Investigation of the Optimal Heat Treatment of As-Cast Al-5.7Si-2Cu-0.3Mg Aluminium Alloys

2021 ◽  
Vol 105 ◽  
pp. 48-58
Author(s):  
M.A. Abdelgnei ◽  
M.Z. Omar ◽  
M.J. Ghazali ◽  
M.N. Mohammed
Keyword(s):  
Heat Treatment ◽  
Aluminium Alloys ◽  
Cast Alloy ◽  
Solution Treatment ◽  
Hot Water ◽  
High Concentration ◽  
Hardness Tester ◽  
Treatment Conditions ◽  
Heat Treated ◽  
Optimum Heat

The aim of this work is to investigate the optimum heat treatment for Al-5.7Si-2Cu-0.3Mg aluminium alloys and study its effect on microstructure, phase transformations, and hardness. The test specimens were taken from the as-received alloy. Solution treatment was performed at 485°C and 500°C under various solution treatment times for 4, 8, 10, and 12h, and the samples were then hot water quenched at 60°C, followed by aged hardening at 150°C, 170°C and 190°C for 2,6,10, and 14h, and subsequently air-cooled. The hardness of the Al-5.7%Si-2Cu%-0.3%Mg alloys were determined using a Rockwell hardness tester. Scanning electron microscopy (SEM) and optical microscopy (OM) were used to determine the microstructure of the samples, while X-ray diffraction (XRD) was used to identify the phase compositions. The resulting microstructures and hardness values were compared to the corresponding as-cast samples. It can be seen that the solution treatment at 485°C for 12 h and aging at 190°C for 10 h are the optimum T6 heat treatment conditions that would result in hardening precipitates over the as-cast alloy. OM and SEM morphologies show significant microstructure evaluation of improved distribution of the Si particles. After T6 treatment, the morphology of Si particles in the as-cast Al-5.7Si-2Cu-0.3Mg alloy changes from long and coarse plate-like grains to fine spherical shaped grain. The XRD plots confirmed the relatively high concentration of Al, Si, and Al2Cu in the heat treated Al-5.7%Si-2Cu%-0.3%Mg alloy relative to that of the as-cast alloy. The hardness of the T6 alloy also increased.

Microstructural and Vickers Microhardness Evolution of Heat Treated Secondary Aluminium Cast Alloy

2013 ◽  
Vol 586 ◽  
pp. 137-140 ◽  
Author(s):  
Lenka Hurtalová ◽  
Eva Tillová ◽  
Mária Chalupová
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Artificial Aging ◽  
Vickers Microhardness ◽  
Cast Alloy ◽  
Solution Treatment ◽  
Holding Time ◽  
Age Hardening ◽  
Structural Components ◽  
Heat Treated

Secondary aluminium alloys are made out of aluminium scrap and aluminium-processable waste by recycling. These alloys contain different alloying elements such as Al, Cu, Fe, Si and Mg that form intermetallic phases in aluminium matrix and influence on the microstructure, basic mechanical properties and microhardness evolution in aluminium cast alloy. As experimental material was used secondary aluminium cast alloy AlSi9Cu3. Material was subjected to heat treatment (age-hardening) consisting of a solution treatment at temperature 515 °C with holding time 4 hours, than water quenching at 40 °C and artificial aging by different temperature 130 °C, 150 °C and 170 °C with different holding time (2, 4, 8, 16 and 32 hours). The age-hardening led to changes in the morphology of structural components, but also leads to precipitation of finer hardening phases in the material substructure. As optimal age-hardening mode for secondary aluminium cast alloy AlSi9Cu3 was determined mode consisting of solution treatment at temperature 515 °C with holding time 4 hours and artificial aging at temperature 170 °C with holding time 16 hours. After this heat treatment cast alloy shows the best changes in microstructure and mechanical properties. These changes are comparable with changes by primary AlSi9Cu3 cast alloy.

