Wear-Resistance Improvement of 65Mn Low-Alloy Steel through Adjusting Grain Refinement by Cyclic Heat Treatment

Refined microstructures achieved by cyclic heat treatment significantly contribute to improving the wear resistance of steels. To acquire the refined microstructures of 65Mn low-alloy steel, first, the specimens were solid solution-treated; then, they were subjected to cyclic heat treatment at cyclic quenching temperatures of 790–870 °C and quenching times of 1–4 with a fixed holding time of 5 min. The mechanical properties of 65Mn low-alloy steel in terms of hardness, tensile strength, elongation and wear resistance were characterized. Afterwards, the effect of cyclic heat treatment on microstructure evolution and the relationships between grain refinement and mechanical properties’ improvement were discussed. The results show that the average grain size firstly decreased and then increased with the increase in the quenching temperature. Hardness increased with grain refinement when the temperature was lower than 830 °C. Once the temperature exceeded 830 °C, hardness increased with the temperature increase owing to the enrichment of carbon content in the martensite. With the increase in cyclic quenching times, hardness continuously increased with grain refinement strengthening. In addition, both tensile strength and elongation could be significantly improved through grain refinement. The relationships among wear loss, hardness and average grain size showed that wear resistance was affected by the synthesis reaction of grain refinement and hardness. Higher hardness and refined grain size contributed to improving the wear resistance of 65Mn low-alloy steel.

Strengthening Mechanism and Carbide Precipitation Behavior of Nb-Mo Microalloy Medium Mn Steel

This study investigates the strengthening mechanism and carbide precipitation behavior of medium Mn steel with Nb-Mo microalloy after cyclic quenching and austenite reverse transformation treatment. The results show that the Nb/Mo element not only precipitates (Nb,Mo)C in the grains, hindering the movement of dislocations and increases the strength, but also segregates at the austenite/ferrite grain boundary, thus delaying the transformation from austenite to ferrite. In addition, a large amount of nano-scale cementite is retained after cyclic quenching and austenite reverse transformation, which has a positive effect on the proportion of retained austenite in medium Mn steel. Moreover, the carbides with small size and low Mn content are dissolved, and the decomposed C and Mn content are beneficial to the nucleation of austenite during the intercritical annealing process at a temperature of 690 °C.

Austenite Stability and Deformation Behavior in Medium Mn Steel Processed by Cyclic Quenching ART Heat Treatment

This study investigated the austenite stability and deformation behavior of cyclic quenching-austenite reverse transformation processed Fe-0.25C-3.98Mn-1.22Al-0.20Si-0.19Mo-0.03Nb medium Mn steel. A number of findings were obtained. Most importantly, the extent of the TRIP effect was mainly determined by an appropriately retained austenite stability rather than its content. Simultaneously, chemical elements were the key factors affecting austenite stability, of which Mn had the greatest impact, while the difference of retained austenite grain size and Mn content resulted in different degrees of retained austenite stability. Additionally, there were still large amounts of strip and granular-retained austenite shown in the microstructure of the CQ3-ART sample after tensile fracture, revealing that the excessively stable, retained austenite inhibited the generation of an extensive TRIP effect.

A Novel Cyclic-Quenching-ART for Stabilizing Austenite in Nb–Mo Micro-Alloyed Medium-Mn Steel

In the context of obtaining an excellent elongation and tensile-strength combination in the third generation of advanced high strength steel, we emphasized the practical significance of adjusting the retained austenite fraction and stability in medium-Mn steel to obtain better mechanical properties. A novel cyclic quenching and austenite reverse transformation (CQ-ART) was used to obtain a large retained austenite content in Fe-0.25C-3.98Mn-1.22Al-0.20Si-0.19Mo-0.03Nb (wt.%) Nb–Mo micro-alloyed medium-Mn steel. The results show that after twice cyclic quenching and ART, the alloy exhibited optimum comprehensive properties, characterized by an ultimate tensile strength of 838 MPa, a total elongation of 90.8%, a product of strength and elongation of 76.1 GPa%, and the volume fraction of austenite of approximately 62 vol.%. The stability of retained austenite was significantly improved with the increasing of the number of cyclic quenching. Moreover, the effects of CQ-ART on the microstructure evolution, mechanical properties, C/Mn partitioning behavior, and austenite stability were investigated. Further, the strengthening effect of microalloying elements Nb–Mo was also discussed.

Microstructure and mechanical properties of Mo-Nb microalloyed medium Manganese trip Steel by cyclic quenching

A novel cyclic quenching (CQ) and austenite reverse transformation (ART) was proposed for a Fe-0.25C-3.98Mn-1.22Al-0.20Si-0.19Mo-0.03Nb (wt.%) Mo-Nb microalloyed medium-Mn TRIP steel to improve strength and ductility. The results show that after twice cyclic quenching and ART exhibited optimum comprehensive properties, characterized by an ultimate tensile strength of 838 MPa, a total elongation of 90.8%, a product of strength and elongation (PSE) of 76.1 GPa·%, and the volume fraction of austenite of approximately 62 vol.%.