Ceramic Bonding to Biocompatible Titanium Alloys Obtained by Powder Metallurgy

2006 ◽  
Vol 530-531 ◽  
pp. 605-611
Author(s):  
M.C. Bottino ◽  
D.K. Oyafuso ◽  
Paulo Guilherme Coelho ◽  
Elisa B. Taddei ◽  
Vinicius André Rodrigues Henriques ◽  
...  
Keyword(s):  
Bond Strength ◽  
Titanium Alloys ◽  
Shear Bond Strength ◽  
Microstructural Analysis ◽  
Testing Machine ◽  
Phase Identification ◽  
Base Metals ◽  
Blended Elemental ◽  
Universal Testing ◽  
One Way Anova

The shear bond strength between a ceramic material (Titankeramik®, Vita Zahnfabrik, Germany) and two biocompatible titanium alloys was investigated. Ti-13%Nb-13%Zr (TNZ) and Ti-35%Nb-7%Zr-5%Ta (TNZT) alloys were obtained based on the blended elemental technique followed by a sequence of cold uniaxial and isostatic pressing and sintering. Characterization involved microstructural analysis (SEM) and crystalline phase identification (XRD). Subsequently, samples were machined to 4 x 4 mm with a base of 5 x 1 mm. The base metals were blasted with Al2O3 particles followed by the application of a coupling agent and opaque ceramic. After ceramic firing, the specimens were loaded in a universal testing machine (0,5mm/min). XRD revealed the presence of α and β-phases for TNZ, and peaks related to β phases and Nb and Ta for the TNZT alloy. SEM evaluation (TNZ) depicted remaining pores and biphasic microstructure formation. SEM micrographs of the TNZT alloy revealed good densification and a homogeneous β structure. Shear bond strength data (MPa) were statistically analyzed (one-way ANOVA and Tukey test, α=.05) revealing that TNZT (37.6 ± 2.91) presented significant higher values (p=0.0002) compared to TNZ (26.03 ± 2.92). In conclusion, it seems that Ti alloy composition plays a significant role on ceramic bonding.

scholarly journals Bond strength of glass-ceramic cemented to a zirconia structure: influence of adhesive cementation strategy

2016 ◽  
Vol 64 (2) ◽  
pp. 140-147
Author(s):  
Gilvan Cutrim TAVARES ◽  
Renan Macedo Cutrim TAVARES ◽  
Milton Edson MIRANDA ◽  
Cecilia Pedroso TURSSI ◽  
Roberta Tarkany BASTING ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
Adhesive System ◽  
Resin Cement ◽  
The Other ◽  
Universal Testing ◽  
Adhesive Cementation ◽  
Adhesive Cement ◽  
One Way Anova

ABSTRACT Objective This study evaluated the shear bond strength (SBS) of lithium disilicate glass (LDG) ceramic bonded to a zirconia (Y-TZP), using different cementation strategies. Methods LDG ceramic cylinders were cemented to Y-TZP structure according to the following adhesive system (AS)/resin cement (RC) (n = 15): U- self-adhesive dual-cure RC; AMBAR- AS containing phosphate monomers (PM) + dual-cure RC; group SBU: PM+Silane/AS + light-cure RC; group ALLB: PM/AS + dual-cure RC. Specimens were subjected to SBS in a universal testing machine (0.5 mm/min). Data (MPa) were subjected to one-way ANOVA and Tukey's test (α = 0,05). Results The groups SBU and ALLB had significantly higher SBS than those provided by the group U, in which the lowest values were observed. For the AMBAR group, intermediate SBS values were found, which did not differ significantly from the values observed in the other groups. Conclusion Regardless of resins cement, the use of adhesives containing phosphate monomers provided superior bond strength than self-adhesive cement.

scholarly journals Shear Bond Strength of Different Adhesive Materials used for Bonding Orthodontic Brackets : A Comparative in vitro Study

