strain-rate sensitivity index, m, was determined. A plot of m versus the log of strain rate was produced in order to identify the key strain rates in which ELI grade Ti-6Al-4V exhibits its superplastic regime. It was determined that this alloy is most sensitive to superplastic forming within a narrow strain-rate band of 10-4-10-3 s-1 and has a maximum strain-rate sensitivity index, m = 0.45. At strain rates below and above this range, the material exhibited negligible levels of superplasticity. The key temperature for superplastic forming was determined to be 950 °C. The effect of temperature on flow stress and flow stability was analysed using the Zener-Holloman parameter. The experimentally determined results showed excellent agreement with Guo and Ridley's activation mathematical model.

scholarly journals Compressive Behaviour of Additively Manufactured Periodical Re-Entrant Tetrakaidecahedral Lattices at Low and High Strain-Rates

Metals ◽  
2021 ◽  
Vol 11 (8) ◽  
pp. 1196
Author(s):  
Michaela Neuhäuserová ◽  
Tomáš Fíla ◽  
Petr Koudelka ◽  
Jan Falta ◽  
Václav Rada ◽  
...  
Keyword(s):  
Strain Rate ◽  
Strain Rate Sensitivity ◽  
High Speed ◽  
Mechanical Response ◽  
Split Hopkinson Pressure Bar ◽  
Deformation Behaviour ◽  
Rate Sensitivity ◽  
Image Correlation ◽  
Strain Rates ◽  
Static Compression

Compressive deformation behaviour of additively manufactured lattice structures based on re-entrant tetrakaidecahedral unit-cell geometry were experimentally investigated under quasi-static and dynamic loading conditions. Specimens of four different structures formed by three-dimensional periodical assembly of selected unit-cells were produced by a laser powder bed fusion technique from a powdered austenitic stainless steel SS316L. Quasi-static compression as well as dynamic tests using split Hopkinson pressure bar (SHPB) apparatus at two strain-rates were conducted to evaluate the expected strain-rate sensitivity of the fundamental mechanical response of the structures. To evaluate the experiments, particularly the displacement fields of the deforming lattices, optical observation of the specimens using a high-resolution camera (quasi-static loading) and two synchronised high-speed cameras (SHPB experiments) was employed. An in-house digital image correlation algorithm was used in order to evaluate the anticipated auxetic nature of the investigated lattices. It was found that neither of the investigated structures exhibited auxetic behaviour although strain-rate sensitivity of the stress–strain characteristics was clearly identified for the majority of structures.

Local Investigations of the Mechanical Properties of Ultrafine Grained Metals by Nanoindentations

2006 ◽  
Vol 503-504 ◽  
pp. 31-36 ◽  
Author(s):  
Johannes Mueller ◽  
Karsten Durst ◽  
Dorothea Amberger ◽  
Matthias Göken
Keyword(s):  
Mechanical Properties ◽  
Strain Rate ◽  
Strain Rate Sensitivity ◽  
Room Temperature ◽  
Rate Sensitivity ◽  
Strain Rates ◽  
Fcc Metals ◽  
Angular Pressing ◽  
Ultrafine Grained ◽  
Indentation Strain

The mechanical properties of ultrafine-grained metals processed by equal channel angular pressing is investigated by nanoindentations in comparison with measurements on nanocrystalline nickel with a grain size between 20 and 400 nm produced by pulsed electrodeposition. Besides hardness and Young’s modulus measurements, the nanoindentation method allows also controlled experiments on the strain rate sensitivity, which are discussed in detail in this paper. Nanoindentation measurements can be performed at indentation strain rates between 10-3 s-1 and 0.1 s-1. Nanocrystalline and ultrafine-grained fcc metals as Al and Ni show a significant strain rate sensitivity at room temperature in comparison with conventional grain sized materials. In ultrafine-grained bcc Fe the strain rate sensitivity does not change significantly after severe plastic deformation. Inelastic effects are found during repeated unloading-loading experiments in nanoindentations.