Development, Microstructure and Corrosion Resistance of Al-Mg-(Si) Binary and Ternary System Samples in 5.3% NaCl Solution for Applications with Environmental Impact

2015 ◽  
Vol 1114 ◽  
pp. 239-244 ◽  
Author(s):  
Ileana Nicoleta Popescu ◽  
Maria Cristiana Enescu ◽  
Vasile Bratu ◽  
Raluca Ioana Zamfir ◽  
Elena Valentina Stoian
Keyword(s):  
Heat Treatment ◽  
Corrosion Resistance ◽  
Mechanical Characteristics ◽  
Structural Evolution ◽  
Tensile Tests ◽  
General Corrosion ◽  
Treatment Conditions ◽  
Heat Treated ◽  
Optimum Heat ◽  
Made In

For ensuring fuel consumption and pollution reduction, the researches made in the past decades considerable efforts to replacing steel with aluminum alloys in manufacturing auto bodies, or in naval transportation, because the promising weight saving. The researches consisted in general corrosion (the gravimetric index and the corrosion rate, Vcorr) and tensile tests (Rm, Rp0.2 and A5) in correlation with microstructure analysis of heat treated Al-Mg-(Si) system samples alloy, in order to obtain the best corrosion resistance and high mechanical characteristics. The Al alloys in extrusion state were solution treated at 510 – 545oC for 10-60 minutes, quenched in water 30-50o C and artificial aging at 150, 180 and 210°C at different time of aging (1, respectively 3, 7 and 11 hours). After heat treatment the obtained alloys were corroded in solution of 53g NaCl + 1000 ml distilled water and boiled in these solutions for 8, 16 respectively 24 hours. The gravimetric index was determinate by mass loss measurements for all types of heat treatment conditions. After corrosion test, samples were prepared for optical microstructural analyzing and mechanical tested. We have compared the obtained results on Al-Mg and Al-Mg-Si alloys. Were established (i) the optimum heat conditions parameters for obtaining of highest values of mechanical characteristics and corrosion resistance and also (ii) was explained the structural evolution during age (precipitation) hardening for both systems.

scholarly journals The Effect of Recrystallization on Creep Properties of Alloy IN939 Fabricated by Selective Laser Melting Process

Metals ◽  
2020 ◽  
Vol 10 (8) ◽  
pp. 1016 ◽  
Author(s):  
Santhosh Banoth ◽  
Chen-Wei Li ◽  
Yo Hiratsuka ◽  
Koji Kakehi
Keyword(s):  
Heat Treatment ◽  
Cast Alloy ◽  
Solution Treatment ◽  
Low Density ◽  
Laser Melting ◽  
Creep Life ◽  
Creep Properties ◽  
Treatment Conditions ◽  
Temperature Heat ◽  
Temperature Heat Treatment

In this research, we studied the creep properties of a selective laser melting (SLM)-processed γ′-strengthened IN939 superalloy along the building direction compared to a conventional cast alloy as a reference specimen. In the as-built condition, high-density dislocations were formed as a result of the SLM process due to the generation of the larger thermal gradient. Post-heat treatment was necessary to obtain specific mechanical properties to match industrial requirements. Two heat treatment conditions were used: the first was lower temperature heat treatment (LTH: solution treatment at 1160 °C/4 h + aging at 850 °C/16 h). The second was higher temperature heat treatment (HTH: solution treatment at 1240 °C/6 h + aging at 850 °C/16 h). Creep tests were conducted at 816 °C/250 MPa. The first and second heat treatment conditions were used for the SLM specimens, but only the first condition was used for the cast alloy (cast-LTH). The SLM specimens in the as-built and LTH conditions showed very poor creep life but good elongation. The poor creep life of the as-built specimen was caused by high dislocation density and the small recrystallized grains formed during testing. In the LTH specimen, poor creep life was due to the formation of the undesirable η phase at the grain boundary, as well as the formation of small recrystallized grains during testing. The creep life of the HTH specimen was 2.7 times longer compared to the LTH specimen. This was because these specimens were covered with recrystallized grains that included low-density dislocations, columnar grain morphology with random orientation, improvement in γ′ precipitate size, and elimination of undesirable η phase. The cast LTH specimen showed longer creep life than SLM specimens because of coarser grains with low-density dislocations, γ′ precipitate coarsening during the creep, and the presence of carbides at grain boundaries. In addition, the cast LTH specimen exhibited lower creep strain rate than SLM specimens also helped in creep life improvement.