2015 ◽  
Vol 5 (1) ◽  
pp. 22-26
Author(s):  
Muzin Shahi Shaik ◽  
Snigdha Pattanaik ◽  
Sudhakar Pathuri ◽  
Arunachalam Sivakumar
Keyword(s):  
Bond Strength ◽  
Treatment Duration ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
Test Group ◽  
In Vitro Study ◽  
Universal Testing ◽  
Materials Used ◽  
Adhesive Materials

Introduction: Bond strength is an important property and determines the amount of force delivered and treatment duration in orthodontics. Many light-cured bonding materials are being used; but it is required to determine the most efficient one withdesired bond strength. Objective: To determine and compare the shear bond strength of three visible light-cured composites (Transbond XT, Heliositand Enlight) and two self-cured composites (Rely-a-bond and Concise). Materials & Method: 100 extracted premolars were collected and randomly divided into 5 test groups of different adhesives. Brackets were bonded to the teeth in each test group with the respective adhesive according to the manufacturer’s instructions. Each specimen was debonded using Universal Testing Machine and the shear bond strength for each specimen was calculated. All the groups were compared by ANOVA one-way test. Results: There were statistically significant differences among the five groups (P<0.05). The shear bond strength of Enlight (13.92 ± 3.92) is similar to Transbond XT (14.30 ± 4.35). Conclusion: Light cure composites showed higher bond strength than self cure composites.

scholarly journals Pengaruh Komposisi Glass Fiber Non Dental dan Penambahan Silane terhadap Kekuatan Geser Fiber Reinforced Composite sebagai Retainer Ortodonsi

2015 ◽  
Vol 1 (1) ◽  
pp. 53
Author(s):  
Dian Noviyanti Agus Imam ◽  
Siti Sunarintyas ◽  
Nuryono Nuryono
Keyword(s):  
Bond Strength ◽  
Glass Fiber ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
Fiber Reinforced ◽  
Fiber Reinforced Composite ◽  
Fiber Composition ◽  
Reinforced Composite ◽  
Universal Testing ◽  
Post Test

Retainer dibutuhkan untuk membantu menstabilkan posisi gigi geligi selama proses reorganisasi jaringan periodontal berlangsung. Retainer FRC ortodonsi dikembangkan sebagai alternatif material estetika serta aman bagi pasien alergi terhadap nikel. E-glass fiber lebih sering digunakan sebagai retainer ortodonsi. Penelitian ini bertujuan untuk mengkaji pengaruh komposisi glass fiber non dental dan penambahan silane terhadap kekuatan geser FRC sebagai retainer ortodonsi. Subjek penelitian terdiri dari 9 kelompok perlakuan dengan 3 jenis glass fiber yang berbeda yaitu glass fiber non dental A (LT, Cina), B (CMAX, Cina) dan C (HJ, Cina). Masing-masing glass fiber diberi perlakuan yang bervariasi yaitu tanpa penambahan silane, penambahan silane 1x dan 2x. Subjek penelitian direndam dalam akuades dan disimpan pada suhu 37ºC selama 24 jam sebelum dilakukan uji kekuatan geser dengan menggunakan alat Universal Testing Machine. Hasil penelitian dianalisis variansi dua jalur dan post hoc Tukey untuk mengetahui perbedaan statistik masing-masing kelompok. Hasil penelitian menunjukkan bahwa glass fiber non dental A dengan penambahan 2x silane memiliki rerata kekuatan geser tertinggi (12,72±2,02 MPa) sedangkan glass fiber non dental B tanpa penambahan silane memiliki rerata kekuatan geser terendah (6,96±1,69 MPa). Terdapat perbedaan bermakna antara komposisi fiber maupun penambahan silane terhadap kekuatan geser FRC (p<0,05). Tidak terdapat perbedaan bermakna pada letak kegagalan FRC (p>0,05). Berdasarkan hasil penelitian dapat disimpulkan bahwa komposisi SiO2 dan Al2O3 yang tinggi pada glass fiber non dental serta penambahan silane dapat meningkatkan kekuatan geser FRC. The Effect of Non Dental Glass Fiber Composition and Silane Addition on The Shear Bond Strength of Fiber Reinforced Composite as An Orthodontic Retainer. Retainers are required to stabilize the position of the teeth to permit reorganization of periodontal tissue. FRC orthodontic retainer was developed as an alternative material aesthetic and safe for nickel allergic patients. E-glass fiber is commonly used as an orthodontic retainer. The purpose of this study was to assess the effect of non dental glass fiber composition and silanes addition on the shear bond strength of the FRC as an orthodontic retainer. This study consisted of 9 treatment groups with three different types of non dental glass fiber, namely non dental glass fiber A (LT, China), B (CMAX, China) and C (HJ, China). Each glass fiber was given a variation treatment, without silanes, one time and two times of silanes addition. All the samples were stored in distilled water at 37ºC for 24 hours and subsequently tested for shear strength by using Universal Testing Machine.The groups were submitted to two way ANOVA analysis of variance with Tukey post test to verify the statictical difference between groups. The results showed that a non dental glass fiber A with two times of silanes addition has the highest shear bond strength (12,72±2,02 MPa), meanwhile a non dental glass fiber B without silane addition has the lowest shear bond strength (6,96±1,69 MPa). There were significant differences between the composition of glass fiber and the addition of silane toward the shear bond strength of FRC (p<0,05). No significant differences in debonded locations of FRC (p>0,05). Based on the results of this study concluded that the composition of the high SiO2 and Al2O3 in the non dental glass fiber  and the silanes addition can increase the shear bond strength FRC.

