Effect of Dislocation Distribution on the Yielding of Highly Dislocated Iron

2007 ◽  
Vol 539-543 ◽  
pp. 228-233 ◽  
Author(s):  
Setsuo Takaki ◽  
Y. Fujimura ◽  
Koichi Nakashima ◽  
Toshihiro Tsuchiyama

Yield strength of highly dislocated metals is known to be directly proportional to the square root of dislocation density (ρ), so called Bailey-Hirsch relationship. In general, the microstructure of heavily cold worked iron is characterized by cellar tangled dislocations. On the other hand, the dislocation substructure of martensite is characterized by randomly distributed dislocations although it has almost same or higher dislocation density in comparison with heavily cold worked iron. In this paper, yielding behavior of ultra low carbon martensite (Fe-18%Ni alloy) was discussed in connection with microstructural change during cold working. Originally, the elastic proportional limit and 0.2% proof stress is low in as-quenched martensite in spite of its high dislocation density. Small amount of cold rolling results in the decrease of dislocation density from 6.8x1015/m-2 to 3.4x1015/m-2 but both the elastic proportional limit and 0.2% proof stress are markedly increased by contraries. 0.2% proof stress of cold-rolled martensite could be plotted on the extended line of the Bailey-Hirsch equation obtained in cold-rolled iron. It was also confirmed that small amount of cold rolling causes a clear microstructural change from randomly distributed dislocations to cellar tangled dislocations. Martensite contains two types of dislocations; statistically stored dislocation (SS-dislocation) and geometrically necessary dislocation (GN-dislocation). In the early deformation stage, SS-dislocations easily disappear through the dislocation interaction and movement to grain boundaries or surface. This process produces a plastic strain and lowers the elastic proportional limit and 0.2% proof stress in the ultra low carbon martensite.

2006 ◽  
Vol 503-504 ◽  
pp. 627-632 ◽  
Author(s):  
Koichi Nakashima ◽  
M. Suzuki ◽  
Y. Futamura ◽  
Toshihiro Tsuchiyama ◽  
Setsuo Takaki

The limit of dislocation density was investigated by means of mechanical milling (MM) treatment of an iron powder. Mechanical milling enabled an ultimate severe deformation of iron powder particles and dislocation density in the MM iron powder showed the clear saturation at around the value of 1016m-2. On the other hand, the relation between hardness and dislocation density was examined in cold-rolled iron sheets, and the linear Bailey-Hirsch relationship; HV[GPa]=0.7+3×10-8ρ1/2 was obtained in the dislocation density region up to 3×1015m-2. Extrapolation of the Bailey-Hirsch relationship indicated that the dislocation strengthening should be limited to about 3.7GPa in Vickers hardness which corresponds to about 1.1GPa in 0.2% proof stress.


2008 ◽  
Vol 137 ◽  
pp. 155-162 ◽  
Author(s):  
Agnieszka Mielczarek ◽  
Yvonne Wöckel ◽  
Werner Riehemann

The ductility of Cu – Al – Mn shape memory alloys at room temperature depends on the aluminium content. High aluminium contents make Cu – Al – Mn very brittle and unsuitable for plastic shaping. Two Cu – Al – Mn shape memory alloys were investigated. The ductile alloy CuAl7.8Mn9.5 (all contents in wt. %) could be easily cold rolled by 86 %. The alloy CuAl12Mn4.3 could be cold rolled by only 12 - 14 %. The amplitude dependence of damping of austenitic specimens increased with increasing degree of cold work, whereas the damping of martensiticaustenitic specimens decreased. These observations can be explained by the creation of stress induced martensite and therefore by new moveable interfaces like phase- and twin boundaries, which contribute to damping. Plastic deformation increases the dislocation density, too. Both the increase of dislocation density and the increase of martensite content can lead to a decrease of damping mainly for high deformation degrees. Same shape memory alloys have shown negligible hardness increase during cold rolling, too. This behaviour, untypical for metals, can be explained by the generation of new martensite and by the fact that the hardness of martensite is smaller than the hardness of austenite. Some aging effects of the specimen after cold rolling, which lead to decrease of damping, were detected. This can be explained by pinning of moveable interfaces by point defects and/or retransformation of martensite into austenite.