Effect of copper incorporation on phase transformation behavior of electroless nickel–phosphorous coating and its effect on the tribological behavior

2020 ◽  
pp. 146442072098160
Author(s):  
Abhijit Biswas ◽  
Suman Kalyan Das ◽  
Prasanta Sahoo
Keyword(s):  
Heat Treatment ◽  
Phase Transformation ◽  
Tribological Behavior ◽  
Electroless Nickel ◽  
Two Phase ◽  
Microstructural Changes ◽  
Treatment Conditions ◽  
Heat Treated ◽  
Higher Temperature ◽  
Effect Of Copper

The microstructural changes of electroless Ni–P–Cu coating at various heat-treatment conditions are investigated to understand its implications on the tribological behavior of the coating. Coatings are heat-treated at temperatures ranging between 200°C and 800 °C and for 1–4 h duration. Ni–P–Cu coatings exhibit two-phase transformations in the temperature range of 350–450 °C and the resulting microstructural changes are found to significantly affect their thermal stability and tribological attributes. Hardness of the coating doubles when heat-treated at 452 °C, due to the formation of harder Ni3P phase and crystalline NiCu. Better friction and wear performance are also noted upon heat treatment of the coating at the phase transformation regime, particularly at 400 °C. Wear mechanism is characterized by a mixed adhesive cum abrasive wear phenomena. Heat treatment at higher temperature (600 °C and above) and longer duration (4 h) results in grain coarsening phenomenon, which negatively influences the hardness and tribological characteristics of the coating. Besides, diffusion of iron from the ferrous substrate as well as greater oxide formation are noticed when the coating is heat-treated at higher temperatures and for longer durations (4 h).

Mechanical Behavior of Friction Stir Welded AA-6061 Thick Plates in Different Heat Treatment Conditions

2021 ◽  
Vol 875 ◽  
pp. 203-210
Author(s):  
Talha Ahmed ◽  
Wali Muhammad ◽  
Zaheer Mushtaq ◽  
Mustasim Billah Bhatty ◽  
Hamid Zaigham
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Aging Treatment ◽  
Travel Speed ◽  
Butt Joint ◽  
Tensile Fracture ◽  
Friction Stir ◽  
Treatment Conditions ◽  
Heat Treated ◽  
Joint Form

In this study, mechanical properties of friction stir welded Aluminum Alloy (AA) 6061 in three different heat treatment conditions i.e. Annealed (O), Artificially aged (T6) and Post Weld Heat Treated (PWHT) were compared. Plates were welded in a butt joint form. Parameters were optimized and joints were fabricated using tool rotational speed and travel speed of 500 rpm and 350 mm/min respectively. Two sets of plates were welded in O condition and out of which one was, later, subjected to post weld artificial aging treatment. Third set was welded in T6 condition. The welds were characterized by macro and microstructure analysis, microhardness measurement and mechanical testing. SEM fractography of the tensile fracture surfaces was also performed. Comparatively better mechanical properties were achieved in the plate with PWHT condition.