scholarly journals Perbedaan Kekuatan Geser Reparasi Gigi Tiruan Cekat dengan Resin Komposit Packable dan Flowable (Uji Laboratoris pada permukaan logam NiCr)

2012 ◽  
Vol 19 (2) ◽  
pp. 102
Author(s):  
Endang Wahyuningtyas ◽  
Suparyono Saleh ◽  
Sri Budi Barunawati
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Composite Resin ◽  
Testing Machine ◽  
Composite Resins ◽  
Distilled Water ◽  
Research Subjects ◽  
Flowable Composite ◽  
Diamond Bur ◽  
Universal Testing

Latar Belakang. Resin komposit merupakan bahan pilihan untuk reparasi Gigi Tiruan Cekat porcelain fused to metal (PFM) Karena estetis baik dan manipulasi mudah. Tujuan penelitian ini adalah mengetahui perbedaan kekuatan geser perlekatan resin komposit pada permukaan logam Gigi Tiruan Cekat dengan menggunakan resin komposit jenis packable dan jenis flowable. Metode penelitian. Subjek penelitian berupa logam NiCr (Noritake, Japan) berbentuk silinder dengan diameter 10 mm dan tinggi 3 mm. Penelitian dibagi menjadi dua kelompok, masing-masing terdiri dari 10 subjek. Kelompok pertama reparasi dengan resin komposit packable (Z250™ 3M ESPE, USA) dan kelompok kedua reparasi dengan resin komposit flowable (Dyad flow, Kerr, USA). Permukaan subjek dikasari dengan wheel diamond bur, dietsa dengan asam fosfat 37 % (Scotchbond™, 3M ESPE, USA) kemudian dicuci dan dikeringkan, selanjutnya diaplikasikan silan (Rely X™ Ceramic Primer, 3M ESPE, USA) dan bonding (Adper™ Single Bond, 3M ESPE, USA). Permukaan kemudian dilapisi dengan resin komposit packable dan flowable, disinari selama 40 detik. Subjek penelitian direndam di dalam distilled water dan dimasukkan ke dalam incubator dengan suhu 37°C selama 7 hari. Uji kekuatan geser dilakukan dengan menggunakan Universal Testing Machine. Data dianalisis dengan uji t. hasil uji t menunjukkan terdapat perbedaan bermakna kekuatan geser reparasi gigi tiruan cekat pada permukaan logam (p<0,05). Kesimpulan penelitian ini adalah kekuatan geser reparasi pada permukaan logam dengan menggunakan resin komposit flowable yang mengandung bahan coupling agent lebih tinggi dibandingkan reparasi pada permukaan porselen dengan menggunakan resin komposit packable. Background. One of selected material by repairing the fixed partial denture was composite resin because of its good aesthetics and low manipulation. The aim. This research was aimed at identifying the differences of shear bond strength of composite resin on metal surface by using different composite resins, namely packable and flowable composite resins. Method. The research subjects were cylinders with 10 mm in diameter and 3 mm in height. The research subjects with metal material of NiCr (Noritke, Japan) involved two groups. The first group comprising 10 repair subjects with composite packable (Z250™, 3M ESPE, USA) and 10 repair subjects with flowable composite (Dyad flow, Kerr, USA). The surface of the subjects were roughned with wheel diamond bur and etched with 37% phosphate acid (Scotbond™, 3M ESPE, USA) were applied. The surface was then coated with packable and flowable composite resins and light-cured for 40 seconds. The research subjects were immersed in distilled water and put into the incubator at temperature of 37°C for 7 days. The shear bond strength test was conducted using the Universal Testing Machine. Data were analyzed using t-test. The result. The research result showed that there were differences of shear bond strength of repair between packable and flowable composite resins. The result of t-test indicated significant diffrences on metal surface (p<0,05). The conclusion of this research is that shear bond strength of repair with flowable composite which contain coupling agent has higher shear bond strength than that of packable composite resin.

