Analysis of Laser Fusion Zone of Lotus-Type Porous Metals by 3-Dimensional FEM

Author(s):  
Takuya Tsumura ◽  
Taichi Murakami ◽  
Soong Keun Hyun ◽  
Hideo Nakajima ◽  
Kazuhiro Nakata
Author(s):  
Takuya Tsumura ◽  
Fu Xing Ye ◽  
Taichi Murakami ◽  
Hideo Nakajima ◽  
Kazuhiro Nakata

2005 ◽  
Vol 502 ◽  
pp. 499-504 ◽  
Author(s):  
Takuya Tsumura ◽  
Taichi Murakami ◽  
Soong Keun Hyun ◽  
Hideo Nakajima ◽  
Kazuhiro Nakata

Effects of pore directions on the profile of fusion zone for lotus-type porous magnesium by laser welding has been investigated by comparing the experimental observations and the results of numerical simulation. The three-dimensional finite element calculations were performed, which takes into account equivalent thermal properties and anisotropy of thermal conductivity. There is the pore anisotropy in the profile of fusion zone by laser beam irradiation and the good weldability was obtained when the growth direction of the original pore equaled to the direction of the laser beam irradiation. A good agreement was obtained between the calculated profile of the weld fusion zone and the experimental results.


2006 ◽  
Vol 47 (9) ◽  
pp. 2248-2253 ◽  
Author(s):  
Takuya Tsumura ◽  
Taichi Murakami ◽  
Hideo Nakajima ◽  
Kazuhiro Nakata

2007 ◽  
Vol 127 ◽  
pp. 307-312 ◽  
Author(s):  
Takuya Tsumura ◽  
Fu Xing Ye ◽  
Taichi Murakami ◽  
Hideo Nakajima ◽  
Kazuhiro Nakata

Lotus-type porous metals, whose pores are aligned in one direction by unidirectional solidification, have a unique combination of properties. These are expected as revolutionary engineering materials with anisotropy of the properties. For the industrial use of the lotus-type porous metals, a reliable joining technology is required. We already reported the melting property of a few lotus-type porous metals by laser welding. These results indicated that these materials possessed anisotropy of melting property with the pore direction perpendicular and parallel to the specimen surface, especially remarkable anisotropy was obtained for the copper specimen owing to the difference of the laser energy absorption to the specimen surface. In this report, the three-dimensional heat transfer analyses, which take into account the difference of the laser energy absorption comparing with the anisotropy of thermal conductivity inherent to lotus-type porous metals, were performed by commercial code with user-defined subroutine. Predicted profile of weld fusion zone is in good agreement with the cross-sectional view obtained by experiments.


Author(s):  
Robert Glaeser ◽  
Thomas Bauer ◽  
David Grano

In transmission electron microscopy, the 3-dimensional structure of an object is usually obtained in one of two ways. For objects which can be included in one specimen, as for example with elements included in freeze- dried whole mounts and examined with a high voltage microscope, stereo pairs can be obtained which exhibit the 3-D structure of the element. For objects which can not be included in one specimen, the 3-D shape is obtained by reconstruction from serial sections. However, without stereo imagery, only detail which remains constant within the thickness of the section can be used in the reconstruction; consequently, the choice is between a low resolution reconstruction using a few thick sections and a better resolution reconstruction using many thin sections, generally a tedious chore. This paper describes an approach to 3-D reconstruction which uses stereo images of serial thick sections to reconstruct an object including detail which changes within the depth of an individual thick section.


Author(s):  
C.W. Akey ◽  
M. Szalay ◽  
S.J. Edelstein

Three methods of obtaining 20 Å resolution in sectioned protein crystals have recently been described. They include tannic acid fixation, low temperature embedding and grid sectioning. To be useful for 3-dimensional reconstruction thin sections must possess suitable resolution, structural fidelity and a known contrast. Tannic acid fixation appears to satisfy the above criteria based on studies of crystals of Pseudomonas cytochrome oxidase, orthorhombic beef liver catalase and beef heart F1-ATPase. In order to develop methods with general applicability, we have concentrated our efforts on a trigonal modification of catalase which routinely demonstrated a resolution of 40 Å. The catalase system is particularly useful since a comparison with the structure recently solved with x-rays will permit evaluation of the accuracy of 3-D reconstructions of sectioned crystals.Initially, we re-evaluated the packing of trigonal catalase crystals studied by Longley. Images of the (001) plane are of particular interest since they give a projection down the 31-screw axis in space group P3121. Images obtained by the method of Longley or by tannic acid fixation are negatively contrasted since control experiments with orthorhombic catalase plates yield negatively stained specimens with conditions used for the larger trigonal crystals.


Author(s):  
Atul S. Ramani ◽  
Earle R. Ryba ◽  
Paul R. Howell

The “decagonal” phase in the Al-Co-Cu system of nominal composition Al65CO15Cu20 first discovered by He et al. is especially suitable as a topic of investigation since it has been claimed that it is thermodynamically stable and is reported to be periodic in the dimension perpendicular to the plane of quasiperiodic 10-fold symmetry. It can thus be expected that it is an important link between fully periodic and fully quasiperiodic phases. In the present paper, we report important findings of our transmission electron microscope (TEM) study that concern deviations from ideal decagonal symmetry of selected area diffraction patterns (SADPs) obtained from several “decagonal” phase crystals and also observation of a lattice of main reflections on the 10-fold and 2-fold SADPs that implies complete 3-dimensional lattice periodicity and the fundamentally incommensurate nature of the “decagonal” phase. We also present diffraction evidence for a new transition phase that can be classified as being one-dimensionally quasiperiodic if the lattice of main reflections is ignored.


Author(s):  
A. Engel ◽  
A. Holzenburg ◽  
K. Stauffer ◽  
J. Rosenbusch ◽  
U. Aebi

Reconstitution of solubilized and purified membrane proteins in the presence of phospholipids into vesicles allows their functions to be studied by simple bulk measurements (e.g. diffusion of differently sized solutes) or by conductance measurements after transformation into planar membranes. On the other hand, reconstitution into regular protein-lipid arrays, usually forming at a specific lipid-to-protein ratio, provides the basis for determining the 3-dimensional structure of membrane proteins employing the tools of electron crystallography.To refine reconstitution conditions for reproducibly inducing formation of large and highly ordered protein-lipid membranes that are suitable for both electron crystallography and patch clamping experiments aimed at their functional characterization, we built a flow-dialysis device that allows precise control of temperature and flow-rate (Fig. 1). The flow rate is generated by a peristaltic pump and can be adjusted from 1 to 500 ml/h. The dialysis buffer is brought to a preselected temperature during its travel through a meandering path before it enters the dialysis reservoir. A Z-80 based computer controls a Peltier element allowing the temperature profile to be programmed as function of time.


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