Strain Rate Sensitivity of Mixed SAC-SnBi Solder Joints

2019 ◽  
Vol 2019 (1) ◽  
pp. 000480-000487
Author(s):  
Luke A. Wentlent ◽  
James Wilcox ◽  
Xuanyi Ding
Keyword(s):  
Melting Point ◽  
Strain Rate ◽  
Strain Rate Sensitivity ◽  
Solder Joints ◽  
Volume Ratio ◽  
Rate Sensitivity ◽  
Thermal Exposure ◽  
Fracture Mechanisms ◽  
Eutectic System ◽  
Strain Rates

Abstract As the electronics industry continues to evolve a concerted effort has developed to implement lower melting point solders. The ability to minimize the thermal exposure that an assembly is subjected to affords significant benefits with respect to both the reliability and the materials that can be used. One of the most popular low melt solder alloys currently being investigated by the industry is the Bi-Sn eutectic system, which has a melting point of 139°C. The BiSn system itself is not particularly novel as it was posited as a SAC alternative during the initial shift from Pb based solders. While a body of knowledge currently exists regarding this system, and the near eutectic variant BiSnAg, there are still concerns regarding its ductility, especially as a function of thermal exposure and strain rate. Bismuth is widely acknowledged as a brittle element and its presence in such quantities raises concerns of not just Cu6Sn5 embrittlement but also solder fragility in high strain rate types of environments. A challenge with regards to near term implementation is that most packages are not available with BiSn solder bumps. Therefore, it will be necessary to use components already balled with SAC 305 solder. This means that the resulting solder interconnect, reflowed below conventional SAC reflow temperatures, will form a type of mixed hybrid microstructure. This non-equilibrium microstructure will be composed of two regions, one Bi-rich region which is well past saturation and a second region which is Bi-deficient. It is of specific industrial interest then to not just investigate the BiSn solder system but also within the context of a realistic mixed interconnect. Recent work by several researchers has shown that this hybrid microstructure is unstable and quite active with respect to the movement and localized concentration of the Bismuth. The degree of mixing of these two regions has been shown to be highly dependent upon reflow temperature and the paste to ball volume ratio. Mixed SAC-BiSn solder joints were formed by placing SAC 305 spheres on BiSn paste deposits for a paste to ball volume ratio of .18. These samples were then reflowed at either 175°C or 200°C. SAC 305 control samples were also made using a conventional Pb-free reflow profile with a peak temperature of 247°C. A 22 mil Cu-OSP pad on a 1.0 mm thick FR4 substrate was used for all samples. A selection of the solder joints were then isothermally aged at 90°C for 200 hours. Using a joint level micromechanical tester, ball shear tests were conducted at a range of strain rates for samples in the as-reflowed and aged state. Using this information, the strain rate sensitivity of the interconnects was mapped and correlated with the observed failure modes. Investigations into the fracture mechanisms were conducted by examining the shear fracture surface with optical and scanning electron microscopy. Additionally, the evolution of the microstructure was characterized. Results showed a clear transition from ductile solder failure to a brittle separation failure at the higher strain rates.

scholarly journals Strain-Rate-Dependent Deformation Behavior and Mechanical Properties of a Multi-Phase Medium-Manganese Steel

Metals ◽  
2019 ◽  
Vol 9 (3) ◽  
pp. 344 ◽  
Author(s):  
Simon Sevsek ◽  
Christian Haase ◽  
Wolfgang Bleck
Keyword(s):  
Mechanical Properties ◽  
Strain Rate ◽  
Strain Rate Sensitivity ◽  
Deformation Behavior ◽  
Rate Sensitivity ◽  
Manganese Steel ◽  
Strain Rates ◽  
Rate Dependent ◽  
Medium Manganese Steel ◽  
Multi Phase

The strain-rate-dependent deformation behavior of an intercritically annealed X6MnAl12-3 medium-manganese steel was analyzed with respect to the mechanical properties, activation of deformation-induced martensitic phase transformation, and strain localization behavior. Intercritical annealing at 675 °C for 2 h led to an ultrafine-grained multi-phase microstructure with 45% of mostly equiaxed, recrystallized austenite and 55% ferrite or recovered, lamellar martensite. In-situ digital image correlation methods during tensile tests revealed strain localization behavior during the discontinuous elastic-plastic transition, which was due to the localization of strain in the softer austenite in the early stages of plastic deformation. The dependence of the macroscopic mechanical properties on the strain rate is due to the strain-rate sensitivity of the microscopic deformation behavior. On the one hand, the deformation-induced phase transformation of austenite to martensite showed a clear strain-rate dependency and was partially suppressed at very low and very high strain rates. On the other hand, the strain-rate-dependent relative strength of ferrite and martensite compared to austenite influenced the strain partitioning during plastic deformation, and subsequently, the work-hardening rate. As a result, the tested X6MnAl12-3 medium-manganese steel showed a negative strain-rate sensitivity at very low to medium strain rates and a positive strain-rate sensitivity at medium to high strain rates.

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