scholarly journals Reconditioning of self-ligating brackets

2011 ◽  
Vol 82 (1) ◽  
pp. 158-164 ◽  
Author(s):  
Maria Francesca Sfondrini ◽  
Esmeralda Xheka ◽  
Andrea Scribante ◽  
Paola Gandini ◽  
Giuseppe Sfondrini
Keyword(s):  
Statistical Analysis ◽  
Bond Strength ◽  
Null Hypothesis ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
Shear Mode ◽  
Universal Testing ◽  
Adhesive Remnant Index ◽  
Significant Difference ◽  
Scanning Electron

Abstract Objective: To test the null hypothesis that there is no significant difference in the shear bond strength (SBS) and Adhesive Remnant Index (ARI) scores of new vs reconditioned self-ligating brackets. Materials and Methods: One hundred and twenty permanent extracted bovine teeth were embedded in resin blocks. Three different new and reconditioned self-ligating orthodontic brackets (Smart Clip [3M Unitek]; Quick [Forestadent]; and Damon3MX [Ormco]) were tested. Scanning electron microphotographs of the different new (groups 1, 3, and 5) and reconditioned (groups 2, 4, and 6) bracket bases were taken before starting the experiments. Brackets were then bonded to the teeth using an orthodontic adhesive and were then tested in shear mode using an Instron Universal Testing Machine. ARI scores were then recorded. Statistical analysis was performed to determine significant differences in SBS and ARI Scores. Results: Smart Clip and Damon3MX reconditioned brackets showed significantly lower SBS than did new ones. On the contrary, Quick reconditioned brackets showed significantly higher SBS than did new ones. No significant differences in ARI scores were found after the reconditioning process for the three different brackets tested. Conclusion: The in-office reconditioning procedure alters the SBS of self-ligating brackets, although SBS values still remain clinically acceptable.

scholarly journals Shear Bond Strengths and Morphological Evaluation of Filled and Unfilled Adhesive Interfaces to Enamel and Dentine

2012 ◽  
Vol 2012 ◽  
pp. 1-9 ◽  
Author(s):  
Vajihesadat Mortazavi ◽  
Mohammadhosein Fathi ◽  
Ebrahim Ataei ◽  
Niloufar Khodaeian ◽  
Navid Askari
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Testing Machine ◽  
The Other ◽  
Adhesive Systems ◽  
Morphological Evaluation ◽  
Bond Strengths ◽  
Post Hoc ◽  
One Way Anova

