scholarly journals Thermodynamic model of freeze-drying of poultry breast using infrared thermography

2018 ◽  
Author(s):  
Pedro J Fito ◽  
Juan Angel Tomas-Egea ◽  
Marta Castro-Giraldez
Keyword(s):  
Infrared Thermography ◽  
Thermodynamic Model ◽  
Freeze Drying ◽  
Thermal Infrared ◽  
Irreversible Thermodynamic ◽  
Main Process ◽  
Drying Process ◽  
Physico Chemical ◽  
Thermographic Camera ◽  
Swelling Mechanism

Food dehydration is one of a main process to preserve meal. In order to optimaze a freeze-drying operation a physic model is needed to well describe the thermodynamic behaviors involved in this process. In this work, a thermographic camera and different physico-chemical determinations are used to monitor many phenomena that occur during the lyophilization of poultry breast. Finally, a non-continuous irreversible thermodynamic model, based on thermal infrared measures and in shrinkage/swelling mechanism, has been developed, wich explains the behaviours produced throughout the meat freeze-drying process. Keywords: freeze-drying, thermodynamic model, infrared thermography, poultry.

Evaluation of physico-chemical properties of tomato powder produced by an optimized freeze drying process

2021 ◽  
Vol 0 (0) ◽  
Author(s):  
Zeyu Wu ◽  
Haiyan Wang ◽  
Li Zhang ◽  
Zhaojun Xian ◽  
Honghong Li ◽  
...  
Keyword(s):  
Ascorbic Acid ◽  
Freeze Drying ◽  
Binding Capacity ◽  
Chemical Properties ◽  
Soluble Solids ◽  
Drying Process ◽  
Total Acid ◽  
Physico Chemical ◽  
Freeze Dried ◽  
Tomato Powder

Abstract In this study, the physico-chemical properties of tomato powder produced by an optimized freeze drying process (FDP) were evaluated. With the lycopene content as the dependent variable, the optimum FDP conditions (i.e., thermal cracking time of 62 s, ascorbic acid addition amount [0.13%], and particle size [Dv90] of 163 μm) were obtained through response surface methodology (RSM). The results showed that the content of lycopene in the prepared tomato powder was higher than that in two commercial products. Aldehydes were the main components among 25 kinds of aromatic substances detected in tomato powder. The values of a * and a */b *, the hydration properties including water holding capacity (WHC) and oil binding capacity (OBC), and the content of total acid, ascorbic acid, and soluble solids were improved compared to commercial spray dried and freeze dried samples. All the above results suggested that FDP was an adequate procedure for the production of high-quality tomato powder.

scholarly journals Reconstitution properties of biologically active polymersomes after cryogenic freezing and a freeze-drying process

RSC Advances ◽  
2018 ◽  
Vol 8 (45) ◽  
pp. 25436-25443 ◽  
Author(s):  
Robert Ccorahua ◽  
Silvia Moreno ◽  
Hannes Gumz ◽  
Karin Sahre ◽  
Brigitte Voit ◽  
...  
Keyword(s):  
Membrane Permeability ◽  
Freeze Drying ◽  
Chemical Properties ◽  
Biologically Active ◽  
Enzymatic Reactions ◽  
Drying Process ◽  
Physico Chemical ◽  
And Storage

Polymersomes can retain their physico-chemical properties and membrane permeability for enzymatic reactions after lyophilization or cryogenic freezing and storage.

scholarly journals Thermodynamic model of Ca(II)-alginate beads drying by spectrophotometry

2018 ◽  
Author(s):  
Pedro J Fito ◽  
Patricio R. Santagapita ◽  
Marta Castro-Giraldez ◽  
Maria Victoria Traffano-Schiffo
Keyword(s):  
Heat Transfer ◽  
Infrared Thermography ◽  
Critical Points ◽  
Thermodynamic Model ◽  
Alginate Beads ◽  
Thermal Imager ◽  
Colloidal Systems ◽  
Drying Process ◽  
Monitoring Tool ◽  
Mechanical Phenomena

The purpose of this work was to study the drying process of Ca(II)-alginate beads with/without sucrose, monitored by infrared thermography (IRT), in order to describe the critical points and the transformations suffered by the systems. Beads were obtained by the drop method and the drying process was performed at 40 ºC and 1.5 m/s. IRT was measured by a thermal imager Optris PI® 160. Mass, aw, xw and volume were also obtained. It was demonstrated that IRT is a good monitoring tool, able to analyzed heat transfer in colloidal systems. A thermodynamic model able to predict the mechanical phenomena of the beads throughout drying process has been developed. Keywords: encapsulation; thermodynamic; spectrophotometry; drying; beads

scholarly journals On the Use of Infrared Thermography for Monitoring a Vial Freeze-Drying Process

2019 ◽  
Vol 108 (1) ◽  
pp. 391-398 ◽  
Author(s):  
Elena Lietta ◽  
Domenico Colucci ◽  
Giovanni Distefano ◽  
Davide Fissore
Keyword(s):  
Infrared Thermography ◽  
Freeze Drying ◽  
Drying Process