Corrosion behavior of heat-treated and cryorolled Al 5052 alloys in different chloride ion concentrations

2020 ◽  
Vol 67 (1) ◽  
pp. 7-15 ◽  
Author(s):  
Anasyida Abu Seman ◽  
Ji Kit Chan ◽  
Muhammad Anas Norazman ◽  
Zuhailawati Hussain ◽  
Dhindaw Brij ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Corrosion Behaviour ◽  
Solution Treatment ◽  
Chloride Ion ◽  
Optical Microscope ◽  
Al Alloy ◽  
Content Type ◽  
Ion Concentrations ◽  
Heat Treated ◽  
Chloride Environment

Purpose This paper aims to investigate the corrosion behaviour of heat-treated and cryorolled Al 5052 alloys in different Cl− ion concentrations. Design/methodology/approach NaCl solutions with concentrations of 0, 0.5, 3.5 and 5.5 per cent were selected. Samples were subjected to pre-heat treatment (annealing at 300 °C and solution treatment at 540 °C) and cryorolling up to 30 per cent reduction before undergoing corrosion tests. The corrosion behaviour of the samples was then investigated by potentiodynamic polarization. The microstructure of the corroded samples was evaluated under an optical microscope, and the percentages of pits on their surfaces were calculated. Findings The cryorolled samples had a lower corrosion rate than the samples that were not cryorolled. The cryorolled sample that underwent solution treatment showed the highest corrosion resistance among all the samples tested. Practical implications The commercial impact of the study is the possibility of using the cryorolled Al alloy in various ion chloride environment. Originality/value The obtained results help in understanding the corrosion behaviour of cryorolled samples under different heat treatment conditions.

Effect of Double-Step Solution Treatment on Rejuvenation Heat Treated Microstructure of IN-738 Superalloy

2020 ◽  
Vol 856 ◽  
pp. 36-42
Author(s):  
Chuleeporn Paa-Rai
Keyword(s):  
Heat Treatment ◽  
Image Analysis ◽  
Electron Microscope ◽  
Solution Treatment ◽  
Single Step ◽  
Double Step ◽  
Heat Treated ◽  
Cast Superalloy ◽  
Scanning Electron

This work investigates the effect of rejuvenation heat treatment, with double-step solution treatment at the temperature from 1150 °C to 1200 °C, on the recovered microstructure of IN-738 cast superalloy. The superalloy has been long-term exposed as a turbine blade in a gas turbine prior to this study. After double solution treatment and aging at 845 °C for 12 h and 24 h, the recovered microstructures were examined by using a scanning electron microscope. Coarse γ΄ particles, that have presented in damaged microstructures, could not be observed in the samples after the rejuvenation heat treatment. In addition, the image analysis illustrates that the reprecipitated γ΄ particles in the samples with double-step solution treatments increase significantly in sizes during aging than that in the samples with the single-step solution treatment. Furthermore, the measurement of the samples hardness presents that the as-receive sample hardness is improved after rejuvenation heat treatment studied in this work.

Failure analysis of heat treated HSLA wheel bolt steels

2010 ◽  
Vol 6 (3) ◽  
pp. 373-382
Author(s):  
Ali Nazari ◽  
Shadi Riahi
Keyword(s):  
Heat Treatment ◽  
Tensile Strength ◽  
Failure Analysis ◽  
Heat Treating ◽  
Boron Steel ◽  
Content Type ◽  
Heat Treated ◽  
Before And After ◽  
Molybdenum Steel ◽  
Optimum Heat

PurposeThe aims of this study is to analyze failure of two types of high‐strength low‐alloy (HSLA) steels which are used in wheel bolts 10.9 grade, boron steel and chromium‐molybdenum steel, before and after heat treatment.Design/methodology/approachThe optimum heat treatment to obtain the best tensile behavior was determined and Charpy impact and Rockwell hardness tests were performed on the two steel types before and after the optimum heat treating.FindingsFractographic studies show a ductile fracture for heat‐treated boron steel while indicate a semi‐brittle fracture for heat‐treated chromium‐molybdenum steel. Formation of a small boron carbide amount during heat treating of boron steel results in increment the bolt's tensile strength while the ductility did not changed significantly. In the other hand, formation of chromium and molybdenum carbides during heat treating of chromium‐molybdenum steel increased the bolt's tensile strength with a considerable reduction in the final ductility.Originality/valueThis paper evaluates failure analysis of HSLA wheel bolt steels and compares their microstructure before and after the loading regime.

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