In this laboratory study shear bond strengths of three filled and one unfilled adhesive systems to enamel and dentine were compared. Forty-eight extracted intact noncarious human mandibular molars were randomly assigned to two groups of 24 one for bonding to enamel and the other for bonding to dentine. Buccal and lingual surfaces of each tooth were randomly assigned for application of each one of filled (Prime & Bond NT (PBNT), Optibond Solo Plus (OBSP), and Clearfil SE Bond (CSEB)) and unfilled (Single Bond (SB)) adhesive systems (n=12). A universal resin composite was placed into the translucent plastic cylinders (3 mm in diameter and 2 mm in length) and seated against the enamel and dentine surfaces and polymerized for 40 seconds. Shear bond strength was determined using a universal testing machine, and the results were statistically analyzed using two-way ANOVA, one-way ANOVA,t-test, and Tukey HSD post hoc test with a 5% level of significance.There were no statistically significant differences in bond strength between the adhesive systems in enamel, but CSEB and SB exhibited significantly higher and lower bond strength to dentine, respectively, than the other tested adhesive systems while there were no statistically significant differences between PBNT and OBSP.

The effect of caries detector dyes and a cavity cleansing agent on composite resin bonding to enamel and dentin

2001 ◽  
Vol 25 (1) ◽  
pp. 57-63 ◽  
Author(s):  
Azza El-Housseiny ◽  
Hana Jamjoum
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Composite Resin ◽  
Testing Machine ◽  
Group Iv ◽  
Acid Etching ◽  
Group V ◽  
Universal Testing ◽  
Group I ◽  
Significant Difference

This study was undertaken to evaluate the effect of caries detector dyes and/or cavity cleanser on composite bonding and etching patterns of enamel and dentin. One hundred and eight non-carious premolars were divided into six groups according to the enamel and dentin pretreatment investigated. The different pretreatment were as follows: Group I: teeth with prophylaxis only, Group II: Sable seek caries detector dye,Groups III: chlorhexidine cavity cleanser,Group IV: the caries detectors dye followed by prophylaxis, Group V: the cavity cleanser followed by the caries detector dye, and Group IV: Snoop caries detector dye. The shear bond strength of composite resin bonded to enamel and dentin was evaluated by the Instron Universal testing machine while, the topographic details of enamel and dentin were examined by the SEM following the different pretreatment and acid etching. Results of the shear bond strength showed no statistically significant difference among the six groups, with no substantial differences in SEM results. It is concluded that using the caries detector dyes and/or chlorhexidine cavity cleanser before acid etching does not significantly affect composite bonding to enamel and dentin.

scholarly journals Evaluation of the shear bond strength of the union between two CoCr-alloys and a dental ceramic

2004 ◽  
Vol 12 (4) ◽  
pp. 280-284 ◽  
Author(s):  
Mariana Pretti ◽  
Edson Hilgert ◽  
Marco Antônio Bottino ◽  
Rander Pereira Avelar
Keyword(s):  
Shear Strength ◽  
Standard Deviation ◽  
Bond Strength ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
Casting Technique ◽  
Universal Testing ◽  
Significant Difference ◽  
Metal Ceramic ◽  
The Mean

INTRODUCTION: Based on the importance of the integrity of the metal/ceramic interface, the purpose of this work was to evaluate the shear bond strength of the metal-ceramic union of two Co-Cr alloys (Wirobond C, Bego; Remanium 2000, Dentaurum) combined with Omega 900 ceramic (Vita Zahnfabrik). MATERIAL AND METHOD: Eleven cylindrical matrixes were made for each alloy, and the metallic portion was obtained with the lost wax casting technique with standardized waxing of 4mm of height and of 4mm of diameter. The ceramic was applied according to the manufacturer's recommendations with the aid of a teflon matrix that allowed its dimension to be standardized in the same size as the metallic portion. The specimens were submitted to the shear bond test in an universal testing machine (EMIC), with the aid of a device developed for such intention, and constant speed of 0.5mm/min. RESULTS AND CONCLUSIONS: The mean resistance was 48.387MPa for Wirobond C alloy, with standard deviation of 17.718, and 55.956MPa for Remanium 2000, with standard deviation of 17.198. No statistically significant difference was observed between the shear strength of the two metal-ceramic alloys.