Video real-time imaging of artificial membranes during freeze-drying by cryo-electron microscopy

1988 ◽  
Vol 46 ◽  
pp. 16-17
Author(s):  
Alan S. Rudolph ◽  
Ronald R. Price
Keyword(s):  
Real Time ◽  
Self Assembly ◽  
Freeze Drying ◽  
Video Capture ◽  
Drying Process ◽  
Artificial Membranes ◽  
The Past ◽  
Cryo Electron Microscopy ◽  
Spherical Structures ◽  
Capture Techniques

We have employed cryoelectron microscopy to visualize events that occur during the freeze-drying of artificial membranes by employing real time video capture techniques. Artificial membranes or liposomes which are spherical structures within internal aqueous space are stabilized by water which provides the driving force for spontaneous self-assembly of these structures. Previous assays of damage to these structures which are induced by freeze drying reveal that the two principal deleterious events that occur are 1) fusion of liposomes and 2) leakage of contents trapped within the liposome [1]. In the past the only way to access these events was to examine the liposomes following the dehydration event. This technique allows the event to be monitored in real time as the liposomes destabilize and as water is sublimed at cryo temperatures in the vacuum of the microscope. The method by which liposomes are compromised by freeze-drying are largely unknown. This technique has shown that cryo-protectants such as glycerol and carbohydrates are able to maintain liposomal structure throughout the drying process.

scholarly journals Environmentally Friendly and Multifunctional Shaddock Peel-Based Carbon Aerogel for Thermal-Insulation and Microwave Absorption

2021 ◽  
Vol 13 (1) ◽  
Author(s):  
Weihua Gu ◽  
Jiaqi Sheng ◽  
Qianqian Huang ◽  
Gehuan Wang ◽  
Jiabin Chen ◽  
...  
Keyword(s):  
Microwave Absorption ◽  
Thermal Insulation ◽  
Freeze Drying ◽  
Thermal Infrared ◽  
Carbon Aerogel ◽  
Carbon Aerogels ◽  
List Type ◽  
Drying Method ◽  
Cross Sectional ◽  
Compression Resistance

Highlights The eco-friendly shaddock peel-derived carbon aerogels were prepared by a freeze-drying method. Multiple functions such as thermal insulation, compression resistance and microwave absorption can be integrated into one material-carbon aerogel. Novel computer simulation technology strategy was selected to simulate significant radar cross-sectional reduction values under real far field condition. . Abstract Eco-friendly electromagnetic wave absorbing materials with excellent thermal infrared stealth property, heat-insulating ability and compression resistance are highly attractive in practical applications. Meeting the aforesaid requirements simultaneously is a formidable challenge. Herein, ultra-light carbon aerogels were fabricated via fresh shaddock peel by facile freeze-drying method and calcination process, forming porous network architecture. With the heating platform temperature of 70 °C, the upper surface temperatures of the as-prepared carbon aerogel present a slow upward trend. The color of the sample surface in thermal infrared images is similar to that of the surroundings. With the maximum compressive stress of 2.435 kPa, the carbon aerogels can provide favorable endurance. The shaddock peel-based carbon aerogels possess the minimum reflection loss value (RLmin) of − 29.50 dB in X band. Meanwhile, the effective absorption bandwidth covers 5.80 GHz at a relatively thin thickness of only 1.7 mm. With the detection theta of 0°, the maximum radar cross-sectional (RCS) reduction values of 16.28 dB m2 can be achieved. Theoretical simulations of RCS have aroused extensive interest owing to their ingenious design and time-saving feature. This work paves the way for preparing multi-functional microwave absorbers derived from biomass raw materials under the guidance of RCS simulations.

scholarly journals Strengthening of Porcine Plasma Protein Superabsorbent Materials through a Solubilization-Freeze-Drying Process

Polymers ◽  
2021 ◽  
Vol 13 (5) ◽  
pp. 772
Author(s):  
Estefanía Álvarez-Castillo ◽  
Carlos Bengoechea ◽  
Antonio Guerrero
Keyword(s):  
Water Uptake ◽  
Plasma Protein ◽  
Freeze Drying ◽  
Meat Industry ◽  
Drying Process ◽  
Uptake Capacity ◽  
Water Uptake Capacity ◽  
Protein Flour ◽  
Hydrophilic Materials ◽  
By Products

The replacement of common acrylic derivatives by biodegradable materials in the formulation of superabsorbent materials would lessen the associated environmental impact. Moreover, the use of by-products or biowastes from the food industry that are usually discarded would promote a desired circular economy. The present study deals with the development of superabsorbent materials based on a by-product from the meat industry, namely plasma protein, focusing on the effects of a freeze-drying stage before blending with glycerol and eventual injection molding. More specifically, this freeze-drying stage is carried out either directly on the protein flour or after its solubilization in deionized water (10% w/w). Superabsorbent materials obtained after this solubilization-freeze-drying process display higher Young’s modulus and tensile strength values, without affecting their water uptake capacity. As greater water uptake is commonly related to poorer mechanical properties, the proposed solubilization-freeze-drying process is a useful strategy for producing strengthened hydrophilic materials.

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