2013 ◽  
Vol 753 ◽  
pp. 201-206
Author(s):  
Ranjit K. Ray ◽  
Rajib Saha

Less attention has been paid to study the recrystallization and grain growth behavior of severe plastically deformed (SPD) metals specially steels that are deformed to very high strain by conventional rolling method. Present work has been focused on systematic investigation of recrystallization and grain growth behavior of a Aluminium Killed (AK), an Interstitial Free (IF) and an Interstitial Free High Strength (IFHS) steels that were subjected to very high levels of strain (ԑeqv= 4.51) by cold rolling. The cold rolled steels show fine lamellar structure with very strong texture consists of both γ and α fibre. All the steels show formation of ultrafine grains and dramatic rise in the intensity of α fibre component in the early stages of annealing. However, progress of annealing for longer time leads to an increase in the mean grain size as well as γ fibre intensity. The results also indicate that the heavily cold rolled material exhibit selective growth of specific texture components.It appears that microstructure and texture is closely related to the observed phenomenon.


2007 ◽  
Vol 550 ◽  
pp. 491-496
Author(s):  
Kim Verbeken ◽  
Leo Kestens

The scope of this work was to study the physical metallurgical behaviour of the microstructure and the texture of ultra low carbon (ULC) steel during cold rolling and subsequent thermally activated phenomena. It was the intention to contribute to the scientific search for the answer to many open questions raised in recent literature. The powerful tool of quantitative texture analysis, together with modern measurement equipment was used for this purpose. At first, a ULC steel was cold rolled to two different rolling reductions and the local strain heterogeneities after the cold rolling were studied. Secondly, crystallographic orientation selection during primary recrystallization was considered both for cold rolled ULC steel and for a Fe-2.8%Si single crystal. The latter was a re-evaluation of the historic growth selection experiment by Ibe and Lücke. Finally, secondary recrystallization in ULC steels was evaluated in terms of oriented nucleation and selective growth.


1978 ◽  
Vol 3 (1) ◽  
pp. 53-72 ◽  
Author(s):  
Kazuo Matsudo ◽  
Takayoshi Shimomura ◽  
Osamu Nozoe

The effects of carbide size prior to cold rolling, cold reduction and heating rate in annealing on r¯-value, and texture of cold-rolled steel sheets were investigated. The main results obtained were as follows: (1) When the carbide size prior to cold rolling is large, r¯-value can be improved with a faster heating rate in annealing. (2) Moreover, the cold reduction of peak r¯-value shifts to the higher cold reduction side, and r¯-value tends to increase with cold reduction up to 90%. These phenomena are thought to be based on the delay in dissolution of carbide at the initial state of recrystallization, the change in recrystallization temperature and the preferred nucleation.


2011 ◽  
Vol 121-126 ◽  
pp. 458-462
Author(s):  
Zi Li Jin ◽  
Hui Ping Ren ◽  
Rong Wang

In this item, the low carbon steel hot sheets by compact strip production (CSP) technology were cold rolled and annealed in laboratory. texture evolution during the production process of CSP-cold rolled strip were investigated by means of the XRD. The results were as follows: After hot deformation of thin slab formed a strong γ- fibre orientation texture, the density of texture increase with the cold rolled reduction increased, especially for the negative texture {100}, in γ-fibre orientation cold rolling texture density has no significant change. Compared to the traditional process, hot rolled steel sheet has higher texture, cold-rolled steel sheet has the same texture, and after-annealing sheet has further higher texture in the CSP-cold rolling process. This study enables better understanding and control on the evolution of textures the cold-rolled steel sheet processed by CSP technique and provides theory support for exploiting the CSP the cold-rolling deep drawing steel sheet


2018 ◽  
Vol 104 (11) ◽  
pp. 683-688 ◽  
Author(s):  
Setsuo Takaki ◽  
Takuro Masumura ◽  
Fulin Jiang ◽  
Toshihiro Tsuchiyama

2007 ◽  
Vol 345-346 ◽  
pp. 189-192 ◽  
Author(s):  
Koichi Nakashima ◽  
Y. Fujimura ◽  
Toshihiro Tsuchiyama ◽  
Setsuo Takaki

The work hardening behavior by cold rolling was investigated in ultralow carbon and low carbon martensitic steels containing 12%Cr or 18%Ni, and then the effect of carbon on the work hardening behavior was discussed in terms of the change in dislocation density and the microstructure development during deformation. In the ultralow carbon steel, the hardness is almost constant irrespective of the reduction ratio. On the other hand, the low carbon steel exhibits marked work hardening. The dislocation density of these specimens was confirmed to be never increased by cold rolling. It was also found that cold rolling gives no significant influence on the morphology of martensite packet and block structure. TEM images of the cold-rolled steels revealed that the martensite laths in the ultralow carbon steel are partially vanished, while those in the carbon bearing steel are stably remained. These results indicate that the solute carbon retards the movement of dislocations, which results in the high work hardening rate through the formation of fine dislocation substructure within laths.


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