Effect of Adhesive Boosters on Bond Strength of Bleached Teeth in Orthodontic Bonding

2021 ◽  
pp. 030157422110044
Author(s):  
I Ranganayakulu ◽  
D Praveen Kumar Varma ◽  
Padma Priya CV ◽  
RSVM Raghu Ram ◽  
K Anand Viswanadh ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
Orthodontic Brackets ◽  
Carbamide Peroxide ◽  
Universal Testing Machine ◽  
Universal Testing ◽  
Significant Difference ◽  
Maxillary Premolars ◽  
And Control

Objectives: To evaluate and compare the effect of adhesion boosters on shear bond strength (SBS) of orthodontic brackets on bleached teeth. Materials and Methods: A sample of 90 extracted maxillary premolars was equally divided into 2 groups of bleached and non-bleached teeth. Twenty-two percent carbamide peroxide gel was used as an agent for bleaching. Each group was further divided equally into 3 subgroups depending on the type of adhesive booster used (Enhance LC, All-bond 2, and no adhesive booster [control]) and maxillary premolars brackets were bonded. Debonding was done with a universal testing machine, and the SBS was recorded. Results: The SBS of non-bleached teeth was highest for All-bond 2 (14.78 ± 2.47 MPa) followed by Enhance LC (13.15 ± 3.49 MPa) and control (10.30 ± 1.06 MPa). The SBS of bleached teeth was highest for All bond 2 (12.23 ± 1.41 MPa) followed by Enhance LC (11.76 ± 1.71 MPa) and control (9.63 ± 1.06 MPa). All subgroups showed a significant difference in SBS (P = .000) on bleached and non-bleached teeth. The SBS showed a significant difference between the bleached and non-bleached teeth in All-bond 2 group (P = .019). Conclusion: Adhesive boosters increased the SBS of both bleached and non-bleached teeth significantly. Among the two adhesive boosters used, All-bond 2 showed more SBS values.

scholarly journals Do Products Preventing Demineralization Around Orthodontic Brackets Affect Adhesive Bond Strength?

2018 ◽  
Vol 12 (1) ◽  
pp. 1029-1035
Author(s):  
Bennett T. Amaechi ◽  
Kaveh Najibfard ◽  
Irene P. Chedjieu ◽  
Hariyali Kasundra ◽  
Linda O. Okoye
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
Adhesive Bond ◽  
Orthodontic Brackets ◽  
Adhesive Systems ◽  
Lesion Formation ◽  
Universal Testing ◽  
Priming Enamel ◽  
Resin Sealant

Objective: This study investigated the effects, on the shear bond strength of orthodontic brackets, of using an antimicrobial selenium-containing sealant (DenteShieldTM) to serve dual functions of priming enamel prior to bonding and as a protective barrier against whitespot lesion formation. Materials and Methods: A total of 150 extracted human premolars were randomly assigned into 10 groups (n=15/group). Stainless steel brackets were bonded with two adhesive systems (DenteShieldTM or Transbond XT) after the enamel was conditioned with a primer (DenteShieldTM or Assure Universal) or a filled resin sealant (DenteShieldTM, Pro SealTM or Opal SealTM). The specimens were stored in deionized water at 37 °C for 24 hours and debonded with a universal testing machine. Results: The use of DenteShieldTM adhesive to bond orthodontic brackets to the enamel surface resulted in a significantly lower (P<0.05), but clinically acceptable, shear bond strength (mean & SD: 14.5±1.6 MPa) as compared with Transbond XT group (mean & SD: 19.3±1.7 MPa). DenteShieldTM sealant used as primer resulted in shear bond strength values comparable to those of Pro SealTM and Opal SealTM. All adhesive-sealant and primer-sealant combinations tested in this study exhibited shear bond strength values greater than 9.6 MPa, sufficient for clinical orthodontic needs. Conclusion: DenteShieldTM sealant can serve as primer as well as anti-demineralization sealant during orthodontic treatment without adversely affecting the shear bond strength of the bracket.

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