Effect of cooling rate after heat treatment on pitting corrosion of super duplex stainless steel UNS S 32750

2018 ◽  
Vol 65 (5) ◽  
pp. 492-498 ◽  
Author(s):  
Byung-Hyun Shin ◽  
Junghyun Park ◽  
Jongbae Jeon ◽  
Sung-bo Heo ◽  
Wonsub Chung
Keyword(s):  
Heat Treatment ◽  
Stainless Steel ◽  
Corrosion Resistance ◽  
Cooling Rate ◽  
Pitting Corrosion ◽  
Heat Treatment Temperature ◽  
Secondary Phase ◽  
Treatment Temperature ◽  
Super Duplex Stainless Steel ◽  
Content Type

Purpose In this study, super duplex stainless steel (SDSS) was heat-treated. The purpose of this study is to assess the effect of the cooling rate after heat treatment on the pitting corrosion of SDSS. Design/methodology/approach The heat treatment from 1,000°C to 1,300°C was applied to SDSS to check the effect of the cooling rate. Findings The heat treatment temperature produced a different SDSS microstructure, and the cooling rate led to the growth of austenite. The casted SDSS indicated the presence of heterogeneous austenite, and the precipitation secondary phase under 1.6 per cent precipitated to bare metal. By applying heat treatment and cooling SDSS, its corrosion resistance changes because of the change in the chemical composition. The cooling rate at 5,600 J/s has the highest critical pitting temperature (CPT) at 1,100°C, and the cooling rate at 1.6 J/s has the highest CPT at 1,200°C. Low cooling rate (0.4 J/s) made the secondary phase at all temperature range. Research limitations/implications The effect of secondary phase not consider because that is well known to decreasing corrosion resistance. Practical implications Solution annealing is taken into account to optimize the corrosion resistance. But that is not consider the cooling rate at each temperature. This study assessed the effect of the cooling rate at each temperature point. Social implications Manufacturers need to know the effect of the cooling rate to optimize the corrosion resistance, and this study can be applied in the industrial scene. Originality/value SDSS is hard the optimization because SDSS is a dual-phase stainless steel. Corrosion resistance can be optimized by controlling heat treatment temperature and the cooling rate. Anyone not studied the effect of the cooling rate at each temperature. The effect of the cooling rate should be considered to optimize the corrosion resistance.

scholarly journals Effects of Si and Sn Contents and Heat-Treatment Temperature on the Corrosion Behavior of AISI 439 Ferrite Stainless Steel

2022 ◽  
Vol 60 (1) ◽  
pp. 26-34
Author(s):  
Chan Yang Kim ◽  
Do hyung Kim ◽  
Won sub Chung
Keyword(s):  
Heat Treatment ◽  
Stainless Steel ◽  
Corrosion Resistance ◽  
Passive Film ◽  
Heat Treatment Temperature ◽  
Inhibitory Effect ◽  
Heat Treatment Condition ◽  
Treatment Temperature ◽  
Fe Oxide ◽  
The Stability

This study was conducted to evaluate the corrosion resistance and optimize the heat-treatment process of AISI 439 ferrite stainless steel silicon and tin alloys with reduced chromium. The microstructure of the specimens and deposition under each condition were analyzed. The production of oxide films was compared based on the thickness of the film and the change in the contents of each element. In addition, electrochemical analyses of each heat-treatment condition was used to quantitatively compare corrosion resistance and passive film stability based on the relative chromium, silicon, and tin contents. It was found that the addition of silicon and tin compensated for the decrease in corrosion resistance induced by the chromium reduction. The addition of the two elements inhibited iron (Fe) oxide production in the surface oxide film, thereby improving the corrosion resistance of the material and improving the stability of the passive film. Moreover, the SiO2 and SnO2 layers inhibited the production of Fe oxide and contributed to the stability of the film along with Cr2O3, the main component of the passive film. However, when the heat treatment temperature increased above a specific temperature, the oxide inhibitory effect of the two elements was relatively offset. Nevertheless, further research to optimize the content of the three elements will help develop materials with superior mechanical properties and corrosion resistance.

scholarly journals Corrosion resistance of UNS S31803 stainless steel welded joints

2018 ◽  
Vol 24 (2) ◽  
pp. 147
Author(s):  
Paolo Ferro ◽  
Jan-Olof Nilsson ◽  
Franco Bonollo
Keyword(s):  
Heat Treatment ◽  
Stainless Steel ◽  
Corrosion Resistance ◽  
Welded Joints ◽  
Heat Treatment Temperature ◽  
Experimental Tests ◽  
Treatment Temperature ◽  
Gas Composition ◽  
Shielding Gas ◽  
Heat Treated

<p>The corrosion resistance of duplex stainless steel welded joints is affected by different parameters such as filler metal chemical composition, heat input, shielding gas composition and post welding heat treatment temperature. In most cases such parameters interact with each other so that it is very difficult to foresee their effect on corrosion resistance of welded joints without specific experimental tests. In this work the best combination of shielding gas composition and post welding heat treatment temperature that guarantees the corrosion resistance of the joint according to ASTM  A932, method C, was found.  Two shielding gases were tested during welding, Ar (100%) and a mixture of Ar (87%), He (10%) and N (3%), while the solution temperatures were 1050 °C and 1070 °C.  It was found that only the samples welded with the mixture of Ar (87%), He (10%), N (3%) as shielding gas and solution heat treated at 1070 °C passed the corrosion test completely.</p>

Precipitation condition and effect of volume fraction on corrosion properties of secondary phase on casted super-duplex stainless steel UNS S32750

2019 ◽  
Vol 66 (1) ◽  
pp. 61-66 ◽  
Author(s):  
Byung-Hyun Shin ◽  
Dohyung Kim ◽  
Sanghyup Park ◽  
Myungwon Hwang ◽  
Junghyun Park ◽  
...  
Keyword(s):  
Stainless Steel ◽  
Corrosion Resistance ◽  
Grain Boundary ◽  
Duplex Stainless Steel ◽  
Corrosion Behavior ◽  
Volume Fraction ◽  
Secondary Phase ◽  
Super Duplex Stainless Steel ◽  
Precipitation Condition ◽  
Content Type

Purpose The secondary phase decreased the corrosion resistance because of the segregation of Cr and Mo. Therefore, this paper aims to study the precipitation condition and the effect of secondary phase with volume fraction on corrosion behavior. Design/methodology/approach Secondary phase precipitated approximately from 375°C to 975°C because of saturated Cr and Mo at grain boundary by growth of austenite. Therefore, heat treatment from 800°C to 1,300°C was applied to start the precipitation of the secondary phase. Findings The secondary phase is precipitated at 1,020°C because of segregation by heterogeneous austenite. The growth of austenite at 1,000°C needs the time to saturate the Cr and Mo at grain boundary. When the volume fraction of austenite is 56 per cent (14 min at 1,000°C), the secondary phase is precipitated with grain boundary of austenite. The secondary phase increased the current density (corrosion rate) and decreased the passivation. That is checked to the critical pitting temperature (CPT) curves. The 1 per cent volume fraction of secondary phase decreased CPT to 60°C from 71°C. Research limitations/implications The precipitation of secondary phase not wants anyone. Casted super-duplex stainless steel (SDSS) of big size precipitates the secondary phase. This study worked the precipitation condition and the suppression conditions of secondary phase. Social implications Manufacturers need precipitation condition to make high-performance SDSS. Originality/value The corrosion resistance of SDSS is hard the optimization because SDSS is dual-phase stainless steel. The precipitation of the secondary phase must be controlled to optimize of the corrosion resistance of SDSS. Anyone not studied the precipitation condition of secondary phase and the effect of secondary phase with volume fraction on corrosion behavior of SDSS.

Effect of Heat Treatment Temperature and Lubricating Conditions on the Fretting Wear Behavior of SAF 2507 Super Duplex Stainless Steel

2019 ◽  
Vol 141 (10) ◽  
Author(s):  
Mengjiao Wang ◽  
Yunxia Wang ◽  
Jianzhang Wang ◽  
Na Fan ◽  
Fengyuan Yan
Keyword(s):  
Heat Treatment ◽  
Stainless Steel ◽  
Wear Resistance ◽  
Duplex Stainless Steel ◽  
Wear Behavior ◽  
Treatment Temperature ◽  
Fretting Wear ◽  
Super Duplex Stainless Steel ◽  
Wear Performance ◽  
Seawater Lubrication

Super duplex stainless steel (SDSS) has excellent mechanical properties and corrosion resistance. However, currently, there are few researches conducted on its fretting wear performance. This paper studies the influence of different heat treatment temperatures and medium environment on the fretting wear performance of SAF 2507 SDSS. Results show that the combined effect of the sigma phase and seawater lubrication can significantly improve the wear resistance of SAF 2507 SDSS. After treated with different heat treatment temperatures, different contents of sigma phases are precipitated out of SAF 2507 SDSS, which improves the wear resistance of the material to different degrees. In addition, the fretting wear performance of SAF 2507 SDSS also relates to the lubrication medium. In air, the friction and wear performance of SAF 2507 SDSS is poor, while in seawater, solution and corrosion products that acted as a lubricant dramatically improve the wear resistance of the material. Under the combined action of heat treatment and seawater lubrication medium, the friction coefficient and wear reduce by 70% and 91%, respectively.

Influence of Sigma Phase Precipitation on Pitting Corrosion of 2507 Super-Duplex Stainless Steel

2010 ◽  
Vol 658 ◽  
pp. 380-383 ◽  
Author(s):  
Ying Han ◽  
De Ning Zou ◽  
Wei Zhang ◽  
Jun Hui Yu ◽  
Yuan Yuan Qiao
Keyword(s):  
Stainless Steel ◽  
Corrosion Resistance ◽  
Ambient Temperature ◽  
Duplex Stainless Steel ◽  
Pitting Corrosion ◽  
Super Duplex Stainless Steel ◽  
Phase Precipitation ◽  
Pitting Potential ◽  
Σ Phase ◽  
Pitting Corrosion Resistance

Specimens of 2507 super-duplex stainless steel aging at 850°C for 5 min, 15 min and 60 min were investigated to evaluate the pitting corrosion resistance in 3.5% NaCl solution at 30°C and 50°C. The results are correlated with the microstructures obtained with different aging time. The precipitation of σ phase remarkably decreases the pitting corrosion resistance of the steel and the specimen aged for 60 min presents the lowest pitting potential at both 30°C and 50°C. With increasing the ambient temperature from 30°C to 50°C, the pitting potential exhibits a reduction tendency, while this tendency is less obviously in enhancing the ambient temperature than in extending the isothermal aging duration from 5 to 60 min. SEM analysis shows that the surrounding regions of σ phase are the preferable sites for the formation of corrosion pits which grew up subsequently. This may be attributed to the lower content of corrosion resistance elements in these regions formatted with σ phase precipitation.

scholarly journals Pitting Corrosion Resistance on Annealing Treated Super Duplex Stainless Steel S32750

Crystals ◽  
2020 ◽  
Vol 10 (4) ◽  
pp. 294
Author(s):  
Shuang Liu ◽  
Chaohua Yue ◽  
Xi Chen ◽  
Qiuhua Zhu ◽  
Yiyou Tu
Keyword(s):  
Stainless Steel ◽  
Corrosion Resistance ◽  
Duplex Stainless Steel ◽  
Pitting Corrosion ◽  
Annealing Temperature ◽  
Super Duplex Stainless Steel ◽  
Boundary Area ◽  
Pitting Potential ◽  
Pitting Corrosion Resistance ◽  
Equivalent Number

The pitting corrosion resistance of S32750 super duplex stainless steel, annealing treated at temperatures of 950–1200 °C for 20–60 min, was investigated using potentiodynamic polarization tests. The results show that the volume fractions of ferrite in the S32750 duplex stainless steel increased from 48.9% to 68.4% as annealing temperatures increased from 950 to 1200 °C. The pitting potential of the sample increased first and then decreased from an annealing temperature of 950 to 1050 °C, and the highest pitting potential was observed after annealing at 1050 °C for 35 min. The pitting corrosion resistance of S32750 stainless steel is due to the combination of pitting resistance equivalent number (PREN) value, phase fraction and grain boundary area fraction, and the imbalance of corrosion potential.

Heat Treatment Effect on Pitting Corrosion of Super Duplex Stainless Steel UNS S32750 GTA Welds

2013 ◽  
Vol 746 ◽  
pp. 467-472 ◽  
Author(s):  
In June Moon ◽  
Bok Su Jang ◽  
Jin Hyun Koh
Keyword(s):  
Heat Treatment ◽  
Stainless Steel ◽  
Duplex Stainless Steel ◽  
Pitting Corrosion ◽  
Super Duplex Stainless Steel ◽  
Σ Phase ◽  
Gas Tungsten Arc ◽  
Weld Metals ◽  
Pitting Corrosion Resistance ◽  
Heat Treated

The purpose of this study was to investigate the effect of heat treatment (930°C, 1080°C, 1230°C) followed by quenching on the pitting corrosion resistance, sigma phase precipitation, and microstructural change of a super duplex stainless steel (UNS S32750) welds made by gas tungsten arc (GTA). Based on the microstructural examination, the σ phase was formed in welds heat treated at 930°C while there were little σ phases formed in welds experienced the relatively fast cooling from 1080°C and 1230°C. Accordingly, the most weight loss due to pitting corrosion occurred in the as received base and weld metals heat treated at 930°C. It was confirmed that the pitting corrosion occurred in the phase boundaries of ferrite/sigma and austenite/sigma